Adding Solid Patents (Class 75/604)
  • Patent number: 10422017
    Abstract: A method for reducing impurities in magnesium comprises: combining a zirconium-containing material with a molten low-impurity magnesium including no more than 1.0 weight percent of total impurities in a vessel to provide a mixture; holding the mixture in a molten state for a period of time sufficient to allow at least a portion of the zirconium-containing material to react with at least a portion of the impurities and form intermetallic compounds; and separating at least a portion of the molten magnesium in the mixture from at least a portion of the intermetallic compounds to provide a purified magnesium, wherein the purified magnesium includes an increased level of zirconium compared to the low-impurity magnesium, wherein the purified magnesium includes greater than 1000 ppm zirconium, and wherein the purified magnesium includes a reduced level of impurities other than zirconium compared to the low-impurity magnesium.
    Type: Grant
    Filed: July 23, 2018
    Date of Patent: September 24, 2019
    Assignee: ATI PROPERTIES LLC
    Inventors: Scott Coffin, Arnel M. Fajardo
  • Patent number: 8808423
    Abstract: Provided is a manufacturing method of a magnesium-based alloy for high temperature. The manufacturing method includes melting a magnesium (Mg) or magnesium alloy into a liquid phase, adding calcium oxide (CaO) 1.4 times the weight of a final calcium (Ca) target composition onto a surface of a melt in which the magnesium or the magnesium alloy is melted, forming a targeted amount of Ca in the magnesium or magnesium alloy through a reduction reaction between the melt and the added CaO. Specifically, the amount of Ca formed is in the range of 0.8 wt % to 2.4 wt %, and a final composition of the Mg alloy includes 6.0-8.0 wt % of aluminum (Al), 0.1-0.3 wt % of manganese (Mn), 0.2-0.3 wt % of strontium (Sr), less than 0.04 wt of zinc (Zn), less than 0.9 wt of tin (Sn), and a balance being Mg.
    Type: Grant
    Filed: March 18, 2011
    Date of Patent: August 19, 2014
    Assignee: Korea Institute of Industrial Technology
    Inventors: Shae K. Kim, Jung-Ho Seo
  • Publication number: 20140202284
    Abstract: The present invention relates to a magnesium-based alloy, and to a method for producing same. The method comprises the steps of: melting a magnesium alloy into a liquid state; adding a silicon compound to said molten magnesium alloy; exhausting the silicon compound through a full reaction between said molten magnesium alloy and said added silicon compound such that the silicon compound does not substantially remain in the magnesium alloy; and exhausting the silicon produced as a result of said exhaustion in the precious step such that the silicon may not substantially remain in said magnesium alloy.
    Type: Application
    Filed: May 18, 2012
    Publication date: July 24, 2014
    Applicant: KOREA INSTITUTE OF INDUSTRIAL TECHNOLOGY
    Inventors: Shae K. Kim, Young Ok Yoon, Jin Kyu Lee, Jung Ho Seo, Hyun Kyu Im
  • Publication number: 20140050608
    Abstract: A method for reducing impurities in magnesium comprises: combining a zirconium-containing material with a molten low-impurity magnesium including no more than 1.0 weight percent of total impurities in a vessel to provide a mixture; holding the mixture in a molten state for a period of time sufficient to allow at least a portion of the zirconium-containing material to react with at least a portion of the impurities and form intermetallic compounds; and separating at least a portion of the molten magnesium in the mixture from at least a portion of the intermetallic compounds to provide a purified magnesium including greater than 1000 ppm zirconium. A purified magnesium including at least 1000 ppm zirconium and methods for producing zirconium metal using magnesium reductant also are disclosed.
    Type: Application
    Filed: August 14, 2012
    Publication date: February 20, 2014
    Applicant: ATI PROPERTIES, INC.
