Having Soot Forming Flame Hydrolysis Burner (e.g., Flame Oxidation, Etc.) Patents (Class 65/531)
  • Patent number: 11981595
    Abstract: This burner for producing a fine glass particle deposited body is provided with a metallic gas-feed pipe that forms a burner body, and a cover for covering the gas-feed pipe, wherein: the gas-feed pipe and the cover are integrally formed; the gas-feed pipe has connected thereto a piping through which material gas, oxyhydrogen gas, and seal gas are supplied; and the cover covers, in the axial direction of the burner over a prescribed length and in a given constant outer diameter, the gas-feed pipe and a connection part of the piping connected to a lateral surface of the gas-feed pipe.
    Type: Grant
    Filed: December 4, 2019
    Date of Patent: May 14, 2024
    Assignee: SUMITOMO ELECTRIC INDUSTRIES, LTD.
    Inventor: Tomomi Moriya
  • Patent number: 9032761
    Abstract: Provided is a porous glass matrix producing burner 10, wherein a third gas jetting opening 17, which is the most outward one of a plurality of gas jetting openings, is clogged by a clogging member 19, and one line or plural lines of gas jetting holes 20 are provided in the clogging member 19 concentrically with respect to the center line of a glass material gas jetting port 11. Hence, there are provided a porous glass matrix producing burner that can have the cross-sectional area of its most outward gas jetting opening changed and can have the flow rate and linear velocity of a combustion improving gas adjusted to thereby suppress diffusion of the combustion improving gas and a combustible gas and improve deposition efficiency, and a porous glass matrix producing method using the porous glass matrix producing burner.
    Type: Grant
    Filed: October 17, 2012
    Date of Patent: May 19, 2015
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventor: Makoto Yoshida
  • Publication number: 20140338400
    Abstract: A soot glass deposit body is manufactured by placing a starting rod and a burner 22 for producing glass particulates in a reaction container, introducing a source material gas to the burner 22 through a supplying pipe 26, producing glass particulates by a pyrolytic oxidation reaction of the source material gas in a flame formed by the burner 22, and depositing the produced glass particulates on the starting rod. At the time, the source material gas to be supplied to the burner 22 is a siloxane, the burner 22 is heated so that temperature of the burner 22 falls within the range of from ?30° C. to +30° C. relative to the boiling point of the siloxane, and also temperature of the supplying pipe is controlled within the range of from the boiling point of the siloxane to the boiling point plus 30° C.
    Type: Application
    Filed: May 13, 2014
    Publication date: November 20, 2014
    Applicant: SUMITOMO ELECTRIC INDUSTRIES, LTD.
    Inventors: Takashi YAMAZAKI, Tomohiro ISHIHARA
  • Patent number: 8869565
    Abstract: A method of producing optical fiber preform includes: forming a deposited layer by depositing glass particles on a periphery of a target element in a deposition mode while burning a mixed gas containing a glass source material gas, a flaming gas, and a supporting gas by use of a flaming burner; maintaining a state where the supporting gas flows at a flow velocity greater than or equal to a flow velocity at which a nozzle end of the supporting gas discharge nozzles does not glow while maintaining a pilot burner by allowing the flaming gas to flow to the seal gas discharge nozzle after a seal gas is replaced with the flaming gas in a case where a mode is changed from the deposition mode to a non-deposition mode; and replacing the flaming gas flowing to the flaming gas port with a purge gas.
    Type: Grant
    Filed: May 1, 2012
    Date of Patent: October 28, 2014
    Assignee: Fujikura Ltd.
    Inventors: Naritoshi Yamada, Shunichirou Hirafune
  • Patent number: 8840858
    Abstract: An apparatus for mixing a vaporized precursor with a gas for producing silica particles is provided. The apparatus includes a mixer housing, a precursor delivery chamber having an output in communication with the mixer housing for delivering a vaporized precursor in the mixer housing, and an oxidizing gas delivery chamber having an output in communication with the mixer housing for delivering an oxidizing gas to be mixed with the vaporized precursor. The apparatus further includes a flashback member disposed within the mixer housing and between the output of the precursor delivery chamber and the output of the oxidizing gas delivery chamber. The flashback member is located at a minimum distance from the output of the oxidizing gas delivery chamber defined by Lminimum (cm)=0.453 U (Re)?0.5567, wherein U is the flow rate in cm/sec of precursor and Re is the flow Reynolds number. The flashback member may include a tapered surface on at least one side to reduce recirculation of vaporized gas.
    Type: Grant
    Filed: July 6, 2011
    Date of Patent: September 23, 2014
    Assignee: Corning Incorporated
    Inventors: Lewis A Bernstein, Dana Craig Bookbinder, Jason A Dillard, Jennifer L Porter, Balram Suman, Pushkar Tandon
  • Publication number: 20140223966
    Abstract: A porous glass base material manufacturing burner comprising a combustible gas emission nozzle having one or more rows of small-diameter combustion assisting gas emission nozzles arranged around a central glass raw material gas emission nozzle,. When a cross section of the burner formed by cleaving in a direction perpendicular to a central axis of the burner is divided into four equal regions by two orthogonal straight lines intersecting at a center of the cross section, total flow path surface area of the small-diameter combustion assisting gas emission nozzles included in two of the four regions through which passes a straight line running along the starting member and through the center of the cross section is less than the total flow path surface area of the small-diameter combustion assisting gas emission nozzles included in the other two of the four regions.
