Producing Solid Particulate Free Metal Directly From Liquid Metal (e.g., Liquid Comminuting, Etc.) Patents (Class 75/331)
  • Patent number: 7988759
    Abstract: A method of producing metal powder using a nozzle including a flow path and an orifice includes: storing molten metal in a supply part; passing the molten metal through a tubular member below the supply part and injecting the molten metal from a bottom end of the tubular member into the flow path; subjecting the molten metal to primary breakup via depressurization inside the flow path to yield liquid droplets; and subjecting the liquid droplets to secondary breakup via contact with fluid injected from the orifice to yield further fine shapes, and solidifying them by cooling to obtain the metal powder, wherein the orifice opens toward a bottom end of the flow path, and the depressurization inside the flow path is generated by a stream of the fluid injected from the orifice into the flow path.
    Type: Grant
    Filed: October 29, 2010
    Date of Patent: August 2, 2011
    Assignee: Seiko Epson Corporation
    Inventor: Tokihiro Shimura
  • Patent number: 7931834
    Abstract: A process for the formation of particles of a target material is disclosed, comprising: (i) introducing the target material into a particle formation vessel, and forming a continuous liquid surface of the target material in the particle formation vessel, and an interface between said liquid surface of the target material and additional gaseous contents of said particle formation vessel; (ii) introducing a stream of cryogenic material including solid particles of cryogenic material into the particle formation vessel and into contact with the target material in a liquid state below the continuous liquid surface; (iii) allowing rapid volumetric expansion of the cryogenic material into a gaseous state while in contact with the target material in a liquid state, and release of the expanded gaseous cryogenic material through the continuous liquid surface, and forming liquid droplet particles of the target material; and (iv) collecting the formed particles of the target material.
    Type: Grant
    Filed: February 13, 2007
    Date of Patent: April 26, 2011
    Assignee: Eastman Kodak Company
    Inventors: Rajesh V. Mehta, Robert Link, Michael A. Marcus
  • Patent number: 7922786
    Abstract: With this invention, in a nanoparticle production method, wherein nanoparticles are produced by irradiating a laser light irradiation portion 2a of a to-be-treated liquid 8 with a laser light, in which suspended particles are suspended, to pulverize the suspended particles in laser light irradiation portion 2a, laser light irradiation portion 2a of to-be-treated liquid 8 is cooled. In this case, by the cooling of to-be-treated liquid 8, the respective suspended particles are cooled in their entireties. When the portion 2a of this to-be-treated liquid 8 is irradiated with the laser light, the laser light is absorbed at the surfaces of the suspended particles at portion 2a. Since to-be-treated liquid 8 is cooled during this process, significant temperature differences arise between the interiors and surfaces of the suspended particles and between the surfaces of the suspended particles and the to-be-treated liquid at laser light irradiation portion 2a, and highly efficient nanoparticulation is realized.
    Type: Grant
    Filed: June 26, 2008
    Date of Patent: April 12, 2011
    Assignee: Hamamatsu Photonics K.K.
    Inventors: Tomonori Kawakami, Bo Li, Mitsuo Hiramatsu
  • Patent number: 7909907
    Abstract: A system and method for high volume production of nanoparticles, nanotubes, and items incorporating nanoparticles and nanotubes. Microwave, radio frequency, or infrared energy vaporizes a metal catalyst which, as it condenses, is contacted by carbon or other elements such as silicon, germanium, or boron to form agglomerates. The agglomerates may be annealed to accelerate the production of nanotubes. Magnetic or electric fields may be used to align the nanotubes during their production. The nanotubes may be separated from the production byproducts in aligned or non-aligned configurations. The agglomerates may be formed directly into tools, optionally in compositions that incorporate other materials such as abrasives, binders, carbon-carbon composites, and cermets.
    Type: Grant
    Filed: September 2, 2009
    Date of Patent: March 22, 2011
    Assignee: Babcock & Wilcox Technical Services Y-12, LLC
    Inventors: Edward B. Ripley, Jonathan S. Morrell, Roland D. Seals, Gerald M. Ludtka
  • Patent number: 7892599
    Abstract: Methods for functionalizing the surface of nanomaterials to improve processing and product manufacturing. These methods are useful for oxides, nitrides, carbides, borides, metals, alloys, chalcogenides, and other compositions.
    Type: Grant
    Filed: July 27, 2004
    Date of Patent: February 22, 2011
    Assignee: PPG Industries Ohio, Inc.
    Inventors: Tapesh Yadav, Karl Pfaffenbach
  • Publication number: 20100307914
    Abstract: A Cu—Ga alloy includes a plurality of phases, and not less than 40 wt % and not more than 60 wt % of gallium (Ga) and a balance consisting of copper and an inevitable impurity. The plurality of phases include a segregation phase including not less than 80 wt % of gallium (Ga), and a rate of a volume of the segregation phase to a total volume of the Cu—Ga alloy is not more than 1%. The plurality of phases include particles including not less than 40 wt % and not more than 60 wt % of gallium (Ga), the particles include a diameter of not less than 0.1 ?m and not more than 30 ?m, and a rate of a volume of the particles to the total volume of the Cu—Ga alloy is not less than 90%.