    Inventors: Scott Coffin, Arnel M. Fajardo
  • Patent number: 8540797
    Abstract: A method to introduce ceramic particles into liquid metal through the polymeric precursor route by cross-linking organic precursor into a hard polymer, which is added to the liquid melt for in-situ pyrolysis of the organic into the ceramic phase. The starting material, the organic, for the above process can be in the form of a liquid or a solid. If it is a solid it is usually dissolved into a solvent to create a liquid form. The organic is then cross linked either directly by a thermal process, by adding a catalyst, or by the well known sol-gel process into a hard polymer. It is this hard polymer which is then pyrolyzed into a high temperature ceramic material by the process outlined above.
    Type: Grant
    Filed: July 29, 2008
    Date of Patent: September 24, 2013
    Assignee: Indian Institute of Science
    Inventors: Rishi Raj, Mirle Krishnegowda Surappa, Sudarshan
  • Patent number: 8357225
    Abstract: The present disclosure provides a method for making magnesium-based composite material. The method comprises the following steps. Firstly, a semi-solid-state magnesium-based material is provided. Secondly, at least one nanoscale reinforcement is added into the semi-solid-state magnesium-based material to obtain a semi-solid-state mixture. Thirdly, the semi-solid-state mixture is heated to a liquid-state mixture. Fourthly, the liquid-state mixture is ultrasonically processed. Fifthly, the liquid-state mixture is cooled to obtain the magnesium-based composite material.
    Type: Grant
    Filed: July 10, 2010
    Date of Patent: January 22, 2013
    Assignees: Tsinghua University, Hon Hai Precision Industry Co., Ltd.
    Inventors: Wen-Zhen Li, Shi-Ying Liu
  • Publication number: 20120115708
    Abstract: A process for producing particle-reinforced composite materials through utilization of an in situ reaction to produce a uniform dispersion of a fine particulate reinforcement phase. The process includes forming a melt of a first material, and then introducing particles of a second material into the melt and subjecting the melt to high-intensity acoustic vibration. A chemical reaction initiates between the first and second materials to produce reaction products in the melt. The reaction products comprise a solid particulate phase, and the high-intensity acoustic vibration fragments and/or separates the reaction products into solid particles that are dispersed in the melt and are smaller than the particles of the second material. Also encompassed are particle-reinforced composite materials produced by such a process.
    Type: Application
    Filed: November 10, 2011
    Publication date: May 10, 2012
    Applicant: PURDUE RESEARCH FOUNDATION
    Inventors: Qingyou Han, Zhiwei Liu
  • Publication number: 20110236250
    Abstract: Provided is a magnesium alloy for room temperature, which is manufactured by adding CaO onto a surface of a molten magnesium alloy and exhausting the CaO through a reduction reaction of the CaO with the molten magnesium alloy. Resultantly, the magnesium alloy with CaO added has more improved room-temperature mechanical properties (tensile strength, yield strength, elongation) than magnesium alloys without using CaO. Furthermore, as the added amount of CaO increases, room-temperature mechanical properties (tensile strength, yield strength, elongation) increase as well.
    Type: Application
    Filed: March 22, 2011
    Publication date: September 29, 2011
    Applicant: KOREA INSTITUTE OF INDUSTRIAL TECHNOLOGY
    Inventors: Shae K. KIM, Jung-Ho SEO
  • Publication number: 20110236251
    Abstract: Provided is a manufacturing method of a magnesium-based alloy for high temperature. The manufacturing method includes melting a magnesium (Mg) or magnesium alloy into a liquid phase, adding calcium oxide (CaO) 1.4 times the weight of a final calcium (Ca) target composition onto a surface of a melt in which the magnesium or the magnesium alloy is melted, forming a targeted amount of Ca in the magnesium or magnesium alloy through a reduction reaction between the melt and the added CaO. Specifically, the amount of Ca formed is in the range of 0.8 wt % to 2.4 wt %, and a final composition of the Mg alloy includes 6.0-8.0 wt % of aluminum (Al), 0.1-0.3 wt % of manganese (Mn), 0.2-0.3 wt % of strontium (Sr), less than 0.04 wt of zinc (Zn), less than 0.9 wt of tin (Sn), and a balance being Mg.
