Including Comminution Patents (Class 75/352)
  • Patent number: 11511393
    Abstract: A particle diameter distribution of shot media before forming an operating mix is bimodal and substantially continuous, and out of a first particle group corresponding to a first peak and a second particle group corresponding to a second peak, one is an aggregate of particles in a shape having an angular part while the other is an aggregate of particles in a shape configured with a convex curved surface.
    Type: Grant
    Filed: January 18, 2019
    Date of Patent: November 29, 2022
    Assignee: SINTOKOGIO, LTD.
    Inventors: Yuto Kato, Hayato Taniguchi
  • Publication number: 20150099117
    Abstract: Methods for producing nanoparticles of metal alloys and the nanoparticles so produced are provided. The methods include addition of surfactant and cationic metal to a novel reagent complex between zero-valent metal and a hydride. The nanoparticles of zero-valent metal alloys produced by the method include ˜7 nm zero-valent manganese-bismuth useful in fabricating a less expensive permanent magnet.
    Type: Application
    Filed: October 4, 2013
    Publication date: April 9, 2015
    Applicant: Toyota Motor Engineering & Manufacturing North America, Inc.
    Inventors: Michael Paul Rowe, Daniel Jeffrey Herrera
  • Patent number: 8979973
    Abstract: A method and a device for recovering hydrogen pulverized powder of a raw-material alloy for rare-earth magnets capable of lowering a possibility that hydrogen pulverized powder after hydrogen was pulverized remains in a recovery chamber and capable of enhancing magnetic properties by reducing an amount of oxygen of an obtained rare-earth magnet, a processing container 50 is carried into a recovery chamber 40 from a processing chamber through a carry-in port after inert gas was introduced into the recovery chamber 40 by inert gas introducing means 12, the raw-material alloy for rare-earth magnets in the processing container 50 is discharged into the recovery chamber 40 after the pressure in the recovery chamber 40 was reduced by evacuating means 33 and thereafter, inert gas is introduced into the recovery chamber 40 by inert gas introducing means 12, and the raw-material alloy for rare-earth magnets is recovered into the recovery container 50 from an discharge port 40a after a pressure in the recovery chamber
    Type: Grant
    Filed: July 7, 2010
    Date of Patent: March 17, 2015
    Assignee: Hitachi Metals, Ltd.
    Inventors: Shoji Nakayama, Kazuhiro Sonoda, Jyunichi Sanai
  • Patent number: 8979972
    Abstract: Disclosed herein is a method of manufacturing a metal flake, including the steps of: applying metal ink containing an organic metal compound onto a substrate; calcining the metal ink applied on the substrate to form a thin metal film; separating the formed thin metal film from the substrate; and pulverizing the separated thin metal film. The method of manufacturing a metal flake is characterized in that the thickness and size of metal flakes can be easily adjusted, metal flakes having excellent conductivity and gloss can be obtained, and metal flakes can be mass-produced using environmentally friendly and economical methods.
    Type: Grant
    Filed: August 24, 2009
    Date of Patent: March 17, 2015
    Assignee: Inktec Co., Ltd.
    Inventors: Kwang Choon Chung, Hyun Nam Cho, Dong Rip Kim, Ji Hoon Yoo
  • Publication number: 20150033912
    Abstract: A system for mechanical milling and a method of mechanical milling are disclosed. The system includes a container, a feedstock, and milling media. The container encloses a processing volume. The feedstock and the milling media are disposed in the processing volume of the container. The feedstock includes metal or alloy powder and a ceramic compound. The feedstock is mechanically milled in the processing volume using metallic milling media that includes a surface portion that has a carbon content less than about 0.4 weight percent.
    Type: Application
    Filed: July 30, 2013
    Publication date: February 5, 2015
    Applicant: General Electric Company
    Inventors: Laura Cerully Dial, Richard DiDomizio, Matthew Joseph Alinger, Shenyan Huang
  • Publication number: 20150021516
    Abstract: A negative active material, a lithium battery including the negative active material, and a method of preparing the negative active material. The negative active material includes a silicon-based alloy including Si, Al, and Fe. The silicon-based alloy includes an active phase of silicon nanoparticles and an inactive phase of Si3Al3Fe2 and Si2Fe in a ratios suitable to improve the lifespan of the lithium battery.
    Type: Application
    Filed: July 14, 2014
    Publication date: January 22, 2015
    Inventors: Seung-Uk Kwon, Young-Ugk Kim, Jae-Hyuk Kim, Yury Matulevich, Yo-Han Park, Chang-Ui Jeong, Soon-Sung Suh, Hee-Young Chu, Duk-Hyoung Yoon
  • Publication number: 20140373681
    Abstract: Provided is a Mo—Si—B-based alloy for a heat-resistant alloy that satisfies, more than conventional, physical properties such as proof stress and hardness adapted to an increase in the melting point of a welding object. A Mo—Si—B-based alloy powder of this invention is such that the full width at half maximum of (600) of Mo5SiB2 in X-ray diffraction peak data is 0.08 degrees or more and 0.7 degrees or less.
    Type: Application
    Filed: December 21, 2012
    Publication date: December 25, 2014
    Applicant: A.L.M.T. Corp.