    Type: Application
    Filed: February 12, 2014
    Publication date: August 14, 2014
    Applicant: SHIN-ETSU CHEMICAL CO., LTD.
    Inventor: Makoto YOSHIDA
  • Patent number: 8783069
    Abstract: In a known process for producing a quartz glass cylinder, a porous soot tube, which is sintered to form the quartz glass cylinder, is produced by depositing SiO2 particles on an outer cylindrical surface of a support, which rotates about the longitudinal axis thereof and has a layer of silicon carbide (SiC layer). In order on this basis to specify a support having a high resistance to fracture, which firstly can easily be removed and which secondly presents a low risk of contamination for the soot body, the invention proposes that the SiC layer is treated at a high temperature in an oxygen-containing atmosphere before the SiO2 particles are deposited, in such a manner that an SiO2 protective layer having a thickness of at least 0.1 ?m is produced by oxidation.
    Type: Grant
    Filed: September 14, 2010
    Date of Patent: July 22, 2014
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Anke Schuster, Rene Sowa, Martin Trommer, Udo Peper
  • Publication number: 20140174135
    Abstract: A glass fine particle synthesis burner comprising a glass raw material gas emission path for emitting glass raw material; a ring-shaped combustible gas emission path for emitting combustible gas arranged outside the glass raw material emission path; a ring-shaped combustion aiding gas emission path for emitting combustion aiding gas arranged outside the combustible gas emission path; and small diameter nozzles for emitting the combustion aiding gas within the combustible gas emission path. In a cross section of the glass fine particle synthesis burner formed by cleaving orthogonal to a central axis thereof, when the glass fine particle synthesis burner is divided into two regions by a predetermined straight line passing through a center of the glass fine particle synthesis burner, a total area of the small diameter nozzles in one of the regions is greater than a total area of the small diameter nozzles in the other region.
    Type: Application
    Filed: December 16, 2013
    Publication date: June 26, 2014
    Applicant: SHIN-ETSU CHEMICAL CO., LTD.
    Inventor: Yuhei URATA
  • Patent number: 8746013
    Abstract: The invention relates to a burner module having a body that is either sintered or photo-cured, and to methods of making such a burner module. The body (110) of the burner (100) is formed from one of a sintered metal, a sintered alloy, a laminated glass ceramic, and a photo-cured polymer. 1 Sintering and photo-curing may be accomplished by irradiating the body with localized heating using a focused energy source, such as a laser. The burner module is resistant to thermal shock and provides a distributed, even stream of a precursor or precursors to be reacted in a flame of the burner module to form soot, which is to deposited on a receptor surface, and may be used for vapor and liquid precursor delivery systems. A soot deposition system having an array of such burner modules and methods of making a fused silica article by depositing soot using the burner modules are also described.
    Type: Grant
    Filed: March 25, 2008
    Date of Patent: June 10, 2014
    Assignee: Corning Incorporated
    Inventors: Muluwork Geremew, Daniel Warren Hawtof, Richard Curwood Peterson, Amy Lu Rovelstad, Christopher Clark Thompson
  • Patent number: 8695380
    Abstract: The present invention provides a quartz glass burner that can enhance the heating power of flame working without unnecessarily increasing the flow of combustion gas and improve the deposition efficiency on depositing glass particles onto a porous glass preform. The quartz glass burner has a large diameter outer tube, and a plurality of small diameter inner tubes enclosed in the outer tube, and a tip of the outer tube has a port defining member defining the outer shape of a combustion gas ejecting port that ejects combustion gas, and the port defining member protrudes from the inner circumference of the outer tube towards the center axis so as to block the outermost area including areas between the outer circumferences of a plurality of inner tubes forming the inner tube row and the inner circumference of the outer tube of the combustion gas flow path.
    Type: Grant
    Filed: September 19, 2011
    Date of Patent: April 15, 2014
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventor: Makoto Yoshida
  • Patent number: 8590344
    Abstract: The invention relates to a known method for the production of a cylinder from quartz glass, comprising a step, wherein an SiO2 body which comprises a porous SiO2 soot layer and has a lower end, an upper end, and an outer casing, is sintered to form said quartz glass cylinder in a vitrification furnace, and is being held in a vertical orientation by means of a retaining device, which comprises an upper retaining element connected at the upper end of the SiO2 body, and a lower retaining element disposed on the lower end. In order to provide a method based thereon, by means of which even heavy bodies made of porous SiO2 can be safely retained during vitrification, the invention provides that the retaining device has a dimensionally stable connecting part, which extends inside the vitrification furnace along the outer casing of the SiO2 body and which connects the upper and the lower retaining elements to each other.
    Type: Grant
    Filed: May 14, 2009
    Date of Patent: November 26, 2013
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Thomas Krause, Udo Peper, Steffen Zwarg, René Sowa
  • Patent number: 8567218
    Abstract: A burner for a vapour deposition process has a central nozzle for ejecting a glass precursor material, at least a crown of nozzles surrounding said central nozzle for ejecting a flame reactant, and a circular nozzle between said central nozzle and said crown of nozzles for ejecting an innershield gas, wherein the central nozzle has a concave shape in a cross section in the axial plane and, preferably, a symmetry about an axial plane.