    Type: Application
    Filed: May 11, 2010
    Publication date: December 9, 2010
    Inventors: Yuichi HIRAMOTO, Tatsuya Tonogi
  • Patent number: 7827822
    Abstract: The invention relates to a process and apparatus for forming a particulate composition, especially a particle glass composition, through the use of shock waves. A nozzle element is utilized having inlets for introduction of cold and heated gas and a delivery tube for introducing molten material. Through the introduction of the cold and heated gases, droplets are formed from a molten stream, a cone-shaped standing shock wave is formed, and shock waves are formed via a modified Hartmann-Sprenger chamber, the shock waves impinging on the droplet stream to break up the larger droplets.
    Type: Grant
    Filed: July 25, 2007
    Date of Patent: November 9, 2010
    Assignee: Schott Corporation
    Inventors: Carsten Weinhold, David John Yuhas
  • Publication number: 20100242727
    Abstract: A new lithium material with high surface area, a method of its production, and a process of using the given material in purification of hydrogen or inert gases stream from active impurities. The material is manufactured in a form of granules of 0.2-2.5 mm in diameter with the structure of a dendritic carcass and is characterized with high sorption capacity and resistance to chemical shocks.
    Type: Application
    Filed: April 22, 2010
    Publication date: September 30, 2010
    Applicant: ADVANCED GETTER INNOVATIONS LTD.
    Inventor: Konstantin CHUNTONOV
  • Publication number: 20100243313
    Abstract: The present invention provides a magnetic composite capable of enhancing the effect of shielding against electromagnetic noise and the like (magnetic shielding effect) while inhibiting a possible eddy current, and a method for producing the magnetic composite, and a shielding structure comprising the magnetic composite. A shielding member 10 as a magnetic composite contains a resin 12 which is an insulator and serves as a matrix material and into which fine powders of an amorphous metal magnetic substance 10a containing Fe, Si, and B are mixed. In the shielding member 10, a plurality of the amorphous metal magnetic substances 10a are contained in the resin 12 at a volume fraction less than a percolation threshold. The type of the amorphous metal magnetic substance 10a is not particularly limited provided that the amorphous metal contains Fe, Si, and B.
    Type: Application
    Filed: December 18, 2009
    Publication date: September 30, 2010
    Inventors: Tomoaki Ueda, Masanori Abe
  • Patent number: 7780757
    Abstract: The present invention provides a method and apparatus for producing fine particles. According to the production method, a molten material 1 which has been formed by melting a raw material to be formed into fine particles is supplied in the form of droplets 1a or a jet flow to a liquid coolant 3, and a vapor film formed so as to cover the molten material supplied to the liquid coolant 3 is forcedly broken to promote vapor explosion, thereby forming and cooling fine particles for solidification. The production method and apparatus can readily produce fine particles from a raw material having a high melting point, and can relatively readily produce submicron fine particles—such particles are difficult to produce by mean of the previously developed technique. The method and apparatus can produce amorphous fine particles, or polycrystalline fine particles having a target particle size by regulating conditions for fine particle formation and for cooling-solidification.
    Type: Grant
    Filed: March 1, 2004
    Date of Patent: August 24, 2010
    Assignee: Central Research Institute of Electric Power Industry
    Inventor: Masahiro Furuya
  • Patent number: 7766992
    Abstract: A metallic article is produced by furnishing one or more nonmetallic precursor compound comprising the metallic constituent element(s), and chemically reducing the nonmetallic precursor compound(s) to produce an initial metallic particle, preferably having a size of no greater than about 0.070 inch, without melting the initial metallic particle. The initial metallic particle is thereafter melted and solidified to produce the metallic article. By this approach, the incidence of chemical defects in the metal article is minimized. The melted-and-solidified metal may be used in the as-cast form, or it may be converted to billet and further worked to the final form.
    Type: Grant
    Filed: February 16, 2005
    Date of Patent: August 3, 2010
    Assignee: General Electric Company
    Inventors: Andrew Philip Woodfield, Clifford Earl Shamblen, Eric Allen Ott
  • Patent number: 7754644
    Abstract: The present invention provides a noble metal particle with an improved methanol-oxidation property. This noble metal particle has a platinum particle and ruthenium particles deposited on only part of the surface of the platinum particle. This noble metal particle suitably can be produced by precipitating the ruthenium particles out of the solution so that the ruthenium particles are deposited on only part of the surface of the platinum particle by further adding a ruthenium salt into the solution and reducing the ruthenium salt after the reduction of the platinum salt in the solution essentially is completed. This noble metal particle is suitable as a catalyst to be supported on an electrode of a polymer electrolyte fuel cell typified by a direct methanol fuel cell.
