Patents Represented by Attorney, Agent or Law Firm Charles Q. Buckwalter
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Patent number: 5456729Abstract: The present invention is directed to a sensitizer provided as a foam that may be used individually and/or added to explosives, propellants, and/or pyrotechnics.Type: GrantFiled: April 9, 1992Date of Patent: October 10, 1995Assignee: ICI Canada Inc.Inventors: Fortunato Villamagna, Arun K. Chattopadhyay, Ming C. Lee
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Patent number: 5454889Abstract: The present invention is directed to intimately combining petroleum products with ammonium nitrate prills forming a coating thereon, whereby said coating is tackified and free flowing.Type: GrantFiled: August 19, 1993Date of Patent: October 3, 1995Assignees: ICI Canada Inc., ICI Explosives USA Inc.Inventors: Melvin A. McNicol, Fortunato Villamagna, J. P. Michel Couture
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Patent number: 5454890Abstract: A cap-sensitive emulsion explosive capable of being used in packaged explosive products. The explosive contains ammonium nitrate prills of a bulk density of 0.70 to 1.00 g/cc, with a particle density of 1.25 to 1.40 g/cc. A polysuccinic anhydride based emulsifying agent is used as an emulsifying agent. Packaged explosives prepared according to the present invention have improved package stability, and allow for control of the ratio of shock energy to heave energy.Type: GrantFiled: February 8, 1993Date of Patent: October 3, 1995Assignee: ICI Canada Inc.Inventors: William B. Evans, Anh D. Nguyen
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Patent number: 5449400Abstract: A stable indelible colored ink composition for invalidating bank notes or similar valuables by staining them permanently, comprises at least one of di- or tri-phenylguanidine.Type: GrantFiled: May 3, 1994Date of Patent: September 12, 1995Assignee: Imperial Chemical Industries PLCInventors: Greg Van Lint, Samuel T. Bebbington
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Patent number: 5449424Abstract: Precipitation of fine azide core particles with in-situ coating with suspended tiny oxide particles, followed by concentration of the dilute suspension of these bodies to form a slurry with residual dissolved azide in the liquor, and finally converting the slurry in to solid aggregates of the pyrotechnic bodies by e.g. prilling whereby liquid phase evaporation releases dissolved azide causing the pyrotechnic bodies to be adhered together in to larger aggregates.Type: GrantFiled: September 21, 1993Date of Patent: September 12, 1995Assignees: Imperial Chemical Industries PLC, ICI Canada Inc.Inventors: Raymond Oliver, Ian J. Kirby, Sek K. Chan
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Patent number: 5447090Abstract: The present invention is directed to a delivery system for bulk explosives whereby said system is remotely controlled by electronic or electrical controls.Type: GrantFiled: September 16, 1993Date of Patent: September 5, 1995Assignee: ICI Explosives USA Inc.Inventor: Robert G. Adams
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Patent number: 5435249Abstract: A shock tube initiator comprises a core charge having an oxidizer-rich fuel-oxidizer mixed particle system the mixed particle system containing co-mingled particles of finely comminuted organic dyestuff of the phthalocyanine family or a similarly thermally-stable organic dyestuff in sufficient quantity to impart a distinct color to the charge, the dyestuff being a material which does not decompose below 250.degree. C.Type: GrantFiled: October 20, 1993Date of Patent: July 25, 1995Assignee: Imperial Chemical Industries PLCInventors: Geoffrey F. Brent, Malcolm D. Harding
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Patent number: 5427031Abstract: A detonator for detonation of explosives which provides protection of a primer charge from sympathetic initiation and provides efficient detonation of a base charge. The detonator is comprised of, a hollow detonator shell having first and second ends, said detonator shell has inserted therein a delay element and a primer capsule. Said delay element is positioned within the first end of the shell and has a core running therethrough. The primer capsule has a protective frustrum top having an opening centrally located therein and a tubular bottom. The primer capsule is inserted into the second end of the shell such that the core of the delay element is in contact with the opening in the frustrum top. The primer capsule top contains a primer charge and the bottom contains primer charge and a small amount of base charge material. The top is constructed with heavy walls such that the primer charge is protected.Type: GrantFiled: May 20, 1993Date of Patent: June 27, 1995Assignee: ICI Explosives USA Inc.Inventor: Arthur F. Bowman