    Type: Grant
    Filed: December 20, 2002
    Date of Patent: October 29, 2013
    Assignee: Prysmian Cavi e Sistemi Energia S.r.l.
    Inventors: Carlo Cognolato, Francesco Mole′, Andrea Demergazzi, Franco Veronelli
  • Patent number: 8561432
    Abstract: The present invention provides an apparatus for fabricating porous glass preforms, in which any damages of a reaction vessel due to the increase in thermal load to the reaction vessel can be controlled without enlarging the reaction vessel. A wall of the reaction vessel includes a plurality of rectangular inner wall metal plates that defines at least apart of inner side walls of the reaction vessel, adjacent inner wall metal plates of a plurality of inner wall metal plates of which being weld bonded at their edges, and a plurality of metal frame members having higher stiffness than that of the inner wall metal plates and being arranged along each edge region of the opposite surface of the inner side walls of each of the plurality of inner wall metal plates and fixed to the edge region by a tightening or welding means.
    Type: Grant
    Filed: September 19, 2011
    Date of Patent: October 22, 2013
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventor: Makoto Yoshida
  • Patent number: 8517721
    Abstract: A burner for fabricating an optical fiber preform, which can suppress the adhesion and deposition of glass particles to the front end of the burner without enlarging the burner diameter, is provided. The burner has a first tube, a second tube and a third tube coaxially arranged and define a glass raw material gas port, a sealing gas port, and a burnable gas port by the front end portions thereof, and a plurality of small diameter nozzles arranged between the second tube and the third tube, each of the nozzles arranged on a concentric circle relative to the glass raw material gas port and defines a combustion assisting gas port by the front end portion thereof, the front end portion of the second tube protrudes ahead of that of the first tube, and the front end portion of the third tube protrudes ahead of those of the second tube and each of the nozzles.
    Type: Grant
    Filed: February 27, 2009
    Date of Patent: August 27, 2013
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventor: Makoto Yoshida
  • Publication number: 20130160496
    Abstract: A method for producing rod lenses with an enveloping diameter of the rod lens face of up to 200 mm and an edge length of at least 800 mm. The method is characterized in that fabrication is performed from a cylindrical rod lens element made from synthetic quartz glass material configured as a fused silica ingot. This is performed using a flame hydrolysis method with a direct one stage deposition process of SIOx particles from a flame stream onto die that rotates and is moveable in a linear manner with respect to the flame stream.
    Type: Application
    Filed: December 20, 2012
    Publication date: June 27, 2013
    Applicant: J-PLASMA GMBH
    Inventor: j-plasma GmbH
  • Patent number: 8459063
    Abstract: A multi-nozzle type burner is used for producing a porous glass preform, the burner having small variations in deposition efficiency with the burner tip being not burned even when axial shift occurs at the concentric multi-tube part of the burner. The present invention provides a burner for producing a porous glass preform with a concentric multi-tube structure, comprising a glass material gas jet port in a center, a plurality of gas jet ports concentrically disposed outside the glass material gas jet port, and small-diameter gas jet ports which are disposed in a line or a plurality of lines concentrically to the glass material gas jet port so as to be enclosed in one of the gas jet ports other than the gas jet ports in the center and at an outermost side, the small-diameter gas jet ports in the same line having an identical focal length.
    Type: Grant
    Filed: April 22, 2011
    Date of Patent: June 11, 2013
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventor: Makoto Yoshida
  • Publication number: 20130091900
    Abstract: Provided is a porous glass matrix producing burner 10, wherein a third gas jetting opening 17, which is the most outward one of a plurality of gas jetting openings, is clogged by a clogging member 19, and one line or plural lines of gas jetting holes 20 are provided in the clogging member 19 concentrically with respect to the center line of a glass material gas jetting port 11. Hence, there are provided a porous glass matrix producing burner that can have the cross-sectional area of its most outward gas jetting opening changed and can have the flow rate and linear velocity of a combustion improving gas adjusted to thereby suppress diffusion of the combustion improving gas and a combustible gas and improve deposition efficiency, and a porous glass matrix producing method using the porous glass matrix producing burner.
    Type: Application
    Filed: October 17, 2012
    Publication date: April 18, 2013
    Applicant: SHIN-ETSU CHEMICAL CO., LTD.
    Inventor: SHIN-ETSU CHEMICAL CO., LTD.
  • Publication number: 20130074552
    Abstract: Provided is a method for manufacturing an optical fiber preform using a combustion burner. The method includes at least one of: a step ? of, when a mode is changed from a deposition mode to a non-deposition mode, changing a gas discharged from a combustion gas port of the burner from a combustion gas to a purge gas, while maintaining a pilot light and a flow rate of a supporting gas from supporting gas discharge nozzles of the burner so that the nozzle tip does not glow; and a step ? of, when the mode is changed from the non-deposition mode to the deposition mode, changing a gas discharged from the combustion gas port from a purge gas to a combustion gas, while maintaining a pilot light and the flow rate of the supporting gas so that the nozzle tip does not glow.
    Type: Application
    Filed: November 21, 2012
    Publication date: March 28, 2013
    Applicant: FUJIKURA LTD.