    Type: Grant
    Filed: September 1, 2006
    Date of Patent: July 13, 2010
    Assignee: Nippon Sheet Glass Company, Limited
    Inventor: Ryohei Ogawa
  • Publication number: 20100139815
    Abstract: A method for producing high strength aluminum alloy containing L12 intermetallic dispersoids by using gas atomization to produce powder that is then consolidated into L12 aluminum alloy billets or by casting the alloy into molds to produce L12 aluminum alloy billets or by casting the alloy into directly useable parts.
    Type: Application
    Filed: December 9, 2008
    Publication date: June 10, 2010
    Applicant: United Technologies Corporation
    Inventor: Awadh B. Pandey
  • Patent number: 7730746
    Abstract: Apparatus to eject on demand discrete hollow microsphere droplets that are characterized by a highly regular and predictable spherical shape, devoid of tails or other irregularities common in the prior art with a selected pure gas contained in the center. With this method and apparatus, droplets may be formed of any suitable material including glass, ceramic, plastic, or metal. A variety of gases at various pressures including complete vacuums may be contained in the hollow microsphere. Microspheres filled with ionizable gas may be used as pixels in a plasma display panel. Microspheres used as a pixel elements may be referred to as Plasma-spheres. The inside of each Plasma-sphere may contain a luminescent material such as a phosphor and/or a secondary electron emission material such as magnesium oxide or a rare earth oxide introduced during the gas filling of the microsphere.
    Type: Grant
    Filed: July 10, 2006
    Date of Patent: June 8, 2010
    Assignee: Imaging Systems Technology
    Inventors: Thomas J. Pavliscak, Carol Ann Wedding
  • Publication number: 20100111747
    Abstract: The present disclosure relates to a glass forming alloy. The glass forming alloy may include 43.0 atomic percent to 68.0 atomic percent iron, 10.0 atomic percent to 19.0 atomic percent boron, 13.0 atomic percent to 17.0 atomic percent nickel, 2.5 atomic percent to 21.0 atomic percent cobalt, optionally 0.1 atomic percent to 6.0 atomic percent carbon, and optionally 0.3 atomic percent to 3.5 atomic percent silicon. Furthermore, the glass forming alloy includes between 5% to 95% by volume one or more spinodal glass matrix microconstituents which include one or more semi-crystalline or crystalline phases at a length scale less than 50 nm in a glass matrix. In addition, the glass forming alloy is capable of blunting shear bands through localized deformation induced changes under tension.
    Type: Application
    Filed: November 4, 2009
    Publication date: May 6, 2010
    Applicant: The NanoSteel Company, Inc.
    Inventors: Daniel James BRANAGAN, Brian E. MEACHAM, Jikou ZHOU, Alla V. SERGUEEVA
  • Patent number: 7628840
    Abstract: Each of the metal nano-particles present in a dispersion, which comprises at least one metal selected from the group consisting of precious metals and transition metals or an alloy of at least two metals selected from the foregoing metals, comprises a metal particle in which an organic metal compound of a fatty acid and/or an amine-metal complex is adhered to the periphery of the metal particle. This organic metal compound and the amine-metal complex are admixed together in a solvent and then the resulting mixture is subjected to a reducing treatment to thus form a dispersion containing metal nano-particles in a concentration of not less than 5% by mass and not more than 90% by mass. The resulting dispersion is applied onto the surface of a base material, followed by drying the applied layer of the dispersion and then firing the dried layer of the dispersion at a low temperature to thus form a thin metallic wire or a metal film having conductivity.
    Type: Grant
    Filed: September 7, 2004
    Date of Patent: December 8, 2009
    Assignees: ULVAC, Inc., JEMCO, Inc.
    Inventors: Tsutomu Atsuki, Masaaki Oda, Toshiharu Hayashi, Reiko Kiyoshima
  • Publication number: 20090272228
    Abstract: One non-limiting embodiment of an apparatus for forming an alloy powder or preform includes a melting assembly, an atomizing assembly, and a field generating assembly, and a collector. The melting assembly produces at least one of a stream of a molten alloy and a series of droplets of a molten alloy, and may be substantially free from ceramic in regions contacted by the molten alloy. The atomizing assembly generates electrons and impinges the electrons on molten alloy from the melting assembly, thereby producing molten alloy particles. The field generating assembly produces at least one of an electrostatic field and an electromagnetic field between the atomizing assembly and the collector. The molten alloy particles interact with the at least one field, which influences at least one of the acceleration, speed, and direction of the molten alloy particles. Related methods also are disclosed.
    Type: Application
    Filed: July 14, 2009
    Publication date: November 5, 2009
    Applicant: ATI Properties, Inc.
    Inventors: Robin M. Forbes Jones, Richard L. Kennedy
  • Publication number: 20090252636
    Abstract: A powder metal steel alloy composition for high wear and temperature applications is made by water atomizing a molten steel alloy composition containing C in an amount of at least 3.0 wt %; at least one carbide-forming alloy element selected from the group consisting of: Cr, V, Mo or W; an O content less than about 0.5 wt %, and the balance comprising essentially Fe apart from incidental impurities. The high carbon content reduces the solubility of oxygen in the melt and thus lowers the oxygen content to a level below which would cause the carbide-forming element(s) to oxidixe during water atomization. The alloy elements are thus not tied up as oxides and are available to rapidly and readily form carbides in a subsequent sintering stage. The carbon, present in excess, is also available for diffusing into one or more other admixed powders that may be added to the prealloyed powder during sintering to control microstructure and properties of the final part.