    Inventors: Shigekazu Yamazaki, Ayuri Tsuji, Masahiro Katoh, Seiji Nakabayashi, Akihiko Ikegaya
  • Publication number: 20140369881
    Abstract: Methods, systems, and apparatus, including computer programs encoded on computer storage media, for recycling magnetic material to restore or improve the magnetic performance. One of the methods includes demagnetizing magnetic material from a waste magnet assembly by cyclic heating and cooling of the magnetic material, fragmenting adhesives attached to the magnetic material, cracking coating layers of the magnetic material, and subjecting the magnetic material to at least one of: a) a mechanical treatment or b) a chemical treatment, to remove the coating layers and prepare the magnetic material without impurities, fragmenting the demagnetized magnetic material to form a powder, and mixing the powder with a rare earth material R and an elemental additive A to produce a homogeneous powder, wherein the rare earth material R comprises at least one of: Nd or Pr, and the elemental additive A comprises at least one of: Nd, Pr, Dy, Co, Cu, and Fe.
    Type: Application
    Filed: June 17, 2014
    Publication date: December 18, 2014
    Inventors: Miha Zakotnik, Peter Afiuny, Scott Dunn, Catalina Oana Tudor
  • Patent number: 8852499
    Abstract: The invention concerns a nanocrystalline alloy of the formula: Fe3?xAl1+xMyTz wherein: M represents at least one catalytic specie selected from the group consisting of Ru, Ir, Pd, Pt, Rh, Os, Re, Ag and Ni; T represents at least one element selected from the group consisting of Mo, Co, Cr, V, Cu, Zn, Nb, W, Zr, Y, Mn, Cd, Si, B, C, O, N, P, F, S, Cl and Na; x is a number larger than ?1 and smaller than or equal to +1 y is a number larger than 0 and smaller or equal to +1 z is a number ranging between 0 and +1 The invention also concerns the use of this alloy in a nanocrystalline form or not for the fabrication of electrodes which in particular, can be used for the synthesis of sodium chlorate.
    Type: Grant
    Filed: May 15, 2008
    Date of Patent: October 7, 2014
    Assignees: Hydro-Québec, Meeir Technologie Inc.
    Inventors: Robert Schulz, Sylvio Savoie
  • Patent number: 8834596
    Abstract: A method for pretreating a sintering material using as a material at least two types of iron ore containing coarse grains and fine powder, using a first granulator to make the fine powder stick to coarse grains forming core grains so as to produce S-type granules, and using a second granulator to granulate only fine powder or mainly fine powder to produce P-type granules, which method producing the S-type granules by adjusting an amount of fine powder supplied into said first granulator so that the average stuck thickness of fine powder to the core grains becomes 50 to 300 ?m and supplying the remaining fine powder not supplied to said first granulator to the second granulator.
    Type: Grant
    Filed: November 11, 2005
    Date of Patent: September 16, 2014
    Assignee: Nippon Steel & Sumitomo Metal Corporation
    Inventors: Kenichi Yakashiro, Takeshi Imai, Akira Gushima, Tsuneo Ikeda
  • Patent number: 8834785
    Abstract: A method for producing a metal article according to one embodiment may involve the steps of: Providing a composite metal powder including a substantially homogeneous dispersion of molybdenum and molybdenum disulfide sub-particles that are fused together to form individual particles of the composite metal powder; and compressing the molybdenum/molybdenum disulfide composite metal powder under sufficient pressure to cause the mixture to behave as a nearly solid mass.
    Type: Grant
    Filed: July 11, 2011
    Date of Patent: September 16, 2014
    Assignee: Climax Engineered Materials, LLC
    Inventors: Matthew C. Shaw, Carl V. Cox, Yakov Epshteyn
  • Patent number: 8808468
    Abstract: The invention relates to a Fe—Si—La alloy having the atomic composition: (La1-a-a?MmaTRa?)1[(Fe1-b-b?CObMb?)1-x(Si1-cXc)x]13(CdNeH1-d-e)y(R)z(I)f Mm representing a mixture of lanthanum, cerium, neodymium and praseodynium in the weight proportion of 22 to 26% La, 48 to 53% Ce, 17 to 20% Nd and 5 to 7% Pr, the said mixture possibly comprising up to 1% by weight of impurities, TR representing one or more elements of the rare earth family other than lanthanum, M representing one or more type d transition elements of the 3d, 4d and 5d layers X representing a metalloid element selected from Ge, Al, B, Ga and In R representing one or more elements selected from Al, Ca, Mg, K and Na, I representing one or two elements selected from O and S, with: 0?a<0.5 and 0?a?<0.2 0?b?0.2 and 0?b?<0.4 0?c?0.5 and 0?d?1 0?e?1 and f?0.1 0.09?x?0.13 and 0.002?y?4 0.0001?z?0.01 the subscripts b, d, e, x and y being such that the alloy further satisfies the following condition: 6.143b(13(1?x))+4.437y[1?0.
