Spheroidizing Or Rounding Of Solid Glass Particles Patents (Class 65/21.3)
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Patent number: 11485681Abstract: Described are cementitious reagent materials produced from globally abundant inorganic feedstocks. Also described are methods for the manufacture of such cementitious reagent materials and forming the reagent materials as microspheroidal glassy particles. Also described are apparatuses, systems and methods for the thermochemical production of glassy cementitious reagents with spheroidal morphology. The apparatuses, systems and methods makes use of an in-flight melting/quenching technology such that solid particles are flown in suspension, melted in suspension, and then quenched in suspension. The cementitious reagents can be used in concrete to substantially reduce the CO2 emission associated with cement production.Type: GrantFiled: December 18, 2020Date of Patent: November 1, 2022Assignee: TERRA CO2 TECHNOLOGY HOLDINGS, INC.Inventor: Donald John Lake
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Patent number: 11326773Abstract: A waste heat recovery boiler in producing glass beads includes an equipment base arranged at the lower part of the waste heat recovery boiler. The upper part of the equipment base is connected with a cylindrical combustion production chamber, the lower part of the combustion production chamber is provided with a raw material inlet with single-layer or staggered layers. A finished product outlet is arranged at the lower end inside the combustion diffusion chamber, a membrane wall is arranged outside the combustion diffusion chamber, a steam-water lead-out straight tube system is symmetrically arranged at the upper end of the combustion diffusion chamber, a top annular water collecting tank is connected between the steam-water lead-out straight tube system and a steam-water lead-out tube system, and the steam-water lead-out tube system is connected with an upper drum.Type: GrantFiled: September 18, 2018Date of Patent: May 10, 2022Inventor: Shang-Yong Huang
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Patent number: 11017975Abstract: An apparatus for coupling to an input connection of an electron gun, the input connection having a heater terminal and a cathode terminal, includes: a connector having a first end and a second end; wherein the first end of the connector is configured to attach to a cable; wherein the second end of the connector is configured to connect to the input connection of the electron gun; and wherein the connector comprises an opening configured to receive the heater terminal of the input connection of the electron gun.Type: GrantFiled: December 20, 2019Date of Patent: May 25, 2021Assignee: Varian Medical Systems, Inc.Inventors: Mark E. Trail, Rudolf H. Potter
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Patent number: 10546711Abstract: An apparatus for coupling to an input connection of an electron gun, the input connection having a heater terminal and a cathode terminal, includes: a connector having a first end and a second end; wherein the first end of the connector is configured to attach to a cable; wherein the second end of the connector is configured to connect to the input connection of the electron gun; and wherein the connector comprises an opening configured to receive the heater terminal of the input connection of the electron gun.Type: GrantFiled: July 23, 2019Date of Patent: January 28, 2020Assignee: Varian Medical Systems, Inc.Inventors: Mark E. Trail, Rudolf H. Potter
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Publication number: 20150107301Abstract: The production of a quartz glass grit comprises the granulation of pyrogenetically produced silicic acid, and the formation of a SiO2 granulate and the vitrification of the SiO2 granulate using a treatment gas, which contains at least 30% by volume of helium and/or hydrogen. Said process is time consuming and cost intensive.Type: ApplicationFiled: April 17, 2013Publication date: April 23, 2015Inventors: Walter Lehmann, Achim Hofmann, Thomas Kayser, Martin Arndt
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Publication number: 20140212626Abstract: A process for making inorganic, metal oxide spheres that includes exposing solidified, molded microparticles that include a glass precursor composition to a temperature sufficient to transform the molded microparticles into molten glass and cooling the molten glass to form inorganic, metal oxide spheres.Type: ApplicationFiled: March 28, 2014Publication date: July 31, 2014Applicant: 3M INNOVATIVE PROPERTIES COMPANYInventors: David C. Kramlich, John L. Vandenberg, Matthew H. Frey, Scott R. Culler, Kathleen M. Schakel-Carlson