    Type: Application
    Filed: April 7, 2009
    Publication date: October 8, 2009
    Inventors: Denis B. Christopherson, JR., Leslie John Farthing, Todd Schoenwetter, Gilles L'Esperance, Phillipe Beaulieu
  • Publication number: 20090252639
    Abstract: An annealed prealloyed water atomised iron-based powder is provided which is suitable for the production of pressed and sintered components having high wear resistance. The iron-based powder comprises 15-30% by weight of Cr, 0.5-5% by weight of each of at least one of Mo, W and V, and 0.5-2%, preferably 0.7-2% and most preferably 1-2% by weight of C. The powder has a matrix comprising less than 10% by weight of Cr, and comprises large chromium carbides. A method for production of the iron-based powder also is provided.
    Type: Application
    Filed: September 20, 2007
    Publication date: October 8, 2009
    Applicant: HÖGANÄS AB (PUBL)
    Inventors: Ola Bergman, Paul Dudfield Nurthen
  • Patent number: 7588622
    Abstract: A method of forming metal spheres includes ejecting a precisely measured droplet of molten metal from a molten metal mass, buffering the molten metal droplet to reduce the internal kinetic energy of the droplet without solidifying the droplet and cooling the buffered droplet until the droplet solidifies in the form of a metal sphere. An apparatus for fabricating metal spheres includes a droplet generator that generates a droplet from a molten metal mass, a buffering chamber that receives the droplet from the droplet generator, and diminishes internal kinetic energy of the droplet without solidifying the droplet, and a cooling drum that receives the droplet from the buffering chamber, and cools the droplet to the extent that the droplet solidifies into a metal sphere. The apparatus may further include a collector arrangement that receives the metal spheres from the cooling drum and makes the metal sphere available for collection.
    Type: Grant
    Filed: March 10, 2008
    Date of Patent: September 15, 2009
    Assignee: Henkel of America, Inc.
    Inventor: Hubert Chow
  • Publication number: 20090158890
    Abstract: A process is described for making metal nanoparticles comprising (a) forming a liquid melt of a first metal having the composition of the desired nanoparticles and a second metal; (b) quenching the melt to form a solid; and (c) removing the second metal from the solid and forming the nanoparticles comprising the first metal.
    Type: Application
    Filed: December 21, 2007
    Publication date: June 25, 2009
    Inventors: Arkady Garbar, Dmitry Lekhtman, Thomas Zak, Fernando de la Vega
  • Publication number: 20090107293
    Abstract: The present invention relates to a method and an apparatus for forming flakes, especially metal flakes. The method comprises producing a heated stream of molten material, feeding the stream in a substantially vertically downward direction, receiving the downwardly directed stream and forming flakes therefrom, and effecting a change in the temperature of the stream subsequent to the production thereof whereby flakes of a desired thickness are obtained. The present invention is applicable to any metal which melts when heated and is capable of being formed into flakes. Examples of metals are Al, Cu, Mo, V, Ag, Cr, Zr, Nb, Ni, Fe, Co, Ti, Au, Pd, W, Hf, Rh, Ir, Pt, Cd or alloys thereof, such as chromium-nickel, iron-nickel, iron-chromium and nickel-cobalt, wherein Cu, Ag, Ti, or Al, or alloys thereof are preferred and Al, or Ag, or alloys thereof are most preferred.
    Type: Application
    Filed: October 9, 2006
    Publication date: April 30, 2009
    Inventors: Patrice Bujard, Peter Simmendinger
  • Publication number: 20090098411
    Abstract: A method of manufacturing ferrite powder, by which a precursor obtained by an in-solution reaction method is heated at a temperature increase rate of 20° C./min or higher until arriving at a final temperature between 750 and 1200° C., the holding time at the final temperature being from 0 to 60 sec, and cooling from the final temperature to 300° C. being performed at a rate of 50° C./min or higher, to produce ferrite powder.
    Type: Application
    Filed: September 25, 2008
    Publication date: April 16, 2009
    Applicant: TDK CORPORATION
    Inventor: Yoshiaki Nakagawa
  • Publication number: 20090072938
    Abstract: The present invention provides an R-T-B system alloy used as a raw material for a rare earth permanent magnet (wherein R represents at least one selected from the group consisting of Sc, Y, La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Ho, Er, Tm, Yb and Lu, T represents a transition metal comprising 80% or more by weight of Fe, and B represents a component comprising 50% or more by weight of B and between 0 to less than 50% by weight of at least one selected from the group consisting of C and N), wherein the content of Mn in the alloy is 0.05% or less by weight.
    Type: Application
    Filed: February 21, 2008
    Publication date: March 19, 2009
    Applicant: SHOWA DENKO K.K.