    Type: Grant
    Filed: December 15, 2008
    Date of Patent: August 19, 2014
    Assignee: Aperam Alloys Imphy
    Inventors: Thierry Waeckerle, Herve Fraisse, Mohamed Balli, Patricia De Rango, Daniel Fruchart, Damien Gignoux, Salvatore Miraglia, Mariana Rosca, Miguel Jose Artigas Alava
  • Patent number: 8690985
    Abstract: A hydrogen storage material is formed by mixing and combining particles of a metal A selected from Mg and Al, particles of a metal B selected from Ni and Cu, and particles of an intermetallic compound A-B of the metal A and the metal B, together. A method of producing the hydrogen storage material includes a step of mixing the particles of the intermetallic compound A-B with the particles of the metal B, a step of adding particles of a hydride A-H of the metal A to the mixture and mixing them together, and a step of dehydrogenating the hydride A-H to convert it to the metal A.
    Type: Grant
    Filed: July 25, 2008
    Date of Patent: April 8, 2014
    Assignee: Toyota Jidosha Kabushiki Kaisha
    Inventors: Tamio Shinozawa, Takanobu Yamada
  • Publication number: 20140072827
    Abstract: A mixed powder of an Ni—Al alloy and alumina is produced by heating a first mixed powder, which is prepared by mixing an Ni—Al mixed powder as prepared by mixing an Al powder with Ni in such a manner that Al therein could fall within a range of from 25 atomic % to 60 atomic %, and an alumina powder in a range of from 40% by mass to 60% by mass, in vacuum or in an inert gas atmosphere at a temperature falling within a range of from 600° C. to 1300° C. for at least 1 hour, and then grinding the resulting product.
    Type: Application
    Filed: March 27, 2013
    Publication date: March 13, 2014
    Applicant: NATIONAL INSTITUTE FOR MATERIALS SCIENCE
    Inventor: NATIONAL INSTITUTE FOR MATERIALS SCIENCE
  • Publication number: 20130164165
    Abstract: Disclosed is a method of forming a multi-element thermoelectric alloy. A plurality of binary alloys and milling balls are put in a milling pot to perform a ball-milling process to obtain a multi-element thermoelectric alloy powders. The milling balls have a diameter of 1 mm to 10 mm. The milling balls and the binary alloys have a weight ratio of 1:1 to 50:1. The rotation rate of the ball-milling process is of 200 rpm to 1000 rpm. The ball-milling process is processed for 4 hours to 12 hours.
    Type: Application
    Filed: March 29, 2012
    Publication date: June 27, 2013
    Applicant: INDUSTRIAL TECHNOLOGY RESEARCH INSTITUTE
    Inventors: Chien-Hsuan Yeh, Ya-Wen Chou, Chia-Hung Kuo
  • Publication number: 20130142690
    Abstract: A safe and industrially advantageous production method is disclosed for producing a rare earth-Mg—Ni based hydrogen storage alloy which realizes production of a nickel-hydrogen rechargeable battery having excellent cycle characteristics and a large capacity. The method is for producing a rare earth-Mg—Ni based hydrogen storage alloy including element A, Mg, and element B, wherein element A is composed of at least one element R selected from rare earth elements including Sc and Y, and optionally at least one element selected from Zr, Hf, and Ca, and element B is composed of Ni and optionally at least one element selected from elements other than element A and Mg. The method includes first step of mixing an alloy consisting of elements A and B and Mg metal and/or a Mg-containing alloy having a melting point not higher than the melting point of Mg metal, and second step of heat-treating a mixture obtained from first step for 0.5 to 240 hours at a temperature 5 to 250° C.
    Type: Application
    Filed: June 24, 2011
    Publication date: June 6, 2013
    Applicant: SANTOKU CORPORATION
    Inventors: Takayuki Otsuki, Toshio Irie
  • Patent number: 8444915
    Abstract: The invention concerns a method for making a thermoelectric element consisting mainly of a crystalline alloy having a cubic structure, the alloy comprising a first constituent having at least a first element selected among the transition metals, a second constituent having at least one element selected among column XIV, XV or XVI of the periodic table, and a third constituent having at least one constituent selected among rare earths, alkalis, alkaline earths or actinides. The method includes making the alloy in the form of nanopowders by mechanosynthesis. The invention also concerns the thermoelectric material obtained by implementing said method.
    Type: Grant
    Filed: April 5, 2006
    Date of Patent: May 21, 2013
    Assignee: Centre National de la Recherche Scientifique (CNRS)
    Inventors: David Berardan, Eric Alleno, Claude Godart, Eric Leroy
  • Publication number: 20130071283
    Abstract: Titanium alloy complex powder is yielded by hydrogenating titanium alloy raw material to generate hydrogenated titanium alloy, grinding and sifting it to obtain hydrogenated titanium alloy powder, adding ceramic powder selected from SiC, TiC, SiOx, TiOx (here, index x is a real number which is in 1?x?2) and Al2O3, and dehydrogenating the mixture of the hydrogenated titanium alloy powder and the ceramic powder. In addition, consolidated titanium alloy material is obtained by CIP process and subsequent HIP process to the titanium alloy complex powder or by HIP process after filling the titanium alloy complex powder into capsule.
    Type: Application
    Filed: May 30, 2011
    Publication date: March 21, 2013
    Applicant: TOHO TITANIUM CO., LTD.
