Abstract: This invention provides smoking compositions which contains a 6-substituted hexahydrobenzofuranone flavorant additive.Under cigarette smoking conditions the flavorant additive enhances the aroma and flavor of the cigarette smoke.

Abstract: A culture of microorganisms requiring oxygen but capable of living anaerobically while using nitrates and/or nitrites as oxygen source, which are brought to their exponential growth phase under anaerobic conditions, and are made to react under like conditions on the nitrates and/or nitrites, until the nitrates and/or nitrites are reduced to the desired level and the effect of the microorganisms is then stopped.

Abstract: High temperature processes and thermophilic organisms for use in those processes for reducing the levels of certain nitrogen-containing compounds in tobacco materials. Tobacco materials are contacted with at least one thermophilic organism characterized by an anaerobic, dissimilatory, metabolic pathway for denitrification of tobacco materials under anaerobic and high temperature conditions that promote such metabolism. Tobacco materials treated in accordance with these high temperature processes and thermophilic organisms, when incorporated into a smoking product, deliver a significantly reduced amount of oxide of nitrogen in smoke. Moreover, such tobacco materials also afford the product of other tobacco products having lower amounts of nitrates and other nitrogen-containing compounds.

Abstract: Process for the start-up of high-temperature processes for the denitrification of tobacco materials via an anaerobic dissimilatory metabolic pathway of thermophilic organisms. The process advantageously permits the induction of denitrification activity through the use of a seed culture which, itself, is the product of a previous thermophilic denitrification treatment of the same type as that to which the start-up process is directed.

Abstract: An improved method of reducing the nitrate, nitrite and ammonium compound content of an aqueous tobacco extract employing microorganisms is described. The nitrates, nitrites and ammonium compounds are eliminated on a continuous basis via an aerobic assimilatory metabolic pathway by introducing aqueous tobacco extract and necessary additives into a work mixture, containing suitable microorganisms, at a dilution rate which does not exceed the growth rate of the microorganisms while withdrawing a portion of the work mixture at a rate such that the volume of the work mixture remains constant. Optionally the biomass may be removed from the withdrawn mixture.

Abstract: Burley tobacco when cured is sought after as a component of commercial cigarette blends. The inventors have found that, to avoid its less desirable features, one may replace Burley with cured bright tobacco which has been heated in the presence of ammonia at moderate temperature.

Abstract: A process for reducing the content of nitrate and/or nitrite salts contained in tobacco is disclosed whereby tobacco is treated, under controlled aerobic conditions, with microorganisms capable of degrading nitrates and/or nitrites to other nitrogen-containing compounds, such as proteins and amino acids.

Abstract: An improved process for the reduction of the nitrate content of tobacco materials via dissimilatory denitrification is disclosed wherein more rapid reduction of nitrate to nitrogen gas is effected by utilizing a vacuum during incubation. The process comprises inoculating nitrate-containing tobacco material with a microorganism capable of dissimilatory denitrification and thereafter incubating the tobacco material under conditions whereby the nitrate is reduced to nitrogen gas via dissimilatory denitrification while applying a vacuum.

Abstract: A method for producing tobacco flavors which comprises the steps of hydrolytically degrading into amino acids the proteins of biomass produced by the assimilation of low molecular weight nitrogen compounds from an aqueous tobacco extract, isolating the amino acid mixture and converting that mixture into flavors by the use of reducing sugars and heat. The flavors of this invention may be added to smoking products to improve their aroma and taste.

Abstract: Microbial degradation of nitrates in a tobacco extract takes place in a first fermenter under exponential growth conditions of the micro-organisms employed and subsequently in a second fermenter under stationary growth conditions of the degrading micro-organisms. In the first fermenter, carbohydrates are added, while in the second fermenter the depot carbohydrates which the micro-organisms have stored in the first fermenter are utilized.

Abstract: A rod-like smoking article with a rod-like mouthpiece core at the mouth end of a tobacco rod, the entire periphery of the mouthpiece core being enveloped by an adhered wrapping paper which is suitable for contact with the lips and which overlappingly follows a covering paper surrounding the tobacco rod and with secondary air channels covered by the wrapping paper on the periphery of the mouthpiece core and an apparatus for producing such an article.