    Inventor: FUJIKURA LTD.
  • Publication number: 20120312054
    Abstract: Apparatus and methods for making an optical fiber preform at low cost avoiding the apparatus from being damaged are provided. Apparatus for making an optical fiber preform by depositing glass particles on the circumferential surface of a glass rod comprises: a chamber, a plasma torch, a glass particle supplying part, a composition modification gas supplying part, and an exhaust part. The chamber surrounds the heating portion of the glass rod heated by the plasma torch. The plasma torch heats the glass particles by a plasma flame. The glass particle supplying part introduces glass particles towards the heating portion of the glass rod in the chamber. The composition modification gas supplying part introduces composition modification gas into the chamber in order to modify the composition of the glass particles to be deposited on the heating portion of the glass rod in the chamber.
    Type: Application
    Filed: June 1, 2012
    Publication date: December 13, 2012
    Applicant: SUMITOMO ELECTRIC INDUSTRIES, LTD.
    Inventor: Tetsuya NAKANISHI
  • Patent number: 8312744
    Abstract: There is provided a burner for producing glass fine particles, including: a glass material gas discharge port; a combustible gas discharge port that is provided so as to surround the glass material gas discharge port, a center of the combustible gas discharge port being positioned on a center of the glass material gas discharge port; and a plurality of small-diameter oxidizing gas discharge ports that are provided within the combustible gas discharge port in one or more concentric circles with respect to the glass material gas discharge port.
    Type: Grant
    Filed: February 23, 2010
    Date of Patent: November 20, 2012
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventor: Makoto Yoshida
  • Publication number: 20120279259
    Abstract: A method of producing optical fiber preform includes: forming a deposited layer by depositing glass particles on a periphery of a target element in a deposition mode while burning a mixed gas containing a glass source material gas, a flaming gas, and a supporting gas by use of a flaming burner; maintaining a state where the supporting gas flows at a flow velocity greater than or equal to a flow velocity at which a nozzle end of the supporting gas discharge nozzles does not glow while maintaining a pilot burner by allowing the flaming gas to flow to the seal gas discharge nozzle after a seal gas is replaced with the flaming gas in a case where a mode is changed from the deposition mode to a non-deposition mode; and replacing the flaming gas flowing to the flaming gas port with a purge gas.
    Type: Application
    Filed: May 1, 2012
    Publication date: November 8, 2012
    Applicant: FUJIKURA LTD.
    Inventors: Naritoshi YAMADA, Shunichirou HIRAFUNE
  • Patent number: 8266928
    Abstract: Provided is a burner for manufacturing a porous glass base material, the burner having: a glass raw material gas ejection port; a burnable gas ejection port provided around and centered on the glass raw material gas ejection port; and one or more sequences of small diameter auxiliary gas ejection ports provided inside the burnable gas ejection port, to be coaxial with respect to the glass raw material gas ejection port, where in each of the sequences, the small diameter auxiliary gas ejection ports have the same focal length as each other, and have a concave portion at an end surface thereof.
    Type: Grant
    Filed: February 22, 2010
    Date of Patent: September 18, 2012
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventor: Makoto Yoshida
  • Patent number: 8245543
    Abstract: To provide a method for the inexpensive manufacture of a deposition burner with small manufacturing tolerances for use in the synthesis of quartz glass, and wherein moreover, when the deposition burner is used as intended, the risk of contamination of the quartz glass to be produced is low, the invention suggests the following method steps: (a) providing a start cylinder of quartz glass (40) which is mechanically provided with longitudinal bores (46, 47); (b) elongating the start cylinder with formation of a burner strand (42), the longitudinal bores being shaped as elongated channels extending in parallel with one another; (c) cutting the burner strand into pieces in the form of cylindrical quartz glass blocks (43), each being provided with passage lines extending in parallel with a central axis of the quartz glass block; and (d) manufacturing the deposition burner by using a respective one of such quartz glass blocks as burner head which has a proximal end and a distal end, the passage lines serving the sup
    Type: Grant
    Filed: May 21, 2008
    Date of Patent: August 21, 2012
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventor: Michael Huenermann
  • Publication number: 20120073332
    Abstract: The present invention provides a quartz glass burner that can enhance the heating power of flame working without unnecessarily increasing the flow of combustion gas and improve the deposition efficiency on depositing glass particles onto a porous glass preform. The quartz glass burner has a large diameter outer tube, and a plurality of small diameter inner tubes enclosed in the outer tube, and a tip of the outer tube has a port defining member defining the outer shape of a combustion gas ejecting port that ejects combustion gas, and the port defining member protrudes from the inner circumference of the outer tube towards the center axis so as to block the outermost area including areas between the outer circumferences of a plurality of inner tubes forming the inner tube row and the inner circumference of the outer tube of the combustion gas flow path.
    Type: Application
    Filed: September 19, 2011
    Publication date: March 29, 2012
    Applicant: SHIN-ETSU CHEMICAL CO., LTD.