    Inventors: Osamu Kano, Hideo Takatori, Satoshi Sugawara
  • Publication number: 20130039825
    Abstract: A method for preparation of a getter material on the basis of intermetallic compounds of barium is described. The method comprises preparing a melt of a ternary mixture containing barium, metal and sodium; directionally solidifying the melt to produce a textured ingot; granulating the textured ingot, thereby obtaining granules having open-ended voids extending therethrough; and evaporating the sodium from the granules by applying a thermovacuum treatment to the granules. The textured ingot comprises a getter body made of intermetallic compounds of barium; and open-ended voids within the getter body.
    Type: Application
    Filed: September 2, 2010
    Publication date: February 14, 2013
    Applicant: FREESPACE MATERIALS LTD.
    Inventor: Konstantin Chuntonov
  • Patent number: 8361242
    Abstract: A powder consists essentially by weight, of 28.00?R?32.00%, where R is at least one rare earth element including Y and the sum of Dy+Tb>0.5, 0.50?B?2.00%, 0.50?Co?3.50%, 0.050?M?0.5%, where M is one or more of the elements Ga, Cu and Al, 0.25 wt %<O?0.5%, 0.15% or less of C, balance Fe.
    Type: Grant
    Filed: March 24, 2011
    Date of Patent: January 29, 2013
    Assignee: Vacuumschmeize GmbH & Co. KG
    Inventors: Rolf Blank, Matthias Katter, Werner Rodewald, Boris Wall
  • Patent number: 8328899
    Abstract: The invention relates to a process for the production of metal alloy powders, in particular the invention relates to a process for producing titanium metal alloys from titanium dioxide and aluminium. Optionally the process can also include the use of one or more other oxides (metal or non-metal). The result is at least a Ti—Al alloy powder. If another metal oxide is used the result is a Ti-ternary alloy powder. If SiO2 is used the result is a Ti—Al—Si alloy.
    Type: Grant
    Filed: July 20, 2007
    Date of Patent: December 11, 2012
    Assignee: Titanox Development Limited
    Inventors: Gorgees Adam, Jing Liang
  • Patent number: 8257464
    Abstract: The present invention relates to pulverulent materials suitable for storing hydrogen, and more particularly to a method of preparing such a material, in which: (A) a composite metallic material having a specific granular structure is prepared by co-melting the following mixtures: a first metallic mixture (m1), which is an alloy (a1) of body-centered cubic crystal structure, based on titanium, vanadium, chromium and/or manganese, or a mixture of these metals in the proportions of the alloy (a1); and a second mixture (m2), which is an alloy (a2), comprising 38 to 42% zirconium, niobium, molybdenum, hafnium, tantalum and/or tungsten and 56 to 60 mol % of nickel and/or copper, or else a mixture of these metals in the proportions of the alloy (a2), with a mass ratio (m2)/(m1+m2) ranging from 0.1 wt % to 20 wt %; and (B) the composite metallic material thus obtained is hydrogenated, whereby the composite material is fragmented (hydrogen decrepitation).
    Type: Grant
    Filed: February 22, 2007
    Date of Patent: September 4, 2012
    Assignee: Centre National de la Recherche Scientifique (C.N.R.S.)
    Inventors: Jean Charbonnier, Patricia De Rango, Daniel Fruchart, Salvatore Miraglia, Sophie Rivoirard, Natalia Skryabina
  • Publication number: 20120093676
    Abstract: Disclosed herein is a composite material comprising a metal and nanoparticles, in particular carbon nano tubes as well as a method of producing the same. A metal powder and the nanoparticles are processed by mechanical alloying, such as to form a composite comprising metal crystallites having an average size in the range of 1-100 nm, preferably 10 to 100 nm or in a range of more than 100 nm and up to 200 nm at least partly separated from each other by said nanoparticles.
    Type: Application
    Filed: January 28, 2010
    Publication date: April 19, 2012
    Applicant: Bayer International SA
    Inventors: Henning Zoz, Michael Dvorak, Horst Adams
  • Patent number: 8088193
    Abstract: A method for making nanoparticles includes the steps of dipping a metal element in a solution that contains metallic ions or ions with a metal, wherein the metal element has a lower electronegativity or redox potential than that of the metal in the ions, and rubbing the metal element to make nanoparticles. Another method for making nanoparticles includes the steps of dipping a metal element in a solution that contains metallic ions or ions with a metal, wherein the metal element has a lower electronegativity or redox potential than that of the metal in the ions, and applying sonic energy to at least one of the metal element and solution. A further method for making copper nanoparticles includes the step of adding ascorbic acid to a copper salt solution.
    Type: Grant
    Filed: December 17, 2007
    Date of Patent: January 3, 2012
    Inventors: Taofang Zeng, Chunwei Wu
  • Publication number: 20110252922
    Abstract: A method is provided for producing a diffusion alloyed powder consisting of an iron or iron-based core powder having particles of an alloying powder containing Cu and Ni bonded to the surface of the core particles, comprising providing a unitary alloying powder capable of forming particles of a Cu and Ni containing alloy, mixing the unitary alloying powder with the core powder, and heating the mixed powders in a non-oxidizing or reducing atmosphere to a temperature of 500-1000° C. during a period of 10-120 minutes to convert the alloying powder into a Cu and Ni containing alloy, so as to diffusion bond particles of the Cu and Ni alloy to the surface of the iron or iron-based core powder. The alloying powder may be a Cu and Ni alloy, oxide, carbonate or other suitable compound that on heating will form a Cu and Ni alloy.