    Type: Application
    Filed: March 18, 2011
    Publication date: September 29, 2011
    Applicant: KOREA INSTITUTE OF INDUSTRIAL TECHNOLOGY
    Inventors: Shae K. KIM, Jung-Ho SEO
  • Publication number: 20110154952
    Abstract: The present disclosure provides a method for making magnesium-based composite material. The method comprises the following steps. Firstly, a semi-solid-state magnesium-based material is provided. Secondly, at least one nanoscale reinforcement is added into the semi-solid-state magnesium-based material to obtain a semi-solid-state mixture. Thirdly, the semi-solid-state mixture is heated to a liquid-state mixture. Fourthly, the liquid-state mixture is ultrasonically processed. Fifthly, the liquid-state mixture is cooled to obtain the magnesium-based composite material.
    Type: Application
    Filed: July 10, 2010
    Publication date: June 30, 2011
    Applicants: TSINGHUA UNIVERSITY, HON HAI PRECISION INDUSTRY CO., LTD.
    Inventors: WEN-ZHEN LI, SHI-YING LIU
  • Publication number: 20110142710
    Abstract: A Ti particle-dispersed magnesium-based composite material is a material having titanium particles uniformly dispersed in a magnesium matrix, and is characterized by having a titanium-aluminum compound layer at an interface between the magnesium alloy matrix and the titanium particles dispersed in the magnesium alloy matrix.
    Type: Application
    Filed: March 16, 2009
    Publication date: June 16, 2011
    Applicant: KURIMOTO LTD.
    Inventors: Katsuyoshi Kondoh, Kantaro Kaneko
  • Patent number: 7651546
    Abstract: The present invention provides a method for manufacturing high-purity hydrogen storage alloy Mg2Ni applicable to industry and capable of manufacturing continuously. First, raw materials of magnesium-nickel with weight percentage of nickel between 23.5 and 50.2 are heated, melt, and mixed uniformly. Cool the magnesium-nickel liquid and control the temperature to be above the solidification temperature and below the liquification temperature in the phase diagram of magnesium-nickel. By making advantage of segregation principle in phase diagrams, solid-state high-purity ?-phase Mg2Ni hydrogen storage alloy is given. Then high-purity ?-phase Mg2Ni hydrogen storage alloy with atomic ratio of 2:1, no other phases, and with excellent hydrogen absorption-desorption dynamics is given.
    Type: Grant
    Filed: October 23, 2007
    Date of Patent: January 26, 2010
    Assignee: Chung Shan Institute of Science and Technology, Armaments Bureau, M.N.D.
    Inventors: Yuan-Pang Wu, Hui-Yun Bor, Rong-Ruey Jeng
  • Patent number: 7156931
    Abstract: The invention relates to magnesium-based alloy and, more specifically, to a magnesium alloy composition and methods of producing the same. The alloy has finer grain size, which results in improving mechanical properties of the alloy. Those mechanical properties make the alloy suitable for high-pressure casting. The alloy comprises aluminium, zinc, manganese, silicon, and calcium. A method for producing said alloy consists of loading the alloying components, pouring the molten magnesium, introducing a titanium-containing fusion cake with a flux agent and continuously agitating. The alloy is then soaked and cast.
    Type: Grant
    Filed: April 22, 2002
    Date of Patent: January 2, 2007
    Assignee: Public Stock Company VSMPO-AVISMA Corporation
    Inventors: Tetyukhin Vladislav Valentinovich, Agalakov Vadim Vladimirovich, Paderina Natalya Sergeevna
  • Patent number: 7135079
    Abstract: The invention relates to magnesium-based alloys and, more specifically, to a magnesium alloy composition and methods of producing the same. The alloys have improved mechanical properties in that creep ratios are decreased. The magnesium-based alloys comprise aluminium, zinc, manganese and silicon. A method for producing said alloy consists of loading the alloying components, pouring the molten magnesium, introducing a titanium-containing fusion cake with a flux agent and continuously agitating. The alloy is then soaked and cast.