Abstract: A method and apparatus for steam injection of tobacco bales for use in the opening process. In the apparatus, at least one orificed steam injection plate is brought in flush contact with a tobacco bale that is stationary or in motion and steam is caused to emit from the orifice and is thereby injected into the bale moistening, conditioning and loosening the bonds between the tobacco leaves. In the method, as the tobacco bale is conveyed past the steam injection orifice plate, the plate is moved in flush contact therewith, steam is supplied to the plate and emits therefrom through the orifices to penetrate the tobacco bale. The bale so conditioned is subsequently broken up by a rotating cylinder.

Abstract: This invention provides tobacco compositions which contain a hydroxy-substituted carboxylate compound as a flavorant additive.In one of its embodiments, this invention provides tobacco compositions which contain a hydroxy-substituted alkanoate flavorant additive such as ethyl 2-(2-butyl)-3-hydroxy-3-methyl-3-phenylpropionate: ##STR1## Under smoking conditions the above illustrated hydroxy-substituted alkanoate additive and its pyrolysis products flavor the mainstream and sidestream smoke.

Abstract: A method and apparatus for adjusting the alignment of a beam of radiant energy relative to a structure. A target is placed in the path of the beam, with an opaque reticle disposed in front of the target in the path of the beam in predetermined alignment with the structure. The beam impinges on the target to form a beam image and the reticle casts a shadow within the beam image. The positional relationship between the shadow and the outline of the beam image will be altered by any misalignment between the beam and the structure. The target is preferably chosen so that it will be permanently altered by the radiant energy of the beam, and the positional relationship between the shadow and the outline is preferably observed after exposure of the target to the beam.

Abstract: Smoking article (10) has a filter mouthpiece (14) with a first stage filter element (18) and second stage filter element (19). First stage filter element (18) is rigidly attached to tipping paper (22). Second stage filter element (19) is free to move longitudinally in mouthpiece (14) and may be made to move axially by tapping the cigarette, thus, covering some of the ventilation holes (16) and changing the smoke to air ratio and the flavor.

Abstract: A process for employing tobacco fines in a system for preparing reconstituted tobacco is disclosed. The tobacco fines are incorporated into concentrated extract before the extract is recombined with the reconstituted sheet or into an aqueous carrier. The slurry of fines in extract or other carrier is passed through a homogenizer and then is applied as a coating to the sheet. The further drying and shredding are done in the conventional way.

Abstract: This invention provides a dispensing assembly which is adapted to deliver two separate instantaneously coreactive liquid streams into an external contacting zone. The two reactants do not make contact within the body of the dispensing assembly, which prevents solid product formation and clogging within the dispensing assembly nozzles.The dispensing assembly is suitable for the coreaction of liquid carbon dioxide and liquid ammonia to produce free-flowing ammonium carbamate powder having a purity of substantially 100 percent.

Abstract: A dynamic circumference gage (70) has a spring which maintains contact with moving cigarette rod (74). Strain gages mounted on opposite faces of the spring indicate changes in the circumference of moving cigarette rod (74). Changes in cigarette rod (74) circumference, as indicated by dynamic circumference gage (70), may be used to make adjustments in folder (42) or short tongue (30) to return cigarette rod (74) circumference to within acceptable limits. A second dynamic circumference gage (80) may be located ninety degrees from dynamic circumference gage (70) to provide accurate circumference measurements for out of round cigarettes.

Abstract: A method and apparatus for applying particulate matter to tobacco during the cigarette making process is disclosed. The amount of particulate matter that is lost during the cigarette making process is minimized by applying the particulate matter to the tobacco as it passes through tongue (30), one of the last steps prior to enclosing the tobacco rod in the cigarette paper at folding unit (42).

Abstract: For the preparation of tobacco, the insoluble proteins are initially made soluble by enzymatic treatment, dissolved and then eliminated in the solution by metabolic assimilation. The remaining solution components are then returned to the tobacco.