    Type: Application
    Filed: December 16, 2009
    Publication date: October 20, 2011
    Inventor: Mats Larsson
  • Patent number: 8034156
    Abstract: A method for producing a decomposer of an organic halogenated compound comprises subjecting an iron powder produced beforehand to plastic deformation that gives the iron powder particles a flat shape. Further, an iron powder and a copper salt powder are mechanically mixed in a ball mill to produce a copper salt-containing iron particle powder in which the particles of the two powders are joined. In this case, the method for producing the decomposer of an organic halogenated compound is characterized in that the iron powder is mechanically deformed to give the particles a flat shape.
    Type: Grant
    Filed: March 22, 2006
    Date of Patent: October 11, 2011
    Assignee: Dowa Eco-System Co., Ltd.
    Inventors: Masami Kamada, Taishi Uehara
  • Patent number: 8025710
    Abstract: Provided are an ancillary material, used for shape processing, which is capable of shortening a processing time, avoiding a reduction in quality of a shape provided to a workpiece material, and allowing a relatively low manufacturing cost; a processing method using the ancillary material; and a method of manufacturing the ancillary material. The tungsten alloy grains (1) comprise: tungsten of greater than or equal to 80% by mass and less than or equal to 98% by mass; nickel; at least one kind of metal selected from the group consisting of iron, copper, and cobalt; and an inevitable impurity, a maximum diameter thereof is greater than or equal to 0.1 mm and less than or equal to 5.00 mm, and a specific surface area thereof is less than or equal to 0.02 m2/g. The tungsten alloy grains (1, 10), the workpiece material (30), an abrasive (20) are blended in a container (100) and the container is rotated, thereby processing the shape of the workpiece material (30).
    Type: Grant
    Filed: November 20, 2006
    Date of Patent: September 27, 2011
    Assignee: A.L.M.T. Corp.
    Inventors: Shinji Kikuhara, Hitoshi Inoue, Noboru Uenishi, Satoshi Umemoto
  • Patent number: 8012452
    Abstract: The invention relates to a method for preparation of a material adapted to reversible storage of hydrogen, including steps consisting of providing a first powder of a magnesium-based material, hydrogenating the first powder to convert at least part of the first powder into metal hydrides, mixing the first hydrogenating powder with a second powder additive, the proportion by mass of the second powder in the mix obtained being between 1% and 20% by mass, wherein the additive is formed from an alloy with a centred cubic structure based on titatnium, vanadium and at least one other metal chosen from chromium or manganese, and grinding the mix of first and second powders.
    Type: Grant
    Filed: April 25, 2007
    Date of Patent: September 6, 2011
    Assignee: Centre National de la Recherche Scientifique
    Inventors: Daniel Fruchart, Patricia De Rango, Jean Charbonnier, Salvatore Miraglia, Sophie Rivoirard, Nataliya Skryabina, Michel Jehan
  • Publication number: 20110020661
    Abstract: The invention relates to a Fe—Si—La alloy having the following atomic composition: (La1-a-a?MmaTRa?)1[(Fe1-b-b,CobMb,)1-x(Si1-cXc)x]13(CdNeH1-d-e)y(R)r(I)r, in which Mm is a mixture of lanthanum, cerium, neodymium and praseodymium in a weight proportion of 22 to 26% of La, 48 to 53% of Ce, 17 to 20% of Nd and 5 to 7% of Pr, wherein said mixture may include up to 1 wt % of impurities, TR is one or more elements of the rare earth family other than lanthanum, M is one or more d-type transition element from layers 3d, 4d and 5d, X is a metalloid element selected from Ge, Al, B, Ga and In, R is one or more element selected from Al, Ca, Mg, K and Na, I is one or two elements selected from O and S, with: 0?a<0.5 and 0?a?<0.2; 0?b?0.2 and 0?b?<0.4; 0?c?0.5 and 0?d?1; 0?e?1 and f?0.1; 0.09?x?0.13 and 0.002?y?4; 0.0001?z?0.01; the indicia b, d, e, x and y being such that the alloy further meets the following condition: 6.143b(13(1?x))+4.437y[1?0.0614(d++e)]?1 Eq.1 d*y?0.005 Eq.2.
    Type: Application
    Filed: December 15, 2008
    Publication date: January 27, 2011
    Applicants: ARCELORMITTAL-STAINLESS & NICKEL ALLOYS, CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE
    Inventors: Thierry Waeckerle, Herve Fraisse, Mohamed Balli, Patricia De Rango, Daniel Fruchart, Damien Gignoux, Salvatore Miraglia, Mariana Rosca, Miguel Jose Artigas Alava
  • Patent number: 7824507
    Abstract: A method of producing high strength nanophase metal alloy powder by cryomilling metal powder under conditions which cause the formation of intrinsic nitrides, and of producing high strength metal articles by subjecting the nitrided cryomilled powder to thermo-mechanical processing. The intrinsic nitrides present within the alloy significantly reduce grain growth during thermo-mechanical processing, resulting in formed metal products of high strength and improved ductility.