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Patent number: 5395559Abstract: A process for the production of explosives grade ammonium nitrate prill (EGAN) comprises the steps of(A). producing seed ammonium nitrate prill as substantially monosized prills; and then(B). fattening using melt/solution of ammonium or mixed nitrates, with drying and thermal treatments, the seed prill in an inclined rotating jacketed pan granulator or a cascade of such pans to produce a final fattened EGAN prill product preferably having at most about 4 mm diameter.Type: GrantFiled: May 5, 1993Date of Patent: March 7, 1995Assignees: Imperial Chemical Industries, PLC, ICI Canada Inc.Inventors: Aida Kaldas, Raymond Oliver
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Patent number: 5354520Abstract: Explosive grade ammonium nitrate (EGAN) prills are made by a process comprising the steps of:a. continuously spraying a 95 to 98% by weight solution/melt of ammonium nitrate (or a mixture of ammonium nitrate and minor proportions of one or more other EGAN--acceptable nitrates) in/with water under spray-head conditions causing the emergent jets to break into cascades of substantially mono-sized droplets;b. allowing the formed droplets to fall within a vertical duct;c. continuously feeding a stream of cooling gas upwards through the duct to effect cooling and solidification of the falling droplets and some removal of moisture so as to form substantially mono-sized EGAN prills of up to about 4 mm diameter, andd.Type: GrantFiled: May 5, 1993Date of Patent: October 11, 1994Assignees: ICI Chemical Industries PLC, ICI Canada Inc.Inventors: Raymond Oliver, Ronald O. Peddie
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Patent number: 5208419Abstract: A method of producing a coloured shock tubing comprising a visibly coloured hollow tube having an inner coating of a reactive material wherein the core loading of the reactive material in the tube may be measured by radiation absorption. The visible colouration of the hollow tube is effected by the addition of a coloured compound, which compound is essentially transparent to the radiation used to measure core loading. A one stage extrusion process may be utilized to prepare a shock tube wherein core loading is easily measured during production, and verified after production.Type: GrantFiled: October 19, 1992Date of Patent: May 4, 1993Assignee: ICI Canada Inc.Inventors: Robert C. Greenhorn, Jacques Lafond
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Patent number: 5204492Abstract: A detonator assembly is provided which increases versatility, reliability and safety by initiating any amount of signal transmission lines up to about 8 without emitting excessive noise or shrapnel which can cause cut off or safety hazards. The detonator assembly comprises a low strength detonator with a single charge of preferably lead azide. A high confinement connection block houses the low strength detonator and comprises a retention block in which the low strength detonator is inserted and a confining wall which surrounds the closed end of the low strength detonator. One to about eight signal transmission lines can be inserted through a gap in the confining wall and operatively confined adjacent the closed end of the low strength detonator.Type: GrantFiled: October 30, 1991Date of Patent: April 20, 1993Assignee: ICI Explosives USA Inc.Inventors: Merritt Jacob, Peter F. Reiss, Samual G. Stednitz
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Patent number: 4915612Abstract: An extrusion die assembly for making honeycomb structures of ceramics, glass, and other extrudable materials. The assembly is provided with an apertured, flow controlling forming plate placed against the input (upstream) surface of the extrusion die. The forming plate has a central opening through which the batch material to the input face of the die passes. A series of angularly spaced, flow controlling openings lies radially outwardly of the rim of this central opening. These forming plate openings are axially aligned with a shim reservoir downstream of the discharge slots of the die. This arrangement permits both the flow volume and rate of the batch material being extruded to the skin forming portions of the die assembly to be at least partially independently controlled relative to the flow volume to the main, radially central portion of the extrudate. By this construction, the formation of air checks in the shim reservoir and the formation of rippled skin on the extrudate is inhibited.Type: GrantFiled: January 26, 1989Date of Patent: April 10, 1990Assignee: Corning IncorporatedInventors: John R. Gangeme, Richard D. Putt
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Patent number: 4912077Abstract: This invention is directed to the preparation of articles exhibiting catalytic activity and, in particular, to articles which are exceptionally suitable for catalytically converting gases from organically fueled power plants, internal combustion engines, and other fluid and gaseous catalysis. The inventive articles comprise a unitary composite structure consisting essentially of a catalytically active precious metal and/or a base metal which, the base metals in particular, become catalytically active upon oxidation. The catalysts are integrally combined with a supporting structural metal.Type: GrantFiled: July 15, 1988Date of Patent: March 27, 1990Assignee: Corning IncorporatedInventors: Irwin M. Lachman, Mallanagouda D. Patil, Jimmie L. Williams, Raja R. Wusirika