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Patent number: 8701441Abstract: A process for making inorganic, metal oxide spheres that includes exposing solidified, molded microparticles that include a glass precursor composition to a temperature sufficient to transform the molded microparticles into molten glass and cooling the molten glass to form inorganic, metal oxide spheres.Type: GrantFiled: August 21, 2006Date of Patent: April 22, 2014Assignee: 3M Innovative Properties CompanyInventors: David C. Kramlich, John L. Vandenberg, Matthew H. Frey, Scott R. Culler, Kathleen M. Schakel-Carlson
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Patent number: 8545733Abstract: Disclosed is a process for the manufacture of glass-crystalline particles comprising a glass component and a crystalline component comprising the steps of: a) providing a precursor solution comprising a solvent, a glass component composition, and a crystalline component composition; b) forming an aerosol comprising finely divided droplets of the precursor solution, wherein the droplet concentration which is below the concentration where collisions and subsequent coalescence of the droplets results in a 10% reduction in droplet concentration; c) heating the aerosol wherein, upon heating, glass-crystalline particles are formed, wherein the glass-crystalline particles comprise a glass component and a crystalline component, and wherein the crystalline component comprises one or more metal oxides; and d) isolating the glass-crystalline particles.Type: GrantFiled: September 27, 2010Date of Patent: October 1, 2013Assignee: E I du Pont de Nemours and CompanyInventors: Eric Lee Brantley, John T. Chaplinsky, Howard David Glicksman, James J. Krajewski, Brian J. Laughlin, Kurt Richard Mikeska, Lawrence V. Triboletti
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Publication number: 20130244857Abstract: The present invention relates to a dielectric ceramic composition for multilayer ceramic capacitor (MLCC), including a first component of 91 to 98 wt % and a second component of 2 to 9 wt %, wherein the first component includes a main component BaTiO3 of 94 to 98 wt %, a first subcomponent of 0.5 to 2 wt % including a glass powder having a mesh structure, and a second subcomponent of 1 to 4 wt % including at least one of MgO, Cr2O3 and Mn3O4, and the second component includes (Ba1-y-xCaySrx)(ZryTi1-y)O3, and x satisfies 0.2?x?0.8 and y satisfies 0.03?y?0.15.Type: ApplicationFiled: March 12, 2013Publication date: September 19, 2013Applicant: SAMHWA CAPACITOR CO., LTD.Inventors: Young Joo OH, Jung Rag YOON, Byong Chul WOO
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Publication number: 20130125586Abstract: A process for producing proppants from waste mineralogical material. The process can include providing the waste mineralogical material in a form such as particles, fines, dust, powders, and the like, and forming a plurality of “green” pellets from the waste mineralogical material. Thereafter, the plurality of green pellets are fed into a provided flame drop tower that has a combustion flame, a hot zone, and a collection basin located downstream from the hot zone. The plurality of green pellets pass through the hot zone, are melted and subsequently solidified in the shape of a sphere downstream from the hot zone to form vitrified glass spheres. In some instances, the vitrified glass spheres are subjected to a devitrification step.Type: ApplicationFiled: January 17, 2013Publication date: May 23, 2013Applicant: THE PENN STATE RESEARCH FOUNDATIONInventor: THE PENN STATE RESEARCH FOUNDATION
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Publication number: 20120175558Abstract: The invention relates to a process for preparing porous glass particles suitable for use as precursor materials for production of an opto-ceramic element. The process comprises: providing particles of a soluble glass composition comprising at least one soluble component, at least one component having low solubility in an aqueous solution, and at least one lasing dopant which also has a low solubility in the aqueous solution; and immersing the particles in an aqueous solution having low solubility for said at least one component and said at least one lasing dopant, to thereby dissolve substantially all of the soluble portions of the glass particles.Type: ApplicationFiled: July 25, 2007Publication date: July 12, 2012Inventors: Samuel David Conzone, Carol Click