    Type: Grant
    Filed: January 25, 2008
    Date of Patent: November 2, 2010
    Assignee: The Boeing Company
    Inventors: Thomas J. Van Daam, Clifford C. Bampton
  • Patent number: 7776131
    Abstract: A manufacturing method for an oxide-dispersed alloy wherein dispersed particles consisting of oxides of one or two or more additive metals are dispersed in a matrix metal, comprising the steps of (a) manufacturing alloy powder or an alloy wire rod consisting of the matrix metal and the additive metal; (b) oxidizing the additive metal in the alloy powder by water to form dispersed particles by introducing the alloy powder or alloy wire rod into a high-energy ball mill with water and by making agitation; and (c) moldedly solidifying the alloy powder or alloy wire rod after oxidation. The present invention is especially useful in manufacturing oxide-dispersed alloys in which the free energy of oxide formation of the matrix metal is higher than water standard free energy of formation, and the free energy of oxide formation of the additive metal is lower than water standard free energy of formation.
    Type: Grant
    Filed: August 22, 2005
    Date of Patent: August 17, 2010
    Assignee: Tanaka Kikinzoku Kogyo K.K.
    Inventors: Toru Shoji, Seiichiro Tanaka, Seiji Takeishi, Hideo Segawa
  • Publication number: 20100154589
    Abstract: Provided is a method of producing a nitride/tungsten nanocomposite powder. The method includes mixing nitride with tungsten or a tungsten alloy, and mechanically alloying the mixture in an inert atmosphere using a milling machine.
    Type: Application
    Filed: October 30, 2009
    Publication date: June 24, 2010
    Inventors: Soonhyung Hong, Kyongho Lee, Yoochul Shin, Dongju Lee
  • Publication number: 20100150822
    Abstract: The present invention relates to pulverulent materials suitable for storing hydrogen, and more particularly to a method of preparing such a material, in which: (A) a composite metallic material having a specific granular structure is prepared by co-melting the following mixtures: a first metallic mixture (m1), which is an alloy (a1) of body-centred cubic crystal structure, based on titanium, vanadium, chromium and/or manganese, or a mixture of these metals in the proportions of the alloy (a1); and a second mixture (m2), which is an alloy (a2), comprising 38 to 42% zirconium, niobium, molybdenum, hafnium, tantalum and/or tungsten and 56 to 60 mol % of nickel and/or copper, or else a mixture of these metals in the proportions of the alloy (a2), with a mass ratio (m2)/(m1+m2) ranging from 0.1 wt % to 20 wt %; and (B) the composite metallic material thus obtained is hydrogenated, whereby the composite material is fragmented (hydrogen decrepitation).
    Type: Application
    Filed: February 22, 2007
    Publication date: June 17, 2010
    Applicant: Centre National De La Recherche Scientifique (C.N. R.S.)
    Inventors: Jean Charbonnier, Patricia De Rango, Daniel Fruchart, Salvatore Miraglia, Sophie Rivoirard, Natalia Skryabina
  • Publication number: 20100119400
    Abstract: A silver free high noble dental alloy comprising at least 60 wt. % noble materials, where 40 wt. % of the material is gold; at least 2.5 wt. % gallium, at least about from 2 to 4 wt. % cobalt; and at least from about 0.01 to 0.25 wt. % lithium and/or boron; and a principal balance of palladium is provided. Dental products and methods of manufacturing dental products using such a high noble dental alloys are also provided.
    Type: Application
    Filed: November 12, 2009
    Publication date: May 13, 2010
    Inventors: Arun Prasad, Paul J. Cascone
  • Publication number: 20100107816
    Abstract: The invention relates to a method of making metal flakes by low- or high-kinetic milling, also known as mechanical alloying. The object of the invention is to further improve such a known method such that it is also suitable for making metal flakes having improved properties. The object is attained according to the invention in that at least one further alloying additive is provided in addition to a metal base material, and that making the metal flakes is carried out by kinetic milling of the base material together with the at least one alloying additive such that the base material and the alloying additive are mechanically alloyed with each other.
    Type: Application
    Filed: October 29, 2009
    Publication date: May 6, 2010
    Inventors: Henning ZOZ, David Jaramillo-Vigueras
  • Patent number: 7699905
    Abstract: A method of making dispersion-strengthened alloy particles involves melting an alloy having a corrosion and/or oxidation resistance-imparting alloying element, a dispersoid-forming element, and a matrix metal wherein the dispersoid-forming element exhibits a greater tendency to react with a reactive species acquired from an atomizing gas than does the alloying element. The melted alloy is atomized with the atomizing gas including the reactive species to form atomized particles so that the reactive species is (a) dissolved in solid solution to a depth below the surface of atomized particles and/or (b) reacted with the dispersoid-forming element to form dispersoids in the atomized particles to a depth below the surface of said atomized particles. The atomized alloy particles are solidified as solidified alloy particles or as a solidified deposit of alloy particles.
    Type: Grant
    Filed: May 8, 2006
    Date of Patent: April 20, 2010
    Assignee: Iowa State University Research Foundation, Inc.