    Inventors: Kenichiro Nakajima, Hiroshi Hasegawa
  • Patent number: 7501095
    Abstract: The invention provides an on-line sampling apparatus for the metal nanoparticle fluid of the vacuum submerged arc process and the method thereof, using the principle of the pressure difference between the vacuum pump and the vacuum chamber and the constant temperature design of the sample pipeline to make the sample precisely be caught and flow into the predetermined collector, and the disadvantage of the vaporization of the sample due to the temperature rise caused by the ambient temperature can be prevented. Further, the invention integrates with a particle size analysis apparatus to carry out real time measurement and data analysis of the nanoparticle fluid with real time process characteristics, wherein the nanoparticle fluid is caught from the nanofluid process line, thus, the optimal design work of the process and the system parameters and particle quality monitoring may be proceeded efficiently.
    Type: Grant
    Filed: February 5, 2004
    Date of Patent: March 10, 2009
    Assignee: National Taipei University of Technology
    Inventors: Liang-Chia Chen, Tshih Tsung, Jen-Yan Sun, Hong-Ming Lin
  • Publication number: 20090035170
    Abstract: An object of the present invention is to provide an R-T-B type alloy (wherein R is at least one element selected from Sc, Y, La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Ho, Er, Tm, Yb, and Lu; T is a transition metal that contains 80% by mass or more of Fe; and B is one that contains 50% by mass or more of boron (B) and also contains at least one element of C and N within a range from 0 to less than 50% by mass) that contains at least Dy, as a raw material for a rare earth-based permanent magnet having excellent magnetic characteristics, and the R-T-B type alloy provided in the present invention includes a main phase such as an R2T14B phase for exhibiting magnetic properties; an R-rich phase that is relatively enriched with R compared to the overall alloy compositional ratio; and a Dy-rich region that is formed close to the R-rich phase and relatively enriched with Dy compared to the compositional ratio.
    Type: Application
    Filed: January 28, 2008
    Publication date: February 5, 2009
    Applicant: Showa Denko K.K.
    Inventors: Kenichiro Nakajima, Hiroshi Hasegawa
  • Publication number: 20080141826
    Abstract: Novel carbon-plus-nitrogen corrosion-resistant ferrous and austenitic alloys, apparatus incorporating an inventive alloy, and methods of making and using the apparatus are described. The corrosion-resistant ferrous and austenitic alloys comprise no greater than about 4 wt. % nickel, are characterized by a strength greater than about 700 MPa (100 ksi), and, when being essentially free of molybdenum (<0.3 wt. %), have minimum Pitting Resistance Equivalence (PRE) numbers of 20 and minimum Measure of Alloying for Corrosion Resistance numbers (MARC) of 30 because of the use of both carbon and nitrogen. The ferrous and austenitic alloys are particularly formulated for use in oilfield operations, especially sour oil and gas wells and reservoirs. This abstract allows a searcher or other reader to quickly ascertain the subject matter of the disclosure. It will not be used to interpret or limit the scope or meaning of the claims.
    Type: Application
    Filed: December 18, 2006
    Publication date: June 19, 2008
    Applicant: SCHLUMBERGER TECHNOLOGY CORPORATION
    Inventors: Manuel Marya, Rashmi Bhavsar
  • Publication number: 20080141827
    Abstract: A method of rapidly cooling molten mixtures of alkali metal alloys in which the metal components of said alloys have a wide divergence of melting points that result in separation of the alaki metals during cool down. A calcium-sodium alloy is produced in an electrolysis cell. A method of high pressure atomization of the calcium-sodium alloy and its subsequent rapid cooling produces a calcium nodular particulate that is encased in a sodium flocculant. The material manufactured is used as a nodular electrolytic flocculant reactant in the electrolyte of an alkaline battery.
    Type: Application
    Filed: December 13, 2006
    Publication date: June 19, 2008
    Inventor: Edward Milton McWhorter
  • Patent number: 7384448
    Abstract: Apparatus for producing silver nano-particle material comprises a furnace and a crucible positioned within the furnace, the crucible containing a quantity of precursor material, the furnace heating the quantity of precursor material contained in the crucible to vaporize the precursor material. A process gas supply operatively associated with the furnace provides a process gas to an interior region of the furnace. A conduit is operatively associated with the furnace so that an inlet end of the conduit is open to the interior region of the furnace. A particle separator system is operatively associated with an outlet end of the conduit.
    Type: Grant
    Filed: February 16, 2004
    Date of Patent: June 10, 2008
    Assignee: Climax Engineered Materials, LLC
    Inventor: Loyal M. Johnson, Jr.
  • Publication number: 20080078476
    Abstract: An alloy is used for production of magnetic refrigeration material particles. The alloy contains La in a range of 4 to 15 atomic %, Fe in a range of 60 to 93 atomic %, Si in a range of 3.5 to 23.5 atomic % and at lease one element M selected from B and Ti in a range of 0.5 to 1.5 atomic %. The alloy includes a main phase containing Fe as a main component element and Si, and a subphase containing La as a main component element and Si. The main phase has a bcc crystal structure and an average grain diameter of 20 ?m or less.