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Patent number: 8117867Abstract: A process for producing spherical inorganic particles which have high flowability, can be incorporated in a high proportion, and are useful as a filler for composite substrates such as printed wiring boards and encapsulating materials. Also provided is a process for producing spherical inorganic particles which have high flowability and can be incorporated in a high proportion and which are useful as a filler for encapsulating materials and give an encapsulating material having high electrical insulating properties. One of the processes for producing spherical inorganic particles comprises: (a1) pulverizing a silicate-containing inorganic material to form a pulverization product; (b1) heating the pulverization product in an atomized state to form the pulverization product into spherical particles; (c1) spraying water over the spherical particles to cool them while maintaining the atomized state of the spherical particles; and (d1) collecting the spherical particles.Type: GrantFiled: August 9, 2006Date of Patent: February 21, 2012Assignee: Nitto Boseki Co., Ltd.Inventors: Shigeo Yamaguchi, Takeo Inoue
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Publication number: 20110233486Abstract: Disclosed is a process for the manufacture of glass-crystalline particles comprising a glass component and a crystalline component comprising the steps of: a) providing a precursor solution comprising a solvent, a glass component composition, and a crystalline component composition; b) forming an aerosol comprising finely divided droplets of the precursor solution, wherein the droplet concentration which is below the concentration where collisions and subsequent coalescence of the droplets results in a 10% reduction in droplet concentration; c) heating the aerosol wherein, upon heating, glass-crystalline particles are formed, wherein the glass-crystalline particles comprise a glass component and a crystalline component, and wherein the crystalline component comprises one or more metal oxides; and d) isolating the glass-crystalline particles.Type: ApplicationFiled: September 27, 2010Publication date: September 29, 2011Applicant: E. I. DU PONT DE NEMOURS AND COMPANYInventors: Eric Lee Brantley, John T. Chaplinsky, Howard David Glicksman, James J. Krajewski, Brian J. Laughlin, Kurt Richard Mikeska, Lawrence V. Triboletti
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Patent number: 7927670Abstract: The invention concerns silica microspheres (M) having an outer diameter between 50 and 125 ?m, preferably between 60 and 90 ?m, a wall thickness not less than 1 ?m, preferably between 1 and 3 ?m and a density between 0.3 and 0.7/cm3, a manufacturing method by injecting silica microsphere precursors (MS, PR1, PR1?, PR2?) into an inductive plasma (P), assembly methods and possible uses of silica microspheres.Type: GrantFiled: September 19, 2005Date of Patent: April 19, 2011Inventor: Sylvain Rakotoarison
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Patent number: 7884055Abstract: A method and apparatus for manufacturing ceramic microspheres from industrial slag. The microspheres have a particle size of about 38 microns to about 150 microns. The microspheres are used to create a cement slurry having a density of at least about 11 lbs/g. The resultant cement slurry may then be used to treat subterranean wells.Type: GrantFiled: December 4, 2008Date of Patent: February 8, 2011Assignee: Intevep, S.A.Inventors: George Quercia, Yibran Perera, Aiskely Blanco, Fedymar Pereira
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Patent number: 7858148Abstract: Artificial turf for use with an artificial turf system, which may also include a base layer and a support layer. The artificial turf comprising a backing supporting pile tufts of between ¼? to 4? in length, in position on its upper surface. The backing may comprise a porous synthetic foam or backing sheet. A filler of particles shaped to have no sharp edges and of substantially equal size are interspersed over the backing and about the tufts up to at least half thick length. The artificial turf substantially retains its resiliency, porosity and equal density throughout.Type: GrantFiled: March 5, 2007Date of Patent: December 28, 2010Assignee: USGreentech, L.L.C.Inventor: Randolph S. Reddick
