Abstract: High levels of durable-press appearance rating and conditioned wrinkle recovery angle together with improved abrasion resistance, breaking strength, and tearing strength are the primary textile qualities imparted to cellulosic textile with aqueous solutions containing N-methylolacrylamide-type reagents, a salt of persulfuric acid, and an alkali metal phosphate, which may be supplemented with standard wetting agents and fabric softeners.
Type:
Grant
Filed:
January 31, 1979
Date of Patent:
March 10, 1981
Assignee:
The United States of America as represented by the Secretary of Agriculture
Inventors:
Stanley P. Rowland, Florine A. Blouin, Frederick F. Shih
Abstract: High levels of durable-press appearance rating and conditioned wrinkle recovery angle together with improved abrasion-resistance, breaking strength, and tearing strength are the primary textile qualities imparted to cellulosic textile with aqueous solutions containing N-methylolacrylamide-type reagents, a salt of persulfuric acid, and an alkali metal phosphate, which may be supplemented with standard wetting agents and fabric softeners.
Type:
Grant
Filed:
February 6, 1980
Date of Patent:
March 3, 1981
Assignee:
The United States of America as represented by the Secretary of Agriculture
Inventors:
Stanley P. Rowland, Florine A. Blouin, Frederick F. Shih
Abstract: A plurality of lint cotton quality measurements is made on lint cotton which is to be fed into the lint cleaning process in a cotton ginning system. The plurality of cotton quality measurements in the form of individual electrical signals is communicated to a synchronizing means which translates the quality electrical signals into a single electrical output signal fed into a controller which controls the flow of lint cotton into the lint cleaning apparatus.
Type:
Grant
Filed:
February 23, 1979
Date of Patent:
March 3, 1981
Assignee:
The United States of America, as represented by the Secretary of Agriculture
Abstract: The title compounds, having the formula (RO.sub.2 CNHCH.sub.2).sub.3 PY where Y=oxygen or sulfur, are prepared by reacting a tris(N-carbalkoxylaminomethyl)phosphine, having the formula (RO.sub.2 CNHCH.sub.2).sub.3 P, with an oxidizing or sulfurizing agent. The products, after methylolation with formaldehyde, are useful as finishing agents for imparting flame retardant properties to cotton fabrics.
Type:
Grant
Filed:
November 29, 1978
Date of Patent:
February 3, 1981
Assignee:
The United States of America as represented by the Secretary of Agriculture
Abstract: An apparatus for analyzing volatile components from raw or processed food products using either direct gas chromatography or combined direct gas chromatography and mass spectrometry is disclosed. An inlet assembly containing a sample is appropriately affixed to a means of supplying helium carrier gas. Volatiles are driven off the sample and fed to a condenser assembly where the moisture is removed. The resultant moisture free volatiles are fed to a gas chromatograph or combined direct gas chromatograph and mass spectrograph for analysis.
Type:
Grant
Filed:
February 26, 1979
Date of Patent:
January 20, 1981
Assignee:
The United States of America as represented by the Secretary of Agriculture
Abstract: Novel ternary salts of tris(aminomethyl) phosphines and their oxides having the formula (R.sub.2 NH.sup.+ CH.sub.2).sub.3 P(0).sub.n 3X.sup.-, wherein R is hydrogen, an alkylradical having from 1 to 6 carbon atoms, or an aryl radical n is an integer from 0 to 1, and X is a halogen, are prepared by the reaction of a hydrohalic acid, HX, with various nitrogen- and phosphorus-containing compounds including tris(aminomethyl)phosphines and their oxides, tris(N-carbalkoxylaminomethyl)phosphines oxides, and 1,3,5-triaza-7-phosphaadamantane and its 7-oxide.
Type:
Grant
Filed:
July 26, 1979
Date of Patent:
December 16, 1980
Assignee:
The United States of America as represented by the Secretary of Agriculture
Inventors:
Arlen W. Frank, Donald J. Daigle, Russell M. H. Kullman
Abstract: Novel quaternary ureidomethyl phosphonium salts having the general formula ##STR1## are prepared by condensing a urea having the formula RNHC(O)NR'R" with a quaternary hydroxymethyl phosphonium salt having the formula (HOCH.sub.2).sub.4 P.sup.+ X.sup.- in a molar ratio of at least 2:1. The products, which are characterized by the absence of residual hydroxymethyl groups, are useful as finishing agents for imparting flame retardant properties to cotton fabrics.
Type:
Grant
Filed:
April 6, 1979
Date of Patent:
October 14, 1980
Assignee:
The United States of America as represented by the Secretary of Agriculture