    Type: Application
    Filed: September 20, 2007
    Publication date: April 3, 2008
    Applicant: Kabushiki KaishaToshiba
    Inventors: Akiko Saito, Tadahiko Kobayashi, Hideyuki Tsuji
  • Patent number: 7291200
    Abstract: It is an object of the present invention to provide spherical metal particles having excellent monodispersity. The present invention relates to a method of manufacturing monodisperse spherical metal particles characterized by passing liquid metal through a porous membrane so as to disperse the resulting liquid metal particles in a continuous liquid phase.
    Type: Grant
    Filed: January 26, 2005
    Date of Patent: November 6, 2007
    Assignee: Miyazaki Prefecture
    Inventors: Masataka Shimizu, Kiyoshi Torigoe, Tadao Nakashima, Izumi Akazaki
  • Patent number: 7246758
    Abstract: A metal atomizing device includes a casing with an inlet tube for providing liquid metal into the casing and an outlet is defined through the casing. The inlet tube and the outlet share a common axis. A polygonal impact member is located at an outlet of the inlet tube and a plurality of gas inlets are connected to the casing so as to provide noble gas into the casing and mixed with the liquid metal that impacts on the impact member. A collection member is located at the outlet of the casing and a pipe communicates with the collection member and the inlet tube so as to send the larger particles into the casing.
    Type: Grant
    Filed: January 31, 2006
    Date of Patent: July 24, 2007
    Inventor: Muh-Rong Wang
  • Patent number: 7220292
    Abstract: The present invention provides a metallic fiber nonwoven fabric manufacturing apparatus mainly including a metallic fiber manufacturing apparatus (7), an ejection nozzle heater (5), a metallic fiber flying apparatus (6), a nonwoven fabric surface density control mechanism, a method for manufacturing an aluminum fiber fabric by using the metallic fiber nonwoven fabric manufacturing apparatus, and a method for manufacturing a laminated aluminum material. By using the metallic fiber nonwoven fabric manufacturing apparatus, manufacture of a high-quality metallic fiber nonwoven fabric and manufacture of an aluminum fiber nonwoven fabric are possible. Further, manufacture of a laminated aluminum material is also possible.
    Type: Grant
    Filed: July 16, 2002
    Date of Patent: May 22, 2007
    Assignees: Kabushiki Kaisha Unix, Akaoarumi Kabushiki Kaisha, Toru Morimoto
    Inventors: Toru Morimoto, Kouichi Onodera, Yoshinori Nakao, Keitaro Nakayama, Masamichi Sekiya
  • Patent number: 7192649
    Abstract: A protective passivation layer is formed on the surface of an aluminum mass, such as bare aluminum particles, creating a protected aluminum mass. Formation of the protective layer onto the aluminum mass may occur from an in-situ process.
    Type: Grant
    Filed: August 6, 2003
    Date of Patent: March 20, 2007
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: R. Jason Jouet, Alfred G. Stern, David M. Rosenberg
  • Patent number: 7189278
    Abstract: A method for producing semiconductor or metal particles comprises the steps of: storing a semiconductor or metal melt in a crucible having a nozzle; supplying a gas comprising at least one selected from the group consisting of He, Ne, Ar, Kr and Xe into the crucible such that the pressure of the supplied gas in a space over the melt in the crucible is higher than the pressure of a gaseous phase into which the melt is dropped; dropping the melt from the nozzle into the gaseous phase by the pressure of the gas to form liquid particles; and solidifying the liquid particles in the gaseous phase to obtain semiconductor or metal particles. The crucible comprises at least one selected from the group consisting of hexagonal BN, cubic BN, Si3N4, TiB2, ZrB2, zirconia and stabilized zirconia at least near the nozzle.
    Type: Grant
    Filed: April 18, 2003
    Date of Patent: March 13, 2007
    Assignee: Clean Venture 21 Corporation
    Inventors: Kenji Kato, Yukio Yamaguchi, Seiichi Isomae, Masaki Miyazaki
  • Patent number: 7097686
    Abstract: Nickel powder batches and methods for producing nickel powder batches. The powder batches include particles having a small particle size, narrow size distribution and a spherical morphology. The present invention is also directed to devices incorporating the nickel metal powders.
    Type: Grant
    Filed: November 9, 2001
    Date of Patent: August 29, 2006
    Assignee: Cabot Corporation
    Inventors: Clive D. Chandler, Daniel J. Skamser, Toivo T. Kodas, Mark J. Hampden-Smith, James Caruso, Quint H. Powell
  • Patent number: 7094370
    Abstract: Metal-carbon composite powders and methods for producing metal-carbon composite powders. The powders have a well-controlled microstructure and morphology and preferably have a small average particle size. The method includes forming the particles from an aerosol of powder precursors. The invention also includes novel devices and products formed from the composite powders.