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Patent number: 7787984Abstract: A sphering apparatus includes a sphering furnace on a body of which a plurality of adhesion preventing air-introducing holes is formed and at a lower position of which a carrier air-introducing hole and a carrier air-withdrawing hole are formed; an air blower introducing both an adhesion preventing air and a carrier air; a first pipe one end of which is connected to a discharging part of the air blower and the other end of which is biforked, one biforked end being connected to the carrier air-introducing hole and the other biforked end being connected to a manifold bundling the plurality of adhesion preventing air-introducing holes; a first damper provided in any one of two pipes in the biforked part of the first pipe; a cyclone connected to the carrier air-withdrawing hole through a second pipe; and a bag filter connected to the cyclone through a third pipe.Type: GrantFiled: September 22, 2005Date of Patent: August 31, 2010Assignee: Taiyo Nippon Sanso CorporationInventors: Yoshiyuki Hagiwara, Shinichi Miyake
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Patent number: 7631518Abstract: Methods for producing glass powders are provided. The methods include generating an aerosol stream comprising droplets that include a liquid and a glass precursor. Glass particles are formed in the aerosol stream having a small average particle size. The powders can also have a small particle size, narrow size distribution, a high density and a spherical morphology. The invention also includes devices and products formed from the glass powders.Type: GrantFiled: December 3, 2004Date of Patent: December 15, 2009Assignee: Cabot CorporationInventors: Toivo T. Kodas, Mark J. Hampden-Smith, James Caruso, Quint H. Powell, Audunn Ludviksson
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Publication number: 20090249833Abstract: A process for producing spherical inorganic particles which have high flowability, can be incorporated in a high proportion, and are useful as a filler for composite substrates such as printed wiring boards and encapsulating materials. Also provided is a process for producing spherical inorganic particles which have high flowability and can be incorporated in a high proportion and which are useful as a filler for encapsulating materials and give an encapsulating material having high electrical insulating properties. One of the processes for producing spherical inorganic particles comprises: (a1) pulverizing a silicate-containing inorganic material to form a pulverization product; (b1) heating the pulverization product in an atomized state to form the pulverization product into spherical particles; (c1) spraying water over the spherical particles to cool them while maintaining the atomized state of the spherical particles; and (d1) collecting the spherical particles.Type: ApplicationFiled: August 9, 2006Publication date: October 8, 2009Applicant: Nitto Boseki Co., Ltd.Inventors: Shigeo Yamaguchi, Takeo Inoue
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Patent number: 7328594Abstract: A process for stably and efficiently producing quality glass articles such as preforms at high yields, and a process for producing an optical device from the preform obtained by the above process. In the process for producing a glass article, molten glass gobs having a predetermined weight each are poured, or molten glass drops having a predetermined weight each are dropped through a nozzle, into a boiling liquid having a boiling point lower than the class transition temperature of the glass constituting said glass article or a liquid which is temperature-adjusted beforehand so as to be caused to boil by the amount of heat of the glass, to form glass articles.Type: GrantFiled: December 12, 2002Date of Patent: February 12, 2008Assignee: Hoya CorporationInventors: Akira Murakami, Katsumi Utsugi, Yoshinori Iguchi, Masahiro Yoshida, Yoshikane Shinkuma, Atsushi Watabe
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Patent number: 7297646Abstract: Ceramics comprising (i) at least one of Nb2O5 or Ta2O5 and (ii) at least two of (a) Al2O3, (b) REO, or (c) at least one of ZrO2 or HfO2. Embodiments of ceramics according to the present invention can be made, formed as, or converted into optical waveguides, glass beads, articles (e.g., plates), fibers, particles (e.g., abrasive particles), and thin coatings.Type: GrantFiled: September 25, 2006Date of Patent: November 20, 2007Assignee: 3M Innovative Properties CompanyInventors: Anatoly Z. Rosenflanz, Craig R. Schardt