    Inventor: Makoto Yoshida
  • Publication number: 20120073333
    Abstract: The present invention provides an apparatus for fabricating porous glass preforms, in which any damages of a reaction vessel due to the increase in thermal load to the reaction vessel can be controlled without enlarging the reaction vessel. A wall of the reaction vessel includes a plurality of rectangular inner wall metal plates that defines at least apart of inner side walls of the reaction vessel, adjacent inner wall metal plates of a plurality of inner wall metal plates of which being weld bonded at their edges, and a plurality of metal frame members having higher stiffness than that of the inner wall metal plates and being arranged along each edge region of the opposite surface of the inner side walls of each of the plurality of inner wall metal plates and fixed to the edge region by a tightening or welding means.
    Type: Application
    Filed: September 19, 2011
    Publication date: March 29, 2012
    Applicant: SHIN-ETSU CHEMICAL CO., LTD.
    Inventor: Makoto Yoshida
  • Patent number: 8079233
    Abstract: The present invention provides a burner for manufacturing a porous glass base material that has small-diameter gas discharge ports and that achieves uniform linear velocity at the gas discharge ports, a uniform reaction, and a stable flame, and improved deposition efficiency.
    Type: Grant
    Filed: August 24, 2010
    Date of Patent: December 20, 2011
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventor: Makoto Yoshida
  • Publication number: 20110259055
    Abstract: A multi-nozzle type burner is used for producing a porous glass preform, the burner having small variations in deposition efficiency with the burner tip being not burned even when axial shift occurs at the concentric multi-tube part of the burner. The present invention provides a burner for producing a porous glass preform with a concentric multi-tube structure, comprising a glass material gas jet port in a center, a plurality of gas jet ports concentrically disposed outside the glass material gas jet port, and small-diameter gas jet ports which are disposed in a line or a plurality of lines concentrically to the glass material gas jet port so as to be enclosed in one of the gas jet ports other than the gas jet ports in the center and at an outermost side, the small-diameter gas jet ports in the same line having an identical focal length.
    Type: Application
    Filed: April 22, 2011
    Publication date: October 27, 2011
    Applicant: SHIN-ETSU CHEMICAL CO., LTD.
    Inventor: Makoto Yoshida
  • Publication number: 20110259056
    Abstract: The present invention provides a burner for manufacturing a porous glass preform, which is provided with a combustible gas injection port involving a plurality of small-diameter supporting gas injection ports such that the injection ports of the same row have the equal focal distance, the small-diameter supporting gas injection ports being arranged on the outside of a glass source gas injection port in the center so as to be in a row or in a plurality of rows and concentric with the glass source gas injection port, wherein the small-diameter supporting gas injection ports are bent toward the burner center axis at predetermined positions from the tip ends of the small-diameter supporting gas injection ports so that the focal points of the small-diameter supporting gas injection ports of the same row agree with each other, and the bend angle of the small-diameter supporting gas injection port row closest to the glass source gas injection port in the center of the small-diameter supporting gas injection port row
    Type: Application
    Filed: April 22, 2011
    Publication date: October 27, 2011
    Applicant: SHIN-ETSU CHEMICAL CO., LTD.
    Inventor: Makoto Yoshida
  • Patent number: 8001808
    Abstract: A burner for a vapor deposition process has a cylindrical central gas passage and a plurality of external gas passages surrounding the central gas passage. The burner has a back block defining an initial section of the gas passages, a face block defining a final section of the gas passages and a manifold plate positioned between the back block and the face block and defining an intermediate section of the external gas passages; the face block, the manifold plate and the back block have inner integral walls that define respective sections of the central gas passage.
    Type: Grant
    Filed: November 26, 2001
    Date of Patent: August 23, 2011
    Assignee: Prysmian Cavi E Sistemi Energia S.R.L.
    Inventors: Antonio Mileo, Andrea Demergazzi, Sergio Pellegrini
  • Patent number: 7823418
    Abstract: A glass base material manufacturing apparatus for manufacturing a glass base material comprising: a plurality burners, arranged in a row at a predetermined intervals along the longitudinal direction of a starting base material of the glass base material, for forming a deposit, which is a base material of the glass base material by depositing glass soot on the starting base material while moving reciprocatory over a section of the entire length of the starting base material along the longitudinal direction of the starting base material; a plurality of flow rate regulators, at least one of which is connected to the plurality of burners, respectively, for regulating a flow rate of raw material gas of the glass soot, which is supplied to the plurality of burners; and a control unit connected to each of the plurality of flow rate regulators for controlling individually the plurality of flow rate regulators.
    Type: Grant
    Filed: May 31, 2006
    Date of Patent: November 2, 2010
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Tadakatsu Shimada, Yuuji Tobisaka, Kazuhisa Hatayama, Hideo Hirasawa
  • Patent number: 7624596
    Abstract: A method for preparing doped oxide material, in which method substantially all the reactants forming the oxide material are brought to a vaporous reduced form in the gas phase and after this to react with each other in order to form oxide particles. The reactants in vaporous and reduced form are mixed together to a gas flow of reactants, which gas flow is further condensated fast in such a manner that substantially all the component parts of the reactants reach a supersaturated state substantially simultaneously by forming oxide particles in such a manner that there is no time to reach chemical phase balances.