    Inventors: Iver E. Anderson, Robert L. Terpstra
  • Publication number: 20100075133
    Abstract: There are provided a surface coating material for a molten zinc bath member with improved zinc corrosion resistance, a production method thereof, and a molten zinc bath member. The surface coating material comprises WC powder particles and a binder metal. The binder metal comprises Co and a metal element electrochemically nobler than Co and constitutes an alloy structure having a single phase.
    Type: Application
    Filed: April 4, 2008
    Publication date: March 25, 2010
    Applicant: SANYO SPECIAL STEEL CO., LTD.
    Inventors: Hiroki Ikeda, Katsu Yanagimoto
  • Publication number: 20100064851
    Abstract: A method for kneading a carbon nanomaterial with a metal material and manufacturing a composite-metal-forming material. A semi-molten metal material obtained by heating the metal material to a temperature of a region where a solid and a liquid are both present is kneaded with the carbon nanomaterial, and the composite metal material is obtained. The composite metal material is heated to the solution temperature of the metal material, and a solution treatment is performed, whereby the composite-metal-forming material is obtained.
    Type: Application
    Filed: September 18, 2008
    Publication date: March 18, 2010
    Inventors: Taku Kawano, Tomoyuki Sato, Atsushi Kato, Masashi Suganuma, Keita Arai, Daisuke Shiba
  • Publication number: 20100068526
    Abstract: Material in particle or powder form containing carbon nano tubes (CNT), where in the material for example a metal is laminated in layers of a thickness of 10 nm to 500,000 nm alternating with layers of CNT in a thickness from 10 nm to 100,000 nm. The material is produced by mechanical alloying i.e. by repeated deformation, breaking and welding of metal particles and CNT particles, preferably by milling in a ball mill containing a milling chamber and milling balls as the milling bodies and a rotary body to generate high energy ball collisions.
    Type: Application
    Filed: October 10, 2007
    Publication date: March 18, 2010
    Inventors: Horst Adams, Michael Dvorak
  • Publication number: 20100015003
    Abstract: The invention relates to a process for the production of metal alloy powders, in particular the invention relates to a process for producing titanium metal alloys from titanium dioxide and aluminium. Optionally the process can also include the use of one or more other oxides (metal or non-metal). The result is at least a Ti—Al alloy powder. If another metal oxide is used the result is a Ti-ternary alloy powder. If SiO2 is used the result is a Ti—Al—Si alloy.
    Type: Application
    Filed: July 20, 2007
    Publication date: January 21, 2010
    Applicant: TITANOX DEVELOPMENT LIMITED
    Inventors: Gorgees Adam, Jing Liang
  • Patent number: 7621976
    Abstract: Provided are silver-containing powders and a method and apparatus for manufacturing the silver-containing particles of high quality, of a small size and narrow size distribution. An aerosol is generated from liquid feed and sent to a furnace, where liquid in droplets in the aerosol is vaporized to permit formation of the desired particles, which are then collected in a particle collector. The aerosol generation involves preparation of a high quality aerosol, with a narrow droplet size distribution, with close control over droplet size and with a high droplet loading suitable for commercial applications.
    Type: Grant
    Filed: December 21, 2006
    Date of Patent: November 24, 2009
    Assignee: Cabot Corporation
    Inventors: Mark J. Hampden-Smith, Toivo T. Kodas, Quint H. Powell, Daniel J. Skamser, James Caruso, Clive Chandler
  • Publication number: 20090277302
    Abstract: The purpose of the present invention is to separate excess coppers leached out in a lead-free solder bath and recover tin with high efficiency. An element X for forming a (CuX)6Sn5 compound between copper and tin in molten lead-free solders is added to separate out a (CuX)6Sn5 compound. Tin is recovered by binding the (CuX)6Sn5 compound by passing thereof through a multi-perforated plate, further generating swirling currents to precipitate and separate the bound (CuX)6Sn5 compounds and removing thereof.
    Type: Application
    Filed: July 20, 2009
    Publication date: November 12, 2009
    Applicant: Nihon Superior Sha Co., Ltd.
    Inventor: Tetsuro Nishimura
  • Publication number: 20090260482
    Abstract: An earth-boring drill bit having a bit body with a cutting component formed from a tungsten carbide composite material is disclosed. The composite material includes a binder and tungsten carbide crystals comprising sintered pellets. The composite material may be used as a hardfacing on the body and/or cutting elements, or be used to form portions or all of the body and cutting elements. The pellets may be formed with a single mode or multi-modal size distribution of the crystals.
    Type: Application
    Filed: February 24, 2009
    Publication date: October 22, 2009
    Applicant: Baker Hughes Incorporated
    Inventors: David A. Curry, James L. Overstreet, Jimmy W. Eason
  • Publication number: 20090249920
    Abstract: The present invention provides an amorphous alloy powder and magnetic powder cores exhibiting excellent high frequency properties and a method for making themof. The composition of said alloy powder by atomic percentage satisfies the following formula: (Fe1-xMx)100-a-b-cPaTbDc, wherein M represents at least one element of Co and Ni; T is over three elements selected from Al, C, B and Si, D is at least one element of Sn, Cr, Mn, Mo, W, V, Nb, Ta, Ti, Zr, Hf, Pt, Pd and Au; the subscripts x, a, b, and c satisfy the relationships 0.01?x?0.16, 8?a?15, 10?b?25 and 0.5?c?6. The said amorphous alloy powder is made by atomization method and a magnetic powder core comprises a molded article of mixture of the said alloy powder and an insulating material. A method of making the amorphous alloy powder core includes the steps of screening, insulating, compacting, annealing and spray painting.