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Patent number: 7240518Abstract: The apparatus for producing glass beads of the present invention comprises a melting pot 2 for heating and melting glass, a nozzle 2A for dripping molten glass 4 in the melting pot 2, which is disposed at the bottom of the melting pot 2, and a liquid glass droplet receiver 11 filled with cooling solution 150 for cooling the liquid glass droplet 10 dripped from the nozzle 2A, which is disposed under the nozzle 2A, wherein the cooling solution 150 is made from a material that forms a bubble layer around the liquid glass droplet 10 as the cooling solution 150 is vaporized due to the heat of the liquid glass droplet 10 during a period when the liquid glass droplet 10 is cooled down to a temperature lower than the glass transfer temperature in the cooling solution 150.Type: GrantFiled: December 25, 2002Date of Patent: July 10, 2007Assignee: Matsushita Electric Industrial Co., Ltd.Inventors: Masahiro Hiraka, Shigeo Furukawa, Mitsuhiro Fujita
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Patent number: 7093463Abstract: A method for producing powders that consist of substantially spherical particles from a material such as glass, ceramics or plastic that produces a highly viscous melt that solidifies at a glass transition temperature Tg or at a solidification temperature Ts. The inventive method comprises the following steps: (a) producing a melt of a viscosity ? in the range of from 0.1 to 100 Ns/m2; (b) atomizing the melt using a first gas, the first gas having a temperature TA?Tg or ?0.5Ts at the outlet of the nozzle and (c) cooling off the particles produced by atomization in a cooling section downstream of the nozzle using a coolant, the temperature of the coolant being smaller than Ts or Tg.Type: GrantFiled: October 9, 2000Date of Patent: August 22, 2006Assignee: Applikations-und Technikzentrum fur Energieverfahrens-Umwelt-und Stromungstechnik (ATZ-EVUS)Inventors: Gerhard Wolf, Andreas Emmel
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Patent number: 7059153Abstract: A powder of solid and spherical glass particles is easily manufactured by subjecting a mixed solution of a raw material oxide powder comprising a glass network-forming element, and an aqueous solution of a water-soluble compound comprising a glass-forming element other than the element of the raw material oxide powder to spray-thermal decomposition, wherein the spray-thermal decomposition temperature is set to be in a specific range according to the amount of the raw material oxide powder in the total of the amount of the raw material oxide powder and the oxide-converted amount of the water-soluble compound, as well as the average particle size of the glass powder to be manufactured.Type: GrantFiled: May 30, 2001Date of Patent: June 13, 2006Assignee: Murata Manufacturing Co., Ltd.Inventors: Koji Hattori, Shinsei Okabe, Toshiyuki Miyoshi
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Publication number: 20040261454Abstract: Disclosed are a process for producing a glass shaped material having high quality and high mass accuracy and a process for producing an optical element, which includes the preparation of a glass shaped material having high quality and high mass accuracy, the heating of said glass shaped material and the precision-press-molding thereof.Type: ApplicationFiled: June 23, 2004Publication date: December 30, 2004Applicant: Hoya CorporationInventors: Masahiro Yoshida, Yoshikane Shinkuma, Xuelu Zou
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Publication number: 20040259713Abstract: The present invention relates to microspheres (i.e., beads) that comprise titania and bismuth oxide. The glass microspheres further comprise zirconia. The invention also relates to retroreflective articles, and in particular pavement markings, comprising such microspheres.Type: ApplicationFiled: June 11, 2003Publication date: December 23, 2004Applicant: 3M Innovative Properties CompanyInventor: Matthew H. Frey
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Patent number: 6758062Abstract: The present invention intends to provide a manufacturing method for a plasma display panel, so as to overcome problems associated with a withstanding voltage of a dielectric glass layer. Glass particles have angular shapes after grinding with a grinder, but as the surface of them has been melted, they are converted into spheroids. Those glass particles can get wet evenly, so that a binder evenly adheres to the surface of a glass particle when a glass paste including the glass particles is applied to the surface of a substrate. In this case, there is a scarce possibility for a gas, generated by baking the binder, to remain in the form of bubbles in a formed dielectric glass layer. There are fewer bubbles remaining in a completed dielectric glass layer than in a dielectric glass layer than in a glass layer made from angular glass particles.Type: GrantFiled: August 1, 2001Date of Patent: July 6, 2004Assignee: Matsushita Electric Industrial Co., Ltd.Inventors: Taku Watanabe, Masaki Aoki, Shigeo Suzuki