    Type: Grant
    Filed: June 27, 2003
    Date of Patent: December 1, 2009
    Assignee: Liekki Oy
    Inventors: Kauko Janka, Markku Rajala
  • Patent number: 7587914
    Abstract: A method for feeding a flow of gas to a burner for manufacturing an optical fiber preform. The burner has a plurality of coaxial tubes, each two adjacent coaxial tubes defining an annular channel between themselves; an annular gas distribution chamber at one extremity of the annular channels and in fluid communication therewith, the annular distribution chamber being delimited in the radial direction by an inner and an outer surface. The flow of gas is introduced into the distribution chamber so that the direction of its radially outermost portion is tangential to the radially outer surface of the distribution chamber. The method allows obtaining a better gas velocity distribution in the annular channels.
    Type: Grant
    Filed: May 27, 2002
    Date of Patent: September 15, 2009
    Assignee: Prysmian Cavi E Sistemi Energia S.R.L.
    Inventors: Giacomo Stefano Roba, Franco Veronelli, Massimo Nutini
  • Publication number: 20090100876
    Abstract: A method of manufacturing an optical fiber base material includes: forming a porous glass base material by depositing glass particles; providing a synthetic quartz glass vessel at least partly made of quartz glass which contains aluminum equal to or less than 0.01 ppm; introducing dehydration reaction gas and inert gas into the vessel; heating a portion made of quartz glass which contains aluminum equal to or less than 0.01 ppm in the vessel that contains the dehydration reaction gas and the inert gas; and inserting the porous glass base material into the heated vessel to dehydrate and sinter the porous glass base material.
    Type: Application
    Filed: December 22, 2008
    Publication date: April 23, 2009
    Applicant: SHIN-ETSU CHEMICAL CO., LTD.
    Inventors: Dai Inoue, Hiroyuki Koide, Takaaki Nagao
  • Publication number: 20090038346
    Abstract: A deposition system for depositing a chemical vapor onto a workpiece, including a deposition chamber having a plurality of components for performing chemical vapor deposition on the workpiece. The deposition chamber includes an inner skin made of Hasteloy for sealing the plurality of components and the workpiece from the air surrounding the deposition system, and an outer skin that encloses the inner skin and is separated from the inner skin by an air gap. The outer skin includes vents that create a convection current in the air gap between the inner skin and outer skin of the deposition chamber. The deposition system also has a gas panel for regulating the flow of gases and vapors into the deposition chamber, and a computer for controlling operation of the gas panel and the components in the deposition chamber.
    Type: Application
    Filed: October 9, 2008
    Publication date: February 12, 2009
    Applicant: ASI/SILICA MACHINERY, LLC
    Inventors: Franklin W. Dabby, Bedros Orchanian
  • Patent number: 7481077
    Abstract: A device including at least one gripping member, rotatably mounted about an axis Z-Z, adapted to hold at least one end of at least one elongated element for chemical vapour deposition for forming a preform. The device includes at least one burner being mobile along a direction substantially parallel to the axis Z-Z and adapted to deposit, on the elongated element, a chemical substance for forming a preform, and at least one suction element arranged on the opposite side of the burner on a portion of a wall of the device on the opposite side of the gripping member from the burner. At least one air suction member, mobile along direction Z, is provided with motion synchronous with respect to the burner. The wall with the air suction member has a pair of respective upper and lower tapes rigidly associated with the burner.
    Type: Grant
    Filed: June 12, 2002
    Date of Patent: January 27, 2009
    Assignee: Prysmian Cavi e Sistemi Energia S.r.l.
    Inventors: Giacomo Stefano Roba, Franco Veronelli
  • Patent number: 7441416
    Abstract: Multi-flame burner wherein each flame is separated with respect to the neighboring flame by at least one separating tube made of a heat resistant material, for example, quartz glass or ceramic material. The burner also has a plurality of co-axial pipes, preferably made of a metallic material. The cross section of the upper end of the separating tube can be modified in order to increase the deposition rate of the burner. Methods for manufacturing optical fibre preforms by vapour deposition using the multi-flame deposition burners.
    Type: Grant
    Filed: November 30, 2001
    Date of Patent: October 28, 2008
    Assignee: Prysmian Cavi E Sistemi Energia S.R.L.
    Inventors: Giacomo Stefano Roba, Massimo Nutini
  • Patent number: 7437893
    Abstract: This invention provides a method for manufacturing an optical glass in order to prevent the deterioration of the burner used in the synthesis of glass particles that form the optical glass, and to obtain a stable quality optical glass. In this invention, the number of residual bubbles with a diameter of 0.3 mm and more is 0.005/cm3 or less per unit volume of the optical glass. Such optical glass is obtained by controlling the temperature of an end face of the burner for glass synthesis during the deposition of the glass particles by regulating the relationship of the flow velocity or the flow volume between an inflammable gas and a combustion-supporting gas.
    Type: Grant
    Filed: February 18, 2003
    Date of Patent: October 21, 2008
    Assignee: Fujikura Ltd.
    Inventors: Kumi Onodera, Manabu Saitou, Masahiro Horikoshi
  • Patent number: 7415844
    Abstract: A device for manufacturing a preform of glass material for optical fibres. A chemical deposition chamber, at least one burner mobile along a direction Z and adapted to deposit a chemical substance on at least an elongated element positioned along an axis Z-Z, at least one suction element mobile along the direction Z for collecting exhaust chemical substances, a collector tube associated with the at least one suction element and adapted to discharge the exhaust chemical substances outside the chemical deposition chamber through an exhaust opening formed on a wall of the chamber, and a coupling device between the collector tube and the wall at the exhaust opening, allowing sliding of the collector along the direction Z and along a direction X towards/away from the axis z-z.