    Type: Grant
    Filed: July 31, 2002
    Date of Patent: August 22, 2006
    Assignee: Cabot Corporation
    Inventors: Toivo T. Kodas, Mark J. Hampden-Smith, James Caruso, Daniel J. Skamser, Quint H. Powell
  • Patent number: 7083747
    Abstract: Provided is an aerosol method, and accompanying apparatus, for preparing powdered products of a variety of materials involving the use of an ultrasonic aerosol generator (106) including a plurality of ultrasonic transducers (120) underlying and ultrasonically energizing a reservoir of liquid feed (102) which forms droplets of the aerosol. Carrier gas (104) is delivered to different portions of the reservoir by a plurality of gas delivery ports (136) delivering gas from a gas delivery system. The aerosol is pyrolyzed to form particles, which are then cooled and collected. The invention also provides powders that include coated particles made by the method and devices made using the coated particles.
    Type: Grant
    Filed: November 1, 2004
    Date of Patent: August 1, 2006
    Assignee: Cabot Corporation
    Inventors: Mark J Hampden-Smith, Toivo T Kodas, Quint H Powell, Daniel J Skamser, James Caruso, Clive D Chandler
  • Patent number: 7060219
    Abstract: A method and apparatus for continuous fabrication of homogeneous thin flake or powder electrolyte material from inorganic salt, metallic or similar materials or from mixtures of such materials for use in Carbonate Fuel Cell (“CFC”) power plants. Electrolyte precursor powders are fed to a continuous blender type mixer using precision metering equipment that controls material feed rates. The homogenous mixture of blended powders is then fed into a high temperature melting tank in which the mixture is melted, forming the desired molten eutectic composition. The liquid eutectic melt drips from the melting tank through ceramic or metallic nozzles and splat-cools on a rotating, water-cooled metal cylinder to produce uniform size, thin flake material. The thin flake electrolyte material can be used as-is, or it may be further processed using continuous grinding and powder fabrication equipment.
    Type: Grant
    Filed: April 30, 2004
    Date of Patent: June 13, 2006
    Assignee: FuelCell Energy, Inc.
    Inventors: Thomas M. Lucas, Jody Doyon
  • Patent number: 6923842
    Abstract: A method and apparatus are invented for producing fine particles, which can readily realize the formation of fine particles of sub-?m order to 100 micron order as well as fine particles of several micrometer which cannot be realized by a conventional method and apparatus available for producing fine particles, and a large quantity of fine particles having the desired particle diameter can be obtained with a high yield. A molten material (1), which is a molten raw material to be fragmented into fine particles, is supplied into a liquid coolant (4), boiling due to spontaneous-bubble nucleation is generated, and the molten material (1) is cooled and solidified while forming fine particles thereof by utilizing a pressure wave generated by this boiling.
    Type: Grant
    Filed: April 23, 2001
    Date of Patent: August 2, 2005
    Assignee: Central Research Institute of Electric Power Industry
    Inventor: Masahiro Furuya
  • Patent number: 6916385
    Abstract: Disclosed herein is a method of manufacturing a magnetic material which can provide a bonded magnet having excellent magnetic properties and having excellent reliability. A melt spinning apparatus 1 is provided with a tube 2 having a nozzle 3 at the bottom thereof, a coil 4 for heating the tube and a cooling roll 5 having a circumferential surface 53 in which gas expelling grooves 54 are formed. A melt spun ribbon 8 is formed by injecting the molten alloy 6 from the nozzle 6 so as to be collided with the circumferential surface 53 of the cooling roll 5, so that the molten alloy 6 is cooled and then solidified. In this process, gas is likely to enter between a puddle 7 of the molten alloy 6 and the circumferential surface 53, but such gas is expelled by means of the gas expelling grooves 54.
    Type: Grant
    Filed: April 12, 2001
    Date of Patent: July 12, 2005
    Assignee: Seiko Epson Corporation
    Inventors: Akira Arai, Hiroshi Kato
  • Patent number: 6841099
    Abstract: Metal-carbon composite powders and methods for producing metal-carbon composite powders. The powders have a well-controlled microstructure and morphology and preferably have a small average particle size. The method includes forming the particles from an aerosol of powder precursors. The invention also includes novel devices and products formed from the composite powders.
    Type: Grant
    Filed: July 31, 2002
    Date of Patent: January 11, 2005
    Assignee: Cabot Corporation
    Inventors: Toivo T. Kodas, Mark J. Hampden-Smith, James Caruso, Daniel J. Skamser, Quint H. Powell
  • Patent number: 6838021
    Abstract: The present invention provides water atomized copper powder comprising substantially irregular shaped copper particles having at least a median D50 particle size of from about 10 ?m to about 50 ?m. The powders of the present invention are suitable for use in electrically conductive compositions, such as copper-based adhesives. The present invention also provides methods of making these copper powders.
    Type: Grant
    Filed: December 10, 2001
    Date of Patent: January 4, 2005
    Assignee: SCM Metal Products, Inc.