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Patent number: 6742364Abstract: A method of manufacturing a micro molten glass droplet, has the steps of, colliding a molten glass droplet with a micro through hole formed in a plate-shaped member; and pushing out at least part of the glass droplet to a reverse surface of the micro through hole as a micro droplet, thereby forming a glass droplet with a diameter of not more than 5 mm.Type: GrantFiled: August 17, 2001Date of Patent: June 1, 2004Assignee: Minolta Co., Ltd.Inventor: Shinichi Nishikawa
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Publication number: 20020139144Abstract: The present invention intends to provide a manufacturing method for a plasma display panel, so as to overcome problems associated with a withstanding voltage of a dielectric glass layer,Type: ApplicationFiled: August 1, 2001Publication date: October 3, 2002Inventors: Taku Watanabe, Masaki Aoki, Shigeo Suzuki
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Publication number: 20020121108Abstract: A retrofit technology for air-fuel fired, vertical glass furnace for oxygen firing or boosting to provide additional heat to the process to increase furnace production capacity. The additional firing using oxygen is strategically controlled to enable enhanced radiation from oxygen flame for the spheroidizing process without negative effects on the overall process. With proper implementation, an increased production from 50% to 200%, depending on the size of the spheres, can be achieved while maintaining acceptable product quality. Processes in accordance with the present invention can be performed using one of a number of methods of oxygen boosting.Type: ApplicationFiled: October 19, 2001Publication date: September 5, 2002Inventors: Eric Streicher, John Foss, Mahendra L. Joshi, Harley A. Borders
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Publication number: 20020053223Abstract: A method of manufacturing a micro molten glass droplet, has the steps of, colliding a molten glass droplet with a micro through hole formed in a plate-shaped member; and pushing out at least part of the glass droplet to a reverse surface of the micro through hole as a micro droplet, thereby forming a glass droplet with a diameter of not more than 5 mm.Type: ApplicationFiled: August 17, 2001Publication date: May 9, 2002Inventor: Shinichi Nishikawa
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Patent number: 6358531Abstract: A method is provided for preparing shells, concentric shells or porous, homogenous gels from alkali borate glass particles at low temperatures (i.e. room temperature or less than above 100° C.). The alkali borate glass particles contain one or more cations such as aluminum which react with an aqueous solution containing an anion such as hydroxide to form an aqueous insoluble material having a solubility limit of less than about 0.01 wt. percent. The resulting shells or gels may be used in many different applications such as a filler in resins, as filters, precursors for nano-sized powders, as thin surface films or catalyst support media. The resulting shells or gels may also have a chemotherapeutic drug added thereto, following which the resulting product is administered to a mammal and the insoluble material is dissolved form the product in vivo through administration of chelating agent.Type: GrantFiled: February 1, 1999Date of Patent: March 19, 2002Assignee: The Curators of the University of MissouriInventors: Delbert E. Day, Samuel D. Conzone
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Publication number: 20020007650Abstract: A powder of solid and spherical glass particles is easily manufactured by subjecting a mixed solution of a raw material oxide powder comprising a glass network-forming element, and an aqueous solution of a water-soluble compound comprising a glass-forming element other than the element of the raw material oxide powder to spray-thermal decomposition, wherein the spray-thermal decomposition temperature is set to be in a specific range according to the amount of the raw material oxide powder in the total of the amount of the raw material oxide powder and the oxide-converted amount of the water-soluble compound, as well as the average particle size of the glass powder to be manufactured.Type: ApplicationFiled: May 30, 2001Publication date: January 24, 2002Applicant: Murata Manufacturing Co., Ltd.Inventors: Koji Hattori, Shinsei Okabe, Toshiyuki Miyoshi