    Type: Grant
    Filed: April 22, 2002
    Date of Patent: November 14, 2006
    Assignee: Joint Stock Company “AVISMA-titanium-magnesium works”
    Inventors: Tetyukhin Vladislav Valentinovich, Agalakov Vadim Vladimirovich, Kornaukhova Lyudmila Fedorovna, Puschkarev Sergey Yuryevich
  • Publication number: 20040261576
    Abstract: A method for grain refinement of magnesium alloy castings includes adding graphite (C) powder and manganese dioxide (MnO2) to a melt of magnesium alloy containing aluminum (Al) and manganese (Mn) to finely divide crystal grains of a cast structure.
    Type: Application
    Filed: April 23, 2004
    Publication date: December 30, 2004
    Applicants: Tetsuichi Motegi, Kiyotaka Yoshiwara, Seiko Idea Center Co., Ltd.
    Inventors: Tetsuichi Motegi, Kiyotaka Yoshihara, Tetsuo Kikuchi
  • Publication number: 20040159188
    Abstract: A method for suppressing oxidation and burning in a molten magnesium alloy which my contain beryllium, comprising covering the exposed surface of the molten alloy in a protective atmosphere and dissolving strontium into the molten alloy is disclosed. This has the benefit of reducing magnesium losses due to oxidation thereby improving efficiency of the process. There is also disclosed a magnesium casting alloy comprising from about 1% to 10% by weight of aluminum, from about 1% to 30% by weight of zinc, from about 0.004% to 0.05 % by weight of strontium and unavoidable impurities, the balance being magnesium. Finally, there is disclosed a beryllium free magnesium die casting which is essentially free of flux inclusions.
    Type: Application
    Filed: April 10, 2003
    Publication date: August 19, 2004
    Inventors: Mihriban O. Pekguleryuz, Pierre Vermette
  • Patent number: 6733566
    Abstract: A method for preventing oxidation of molten aluminum alloy and magnesium alloy surfaces, the method comprising providing a molten aluminum alloy or magnesium alloy having a molten aluminum or magnesium alloy surface; covering the molten aluminum or magnesium alloy surface with an initial layer of petroleum coke, the initial layer of petroleum coke having an initial layer thickness of about 0.75 inches; oxidizing a portion of the initial layer of petroleum coke to form a working layer of petroleum coke covering the molten metal surface, the working layer of coke having a working layer thickness of about 0.5 inches, and a layer of carbon dioxide immediately adjacent to and contiguous with the working layer of petroleum coke; and adding additional petroleum coke to the working layer of petroleum coke to maintain the working layer thickness at about 0.5 inches.
    Type: Grant
    Filed: June 9, 2003
    Date of Patent: May 11, 2004
    Assignee: Alcoa Inc.
    Inventors: Que-Tsang Fang, Jen C. Lin, Timothy A. Kuhn, Holger Haddenhorst
  • Patent number: 6652621
    Abstract: A method of manufacturing a material for a magnesium alloy member, characterized in that the method comprises the steps of: heating a solid-liquid coexistent magnesium alloy up to a temperature in the range of from the solidus temperature or more to the liquidus temperature thereof or less; homogeneously dispersing carbon fibers into the solid-liquid coexistent magnesium alloy, wherein the carbon fibers have been cut into arbitrary lengths or powdered and have not been subjected to surface treatment; and then cooling the magnesium alloy.
    Type: Grant
    Filed: November 13, 2001
    Date of Patent: November 25, 2003
    Inventors: Hiroji Oishibashi, Yutaka Matsuda
  • Patent number: 6616729
    Abstract: A method of grain refining cast magnesium alloy includes adding to a magnesium alloy melt containing aluminum and manganese, pure carbon powder, or a carbon source in combination with niobium pentoxide or vanadium pentoxide.