    Type: Application
    Filed: May 26, 2009
    Publication date: October 8, 2009
    Inventors: Zhichao Lu, Caowei Lu, Deren Li, Ko Sun, Shaoxlong Zhou
  • Publication number: 20090226340
    Abstract: A method of making a degradable alloy includes adding one or more alloying products to an aluminum or aluminum alloy melt; dissolving the alloying products in the aluminum or aluminum alloy melt, thereby forming a degradable alloy melt; and solidifying the degradable alloy melt to form the degradable alloy. A method for manufacturing a product made of a degradable alloy includes adding one or more alloying products to an aluminum or aluminum alloy melt in a mould; dissolving the one or more alloying products in the aluminum or aluminum alloy melt to form a degradable alloy melt; and solidifying the degradable alloy melt to form the product. A method for manufacturing a product made of a degradable alloy includes placing powders of a base metal or a base alloy and powders of one or more alloying products in a mould; and pressing and sintering the powders to form the product.
    Type: Application
    Filed: February 24, 2009
    Publication date: September 10, 2009
    Applicant: SCHLUMBERGER TECHNOLOGY CORPORATION
    Inventor: Manuel Marya
  • Publication number: 20090208364
    Abstract: The invention concerns a method for making a thermoelectric element consisting mainly of a crystalline alloy having a cubic structure, the alloy comprising a first constituent having at least a first element selected among the transition metals, a second constituent having at least one element selected among column XIV, XV or XVI of the periodic table, and a third constituent having at least one constituent selected among rare earths, alkalis, alkaline earths or actinides. The method includes making the alloy in the form of nanopowders by mechanosynthesis. The invention also concerns the thermoelectric material obtained by implementing said method.
    Type: Application
    Filed: April 5, 2006
    Publication date: August 20, 2009
    Applicant: Centre National de la Recherche Scientifique (CNRS)
    Inventors: David Berardan, Eric Alleno, Claude Godart, Eric Leroy
  • Publication number: 20090193935
    Abstract: The present invention relates to the a method for manufacturing high strength ultra-fine/nano-structured aluminum/aluminum nitride or aluminum alloy/aluminum nitride composites using mechanical milling or mechanical alloying process which is conducted in the nitride-forming atmosphere such as nitrogen gas (N), ammonia gas (NH) or mixed gas including both gases, subsequent heat treatment process, and hot consolidation process. Also, high strength ultra-fine/nano-structured Al/ALN or Al alloy/ALN composite materials fabricated by the method of present invention have superior mechanical strength and heat resistance to those fabricated by conventional powder metallurgy process or liquid processes.
    Type: Application
    Filed: May 30, 2006
    Publication date: August 6, 2009
    Applicant: Dynamaterials Co., Inc.
    Inventors: Kwang Seon Shin, Seung Hoon Yu
  • Publication number: 20090175752
    Abstract: An electrosurgical forceps has at least the tip of one blade member formed of a composite material having aligned elongated particles of nickel interspersed in a matrix of silver particles. The tip can be provided as a tip member attached, such as by brazing, to the body of the blade member, or the entire blade member can be formed of the silver/nickel composite material. In another embodiment, the tip or blade member is formed of a dispersion strengthened silver or copper composite material.
    Type: Application
    Filed: March 5, 2009
    Publication date: July 9, 2009
    Applicant: Kirwan Surgical Products, Inc.
    Inventors: John P. Ariola, JR., Lawrence T. Kirwan
  • Patent number: 7537637
    Abstract: The present invention relates to a method of making an agglomerated powder mixture by wet milling a powder mixture containing hard constituent powder(s) based on carbides of Ti, Zr, Hf, V, Nb, Ta, Cr, Mo and/or W and greater than about 15 wt-% binder phase powder(s) of Co and/or Ni as well as pressing agents and spray drying said slurry. By adding to said powder mixture before milling in addition from about 0.05 to about 0.50 wt-% of a complex forming and/or pH-decreasing/increasing additive such as triethanolamine, hydroxides or acids and a thickener in an amount of from about 0.01 to about 0.10 wt-% agglomerates with excellent flow properties are obtained.
    Type: Grant
    Filed: May 16, 2006
    Date of Patent: May 26, 2009
    Assignee: Sandvik Intellectual Property AB
    Inventors: Ulf Jutterström, Annika Kauppi
  • Patent number: RE40717
    Abstract: The present invention relates to a method of making a cemented carbide with submicron WC grain size with a powder metallurgical technique including milling, pressing and sintering. The method includes milling all components except WC for about three hours, then adding the WC powder and milling for about ten additional hours. In this way a cemented carbide powder with acceptable low compacting pressure is obtained.
    Type: Grant
    Filed: July 12, 2006
    Date of Patent: June 9, 2009
    Assignee: Sandvik Intellectual Property AB
    Inventor: Mats Waldenstrom