    Inventors: Rajesh Khatter, Anil V. Nadkarni, Hsiao L. Cheng
  • Patent number: 6830633
    Abstract: A magnetic material manufacturing method, a ribbon-shaped magnetic material manufactured by the method, a powdered magnetic material formed from the ribbon-shaped magnetic material and a bonded magnet manufactured using the powdered magnet material are disclosed. The method and the magnetic materials can provide magnets having excellent magnetic properties and reliability. A melt spinning apparatus 1 is provided with a tube 2 having a nozzle 3 at the bottom thereof, a coil 4 for heating the tube and a cooling roll 5 having a circumferential surface 53 on which dimple correcting means is provided. A melt spun ribbon 8 is formed by injecting the molten alloy 6 from the nozzle 3 so as to be collided with the circumferential surface 53 of the cooling roll 5 in an inert gas atmosphere (ambient gas) such as helium gas, so that the molten alloy 6 is cooled and then solidified.
    Type: Grant
    Filed: May 30, 2001
    Date of Patent: December 14, 2004
    Assignee: Seiko Epson Corporation
    Inventors: Akira Arai, Hiroshi Kato
  • Publication number: 20040211291
    Abstract: There is provided an in-oil atomization method wherein a solder is fused and dispersed in a heated particle dispersion medium, the method being featured in that even if the quantity of the particle dispersion medium to be employed is relatively small, fine solder particles can be effectively obtained. Namely, this invention provides a method of manufacturing fine particles, wherein solder is fused in the heated particle dispersion medium to obtain a molten solder, which is then dispersed by means of an agitator to obtain molten solder particles which are subsequently cooled and solidify, the method being characterized in that the above dispersing step is performed in the presence of a particle coalescence-preventing agent. This invention also provides a fine metal particles-containing substance and a paste solder composition.
    Type: Application
    Filed: April 2, 2004
    Publication date: October 28, 2004
    Applicant: Tamura Kaken Corporation
    Inventors: Takao Ono, Yoshiyuki Takahashi, Mitsuru Iwabuchi, Yuji Ohashi
  • Patent number: 6770366
    Abstract: The invention relates to a cored wire for introducing additives into a molten metal bath comprising a metallic sheath (5) containing an additive (6), which metallic sheath is covered by a wrapping (7) which, being combustible without leaving harmful residues, momentarily retards the propagation of heat to the core of the cored wire, this cored wire being characterized in that on top of this combustible wrapping, a protective metallic casing encloses the assembly thus constituted by the additive, the metallic sheath and the combustible wrapping.
    Type: Grant
    Filed: March 16, 2001
    Date of Patent: August 3, 2004
    Assignee: Affival S.A.
    Inventors: Dominique Bernard Riche, Jean-Claude Becart
  • Publication number: 20040118244
    Abstract: Produce metal powder, especially titanium powder, offering high purity and uniform granular shape and size, in an economical manner using an apparatus that comprises a pressure-resistant container comprising a high-pressure water tank, an injector nozzle for mixture gas of oxygen and hydrogen, a material element-metal feeder part, an ignition plug and a combustion chamber.
    Type: Application
    Filed: February 19, 2004
    Publication date: June 24, 2004
    Inventors: Yoshihiro Hirata, Yoshio Ueda, Hiaroaki Takase, Kazuaki Suzuki
  • Publication number: 20040115532
    Abstract: A zinc powder for use in a zinc anode, negative electrode or electrochemical cell including zinc metal or zinc alloy particles. The zinc particles have a narrow particle size distribution and a major portion of the zinc particles having a well controlled chemistry and specific shape, such as teardrop, strand teardrop, acicular or spherical thereby providing improved discharge characteristics and reduced gassing.
    Type: Application
    Filed: August 5, 2003
    Publication date: June 17, 2004
    Inventors: Martin Malservisi, Jean-Yves Huot
  • Publication number: 20040107798
    Abstract: Produce metal particles offering high purity and uniform granular shape and size: by forming a combustion chamber comprising an injector nozzle for mixture gas of oxygen and hydrogen, an ignition device and a material metal feeder in the upper space of a high-pressure water tank filled with inert gas; igniting inside the combustion chamber via the ignition device the injector nozzle for mixture gas of oxygen and hydrogen and melting (vaporize) the material fed by the material metal feeder; and then causing the produced molten metal droplets to contact high-pressure water and let the resulting metallic particles to precipitate in water.
    Type: Application
    Filed: January 12, 2004
    Publication date: June 10, 2004
    Inventors: Yoshihiro Hirata, Yoshio Ueda, Hiroaki Takase, Kazuaki Suzuki
  • Patent number: 6713017
    Abstract: Cooling rolls are spaced to have a gas of a size greater than thickness of metal thin bodies to be produced. A nozzle is arranged to eject molten metal onto a surface of the cooling roll. The first cooling roll quenches molten metal ejected from the nozzle into metal thin bodies. On the next cooling roll, the produced metal thin bodies are hit into flakes and excessive molten metal is made into metal thin bodies. Thus, freedom of supplying the molten metal flakes can be efficiently produced.
    Type: Grant
    Filed: July 9, 2001
    Date of Patent: March 30, 2004
    Assignee: Ishikawajima-Harima Jukogyo Kabushiki Kaisha
    Inventors: Hiroki Yoshizawa, Kenji Matsuda, Kiyoshi Nebashi