    Type: Grant
    Filed: July 30, 2002
    Date of Patent: September 9, 2003
    Assignees: Seiko Idea Center Co., Ltd.
    Inventors: Tetsuichi Motegi, Kiichi Miyazaki, Yoshitomo Tezuka, Kiyotaka Yoshihara, Eiji Yano
  • Patent number: 6485541
    Abstract: A method to minimize oxidation of metal during melting processes is provided, the method comprising placing solid phase metal into a furnace environ-ment, transforming the solid-phase metal into molten metal phase having a molten metal surface, and creating a barrier between the surface and the environment. Also provided is a method for isolating the surface of molten metal from its environment, the method comprising confining the molten metal to a controlled atmos-phere, and imposing a floating substrate between the surface and the atmosphere.
    Type: Grant
    Filed: August 4, 2000
    Date of Patent: November 26, 2002
    Assignee: The University of Chicago
    Inventors: John N. Hryn, Michael J. Pellin, Wallis F. Calaway, Jr., Jerry F. Moore, Gregory K. Krumdick
  • Patent number: 6197089
    Abstract: The invention relates to activated magnesium metal, to a method of activating magnesium metal and to its use for the preparation of organomagnesium compounds. The activated magnesium metal is obtainable by reacting molten magnesium metal with magnesium hydride; or by heating a mixture of magnesium metal and magnesium hydride until molten.
    Type: Grant
    Filed: February 23, 2000
    Date of Patent: March 6, 2001
    Assignee: Goldschmidt, A.G
    Inventors: Georg Frommeyer, Wilfried Knott, Andreas Weier
  • Patent number: 6132490
    Abstract: A weightening composition for weightening a molten salt in the refinement of magnesium or magnesium alloys, characterized in that it comprises one or more bromide salts, selected from among NaBr, KBr, MgBr.sub.2 or CaBr.sub.2.
    Type: Grant
    Filed: June 11, 1998
    Date of Patent: October 17, 2000
    Assignee: Dead Sea Works Ltd.
    Inventors: Gilad Golub, Gennady Katsnelson, Menachem Zinn, Eliyahu Aghion
  • Patent number: 5536295
    Abstract: An apparatus for the processing of molten metal including a crucible furnace for receiving magnesium scrap and for converting the magnesium scrap into molten metal, a robotic arm positioned so as to extend into the molten metal in the crucible furnace and having a three-axis range of motion. The robotic arm has a connector formed thereon so as to receive a tool. The tool can be a pump which is connected to the robotic arm means so as to transfer the molten metal from the crucible furnace to another location. The pump includes a pump nozzle which is connected to the robotic arm and extends from the robotic arm into the molten metal, an outlet conduit fixedly positioned relative to the crucible furnace, and a pump connected to the pump nozzle and to the outlet conduit. A mixer member is attachable to the connector of the robotic arm to as to extend into the molten metal for the purpose of pushing the magnesium scrap into the molten metal.
    Type: Grant
    Filed: May 15, 1995
    Date of Patent: July 16, 1996
    Assignee: Garfield Alloys, Inc.
    Inventor: Charles M. Slovich
  • Patent number: 5282882
    Abstract: The invention relates to a process for refining crude magnesium, and, in particular, the magnesium obtained by reducing the magnesium ore using iron-silicon.The process consists in treating the liquid magnesium with a metallic sulphide such as iron monosulphide, iron bisulphide or molybdenum bisulphide.The sulphides are contacted with the metallic bath which is agitated to promote the liquid-solid reactions and the formation of insoluble products which precipitate.This contacting is followed by decantation of the insoluble products and their separation from the refined magnesium.The process permits a significant reduction in the contents of calcium and silicon.
    Type: Grant
    Filed: January 21, 1993
    Date of Patent: February 1, 1994
    Assignee: Pechiney Electrometallurgie
    Inventors: Paul-Henri Galvin, Jean-Pierre Bessaguet