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Patent number: 4892857Abstract: An apparatus for use in liquid-phase, gas-phase and mixed-phase reactions is disclosed for providing an efficient flow-through design within which results a low pressure drop. The apparatus may be used as a catalyst or electrocatalyst and consists essentially of a ceramic substrate having thin walls with open porosity wherein said walls define a plurality of cells extending substantially longitudinally parallel through-and-through the substrate. The substrate includes an electrically conductive layer, having a resistivity of no greater than about 100 ohm-cm. The apparatus exhibits an improved structural geometry and provides greater meniscus control.Type: GrantFiled: May 20, 1987Date of Patent: January 9, 1990Assignee: Corning IncorporatedInventors: David L. Tennent, Gerald D. Fong, Christine L. Hoaglin
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Patent number: 4888317Abstract: A structure with encapsulated catalyst-agglomerate bodies which are integral to a porous structure is presented. The catalysts may be singly and/or multiply dispersed on and/or throughout a high surface area material and subsequently mixed with batch material prior to firing the structure. This results in a structure wherein encapsulated catalyst-agglomerate bodies in a porous structure exhibit the same catalytic activity as in a break in aged catalyst coated substrate.Type: GrantFiled: July 15, 1988Date of Patent: December 19, 1989Assignee: Corning IncorporatedInventors: Thomas P. DeAngelis, Irwin M. Lachman, Raja R. Wusirika
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Patent number: 4877766Abstract: A rigid mini-monolith structure formed by extrusion from a die. Such structures are useful as catalyst supports for treating exhaust gases from automobile. The structure is in the shape of a right circular cylinder with a plurality of internal cells extending along the substrate and an opening on both ends. In order to provide maximum crushing strength of the structure, as well as permitting uniform intercell wall thickness at the downstream face of the extrusion die which forms the structure, the majority of the cells are formed in the transverse cross section of a truncated (circular) sector and have the property that they each possess the same hydraulic diameter, although not all are of the same transverse cross sectional shape. The invention also is defined by a novel extrusion die formed by a plurality of concentric, collared tubes provided with longitudinally running slots in the tubes and notches on the collars, the tubes being radially spaced from each other.Type: GrantFiled: July 18, 1988Date of Patent: October 31, 1989Assignee: Corning IncorporatedInventor: Rodney I. Frost
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Patent number: 4876227Abstract: This invention is directed to the production of oxide-boride-silicon nitride ceramics consisting essentially of ceramic bodies of oxide and boride phases which have silicon nitride added to improve the properties of the ceramic body for use as wear material, durable interface material, and cutting tool inserts. The addition of Si.sub.3 N.sub.4 to the oxide-boride body provides a durable ceramic material which provides a range of cutting speeds that may be utilized in both turning and milling operations.Type: GrantFiled: August 24, 1988Date of Patent: October 24, 1989Assignee: Corning IncorporatedInventor: Thomas P. DeAngelis
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Patent number: 4855265Abstract: This invention relates to the high temperature stabilization of aluminum titanate and aluminum titanate-mullite compositions by the addition of iron oxide. It has been found that iron oxide concentrations greater than 5 weight percent and as high as approximately 25 weight percent have a stabilization effect at high temperatures on aluminum titanates. The resultant ceramic body is further enhanced by the addition of from 0.1 to 5 weight percent rare earth oxide.Type: GrantFiled: April 4, 1988Date of Patent: August 8, 1989Assignee: Corning IncorporatedInventors: John P. Day, Robert J. Locker
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Patent number: 4800187Abstract: A method is provided of crystallizing strong-bound zeolites on the surfaces of a monolithic ceramic substrate by hydrothermally treating the substrate, in the presence of active silica, with a caustic bath to zeolitize the silica. According to various embodiments of the invention, the active silica can be present as a component of the caustic bath, in the form of a dried coating pre-deposited on the substrate, or as a separate phase of the monolithic substrate, homogeneous dispersed within the ceramic material.Type: GrantFiled: October 28, 1987Date of Patent: January 24, 1989Assignee: Corning Glass WorksInventors: Irwin M. Lachman, Mallanagouda D. Patil