    Type: Grant
    Filed: June 18, 2002
    Date of Patent: August 26, 2008
    Assignee: Prysmian Cavi e Sistemi Energia S.R.L.
    Inventors: Giacomo Stefano Roba, Franco Veronelli
  • Patent number: 7383704
    Abstract: An outside chemical vapor deposition apparatus is disclosed for depositing porous glass-forming material onto a target rod to form a cylindrical body, with substantially higher efficiency than could prior apparatus. The apparatus includes two separate burner arrays, one array optimized for depositing the material during an initial stage of the process, when the cylindrical body has a relatively small diameter, and the other array optimized for depositing the material during a later stage of the process, when the cylindrical body has a relatively large diameter. In addition, each burner array can include a plurality of burners, with each burner azimuthally angled relative to the apparatus' air-flow axis, and with adjacent burners angled in opposite directions relative to that axis, to minimize the density gradient within the deposited porous material.
    Type: Grant
    Filed: February 1, 2005
    Date of Patent: June 10, 2008
    Assignee: Nextrom Oy
    Inventors: Arnab Sarkar, Bedros Orchanian
  • Patent number: 7310975
    Abstract: A known method for producing a cylindrical body uses a precipitation assembly (5) consisting of several precipitators (4), to which a parent substance is fed via medium supply lines (9), whereby the precipitation assembly (5) completes a closed trajectory (6) according to a predetermined displacement course, said trajectory comprising at least one precipitation path (8) that runs along the longitudinal axis (2) of the support. The aim of the invention is to provide an economical, reproducible, failsafe method based on said known procedure, which enables in particular the production of soot layers (3) on a support (1) at a high precipitation rate and nevertheless a high degree of uniformity. To achieve this, the displacement course (6) comprises a first loop (7a, 8) and a second loop (7b, 8), whereby the completion of the first loop (7a, 8) causes a right-hand torsion in the medium supply lines (9) and the completion of the second loop (7b, 8) causes a left-hand torsion in said lines (9).
    Type: Grant
    Filed: October 27, 2003
    Date of Patent: December 25, 2007
    Assignee: Heraeus Tenevo GmbH
    Inventor: Michael Hünermann
  • Patent number: 7299659
    Abstract: Method and burner for increasing the deposition rate of porous glass deposit in the manufacture of optical preforms, by modifying the cross-sectional shape of the flow of glass particles impacting onto a target preform. In particular, the cross-section of the flow of glass particles is modified by increasing the dimension of the flow from a circular cross-section to one having a major and minor axis in a direction substantially perpendicular to the longitudinal axis of the target preform.
    Type: Grant
    Filed: November 30, 2001
    Date of Patent: November 27, 2007
    Assignee: Prysmian Cavi e Sistemi Energia S.r.l.
    Inventors: Giacomo Stefano Roba, Massimo Nutini
  • Publication number: 20070151298
    Abstract: Vapor Axial Deposition (VAD) apparatus and method is provided. The VAD apparatus includes a first torch, a second torch, a thermometer, a controller, and a moving device. The first torch grows a core by depositing a soot at an end of a soot preform arranged on an axis. The second torch grows a clad by depositing a soot on the face of the core. The thermometer detects the temperature of the end of the soot preform along the axis and the temperature of an other/lower portion of the core. The controller calculates a difference between a temperature (T1) of the end of the soot preform and a temperature (T4) of a lower portion of the core and controls the movement of the soot preform according to the difference. The moving device moves the soot preform along the axis according to the instruction of the controller.
    Type: Application
    Filed: July 20, 2006
    Publication date: July 5, 2007
    Inventors: Jin-Haing Kim, Ho-Jin Lee, Mun-Hyun Do, Jae-Hyeon Seong, Yun-Ho Kim
  • Patent number: 7213416
    Abstract: A glass base material manufacturing apparatus for manufacturing a glass base material comprising: a plurality burners, arranged in a row at a predetermined intervals along the longitudinal direction of a starting base material of the glass base material, for forming a deposit, which is a base material of the glass base material by depositing glass soot on the starting base material while moving reciprocatory over a section of the entire length of the starting base material along the longitudinal direction of the starting base material; a plurality of flow rate regulators, at least one of which is connected to the plurality of burners, respectively, for regulating a flow rate of raw material gas of the glass soot, which is supplied to the plurality of burners; and a control unit connected to each of the plurality of flow rate regulators for controlling individually the plurality of flow rate regulators.
    Type: Grant
    Filed: July 18, 2001
    Date of Patent: May 8, 2007
    Assignee: Shin-Etsu Chemical Co., LTD.
    Inventors: Tadakatsu Shimada, Yuuji Tobisaka, Kazuhisa Hatayama, Hideo Hirasawa
  • Patent number: 7165425
    Abstract: A multi-tube burner is provided which includes a cylindrical outermost nozzle and at least one cylindrical inner nozzle provided coaxially with the outermost nozzle to form annular jet openings for gases used to manufacture a glass preform. The angle between a center axis of an outer circumference of the outermost nozzle and a distal end portion of each of the inner nozzles is 90°± not more than 3°. Furthermore, the distance between the center axis of the outer circumference of the outermost nozzle and each of center axes of inner circumferences and outer circumferences of the inner nozzles is not more than 0.20 mm.
    Type: Grant
    Filed: July 2, 2003
    Date of Patent: January 23, 2007
    Assignee: Fujikura Ltd.
    Inventors: Keisuke Uchiyama, Masahiro Horikoshi, Koichi Harada
  • Patent number: 7143608
    Abstract: A concentric multi-tubular burner for synthesizing glass particles having a center port group constituted by a combination of jet ports of raw material gas, combustible gas and oxygen gas, wherein an outer wall of the oxygen gas jet port in the center port group protrudes more toward a burner head than an inner wall of the oxygen gas jet port. The flow rate of oxygen gas jetted from the oxygen gas jet port of the center port group is controlled to be in a proper range.
    Type: Grant
    Filed: March 4, 2004
    Date of Patent: December 5, 2006
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Tadashi Enomoto, Yuichi Ohga, Nobuya Akaike, Haruhiko Aikawa, Takashi Matsuo, Motonori Nakamura
  • Patent number: 7082791
    Abstract: An apparatus for fabricating a soot preform for an optical fiber. The soot preform is fabricated by depositing glass particles on a starting rod capable of being rotated and pulled up. The apparatus comprises elements as follows. A reaction chamber is used for depositing the glass particles on the starting rod. An upper room is located above the reaction chamber for receiving the soot preform formed in the upper portion of the reaction chamber. At least one core burner is installed in the reaction chamber. A gas-supplying inlet is located in the top part of the sidewall of the reaction chamber closest to burner(s), and a gas-exhausting outlet is located in the top part of another sidewall opposite to the gas-supplying inlet. In addition, at least one cladding burner is installed in the reaction chamber.
    Type: Grant
    Filed: October 31, 2003
    Date of Patent: August 1, 2006
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Dai Inoue, Go Ogino, Tetsuya Otosaka, Tadakatsu Shimada, Hideo Hirasawa
  • Patent number: 6941773
    Abstract: An apparatus for manufacturing an optical fiber soot, which comprises a core partition having an opening portion at core burner side provided on a periphery of a core burner, in a reactor of the apparatus to be used in a conventional VAD method.
    Type: Grant
    Filed: September 28, 2001
    Date of Patent: September 13, 2005
    Assignee: The Furukawa Electric Co., Ltd.
    Inventors: Hiroyuki Wada, Kiyoshi Arima, Masahide Kuwabara, Sadayuki Toda
  • Patent number: 6920766
    Abstract: A synthetic quartz glass preform is produced by flame hydrolysis with subsequent cooling and is suitable for the application of high-energy DUV radiation in the wave length range under 250 nm. The preform has a core area which contains ?1150 ppm OH, a strain double refraction of ?5 nm/cm and a resistance to high-energy DUV radiation as a result of a transmission reduction of ?T ?0.1%/cm thickness. The quartz glass has been exposed to the following radiation: wavelength ?1=248 nm, laser shot frequency ?300 Hz, laser shot value ?109 and lumination ?10 mJ/cm2, and wavelength ?2=193 nm, laser shot frequency ?300 Hz, laser shot value ?109 and lumination <5 mJ/cm2. Apparatus for producing the preform comprises a horizontally positioned muffle with two different sized openings facing each other. The larger of the openings is for removing the preform, the smaller opening being for introducing a burner. The internal chamber of the muffle narrows from the larger opening to the smaller opening.
    Type: Grant
    Filed: May 30, 2002
    Date of Patent: July 26, 2005
    Assignee: Schott ML GmbH
    Inventors: Frank Coriand, Andreas Menzel, Andreas Voitsch
  • Patent number: 6910352
    Abstract: The invention includes methods of making a fluorine doped soot particle. One method of the invention includes the steps of (1) delivering a silicon containing precursor to a first opening in a burner face; (2) delivering a source of oxygen to a second opening, wherein the second opening is spaced apart from the first opening such that the silicon precursor and oxygen source react to form a soot particle having a surface area of more than about 20 m2/g; and (3) delivering a fluorine precursor to a third opening, said third opening is spaced apart from the first opening. A second method of the invention includes the steps of (A) delivering a silicon containing precursor to a first opening in a burner face; (B) delivering a fluorine precursor to a second opening, wherein said second opening is spaced apart from said first opening; and (C) delivering a fuel to a third opening, said third opening is spaced apart from said first opening.
    Type: Grant
    Filed: April 24, 2002
    Date of Patent: June 28, 2005
    Assignee: Corning Incorporated
    Inventor: William W Johnson
  • Patent number: 6837076
    Abstract: A burner and a method for producing an inorganic soot such as silica comprising a plurality of substantially planar layers having multiple openings therethrough formed by a micromachining process. The openings are in fluid communication with a precursor inlet and a gas inlet to permit the gas and the precursor to flow through and exit the burner. The burner produces a flame from a combustible gas in which the precursor undergoes a chemical reaction to form the soot.
    Type: Grant
    Filed: February 10, 2003
    Date of Patent: January 4, 2005
    Assignee: Corning Incorporated
    Inventor: Daniel W. Hawtof