Patents Represented by Attorney, Agent or Law Firm Derek H. Maughan
  • Patent number: 8182965
    Abstract: Lanthanum strontium cobalt iron oxides (La(1-x)SrxCoyFe1-yO3-f; (LSCF) have excellent power density (>500 mW/cm2 at 750° C.). When covered with a metallization layer, LSCF cathodes have demonstrated increased durability and stability. Other modifications, such as the thickening of the cathode, the preparation of the device by utilizing a firing temperature in a designated range, and the use of a pore former paste having designated characteristics and combinations of these features provide a device with enhanced capabilities.
    Type: Grant
    Filed: September 30, 2008
    Date of Patent: May 22, 2012
    Assignee: Battelle Memorial Institute
    Inventors: Jin Yong Kim, Vincent L. Sprenkle, Nathan L. Canfield, Kerry D. Meinhardt, Lawrence A. Chick
  • Patent number: 8088502
    Abstract: A durable coating made up of superimposed microlayers of preselected materials, and a method of making and utilizing such a coating. In one embodiment of the invention, at least 200 microlayers of at least one transparent material, having a thickness of less than 50 nms are superimposed in a sequential manner so as to obtain a desired arrangement between the layers. This structure then forms a transparent coating that has strength characteristics that are substantially greater than the strength of a layer of the coating material alone.
    Type: Grant
    Filed: September 20, 2007
    Date of Patent: January 3, 2012
    Assignee: Battelle Memorial Institute
    Inventors: Peter M. Martin, Charles H. Henager, Jr., Wendy D. Bennett, Ralph E. Williford
  • Patent number: 7966882
    Abstract: A method for determining a velocity and density of a fluid without requiring the transmission of ultrasound through the fluid, and a system for performing such a method. The method involves the steps of delivering, receiving and analyzing ultrasound pulses sent from a longitudinal and a shear wave transducers to a member that is in contact with a fluid. The ultrasound pulses reflecting between surfaces provide a first ultrasound pulse echo series, that is transmitted, received and processed. The shear wave ultrasound pulses are also delivered through a shear wave transducer at a predesignated angle relative to the interface of the member and the fluid and the results of this are received to obtain a second ultrasound pulse echo series. Reflection coefficients for the first and second ultrasound pulse echo series are then calculated and the density of the fluid and the velocity of sound in the fluids are extracted.
    Type: Grant
    Filed: April 23, 2008
    Date of Patent: June 28, 2011
    Assignee: Battelle Memorial Institute
    Inventor: Margaret Stautberg Greenwood
  • Patent number: 7956224
    Abstract: The invention provides palladium-catalyzed hydrogenations of bio-oils and certain organic compounds. Experimental results have shown unexpected and superior results for palladium-catalyzed hydrogenations of organic compounds typically found in bio-oils.
    Type: Grant
    Filed: June 17, 2008
    Date of Patent: June 7, 2011
    Assignee: Battelle Memorial Institute
    Inventors: Douglas C. Elliott, Jianli Hu, Todd R. Hart, Gary G. Neuenschwander
  • Patent number: 7928399
    Abstract: A method for imaging a radiation source, and a device that utilizes these methods that in one embodiment include the steps of: calculating at least one Compton cone of a first parameter of a radiation emission from information received from a sensor occurrence; and tracing this Compton cone on to a unit sphere having preselected characteristics using an estimated angular uncertainty to limit at least a portion of said tracing. In another embodiment of the invention at least two Compton cones are calculated and then intersected upon a predefined surface such as a sphere. These intersection points can then be iterated over a preselected series of prior events.
    Type: Grant
    Filed: December 18, 2007
    Date of Patent: April 19, 2011
    Assignee: Battelle Memorial Institute
    Inventors: Mitchell J. Myjak, Carolyn E. Seifert, Scott J. Morris
  • Patent number: 7926793
    Abstract: Advanced wicking structures and methods utilizing these structures are described. The use of advanced wicking structures can promote rapid mass transfer while maintaining high capillary pressure through the use of small pores. Particularly improved results in fluid contacting processes can be achieved by enhanced mixing within a wicking layer within a microchannel.
    Type: Grant
    Filed: April 25, 2009
    Date of Patent: April 19, 2011
    Assignee: Battelle Memorial Institute
    Inventors: Victoria S. Stenkamp, Ward E. TeGrotenhuis, Robert S. Wegeng
  • Patent number: 7923253
    Abstract: A method and system for classifying subject populations utilizing predictive and diagnostic biomarkers for type I diabetes mellitus. The method including determining the levels of a variety of markers within the serum or plasma of a target organism and correlating this level to general populations as a screen for predisposition or progressive monitoring of disease presence or predisposition.
    Type: Grant
    Filed: November 5, 2008
    Date of Patent: April 12, 2011
    Assignee: Battelle Memorial Institute
    Inventors: Thomas O Metz, Weijun Qian, Jon M. Jacobs, David G. Camp, II, Richard D. Smith
  • Patent number: 7883670
    Abstract: New designs, methods and processes are described that in which laminated devices and configured in a style named the “ortho” style. To form a device in the ortho style, plates or sheets are machined to have apertures and then stacked together such that the apertures connect and fluid can flow through the device in a direction that is substantially parallel to the direction of sheet thickness. Various laminated devices and processes using them are also described. For example, devices in which non-rectangular microchannels conform around reaction chambers or other bodies that need to be heated or cooled, are described. Features that separate or trip boundary layer and enhance heat transfer are also described.
    Type: Grant
    Filed: February 14, 2002
    Date of Patent: February 8, 2011
    Assignee: Battelle Memorial Institute
    Inventors: Anna Lee Tonkovich, Gary Roberts, Sean P. Fitzgerald, Paul W Neagle, Dongming Qiu, Matthew Schmidt
  • Patent number: 7875106
    Abstract: A method device and material for performing adsorption wherein a fluid mixture is passed through a channel in a structured adsorbent bed having a solid adsorbent comprised of adsorbent particles having a general diameter less than 100 um, loaded in a porous support matrix defining at least one straight flow channel. The adsorbent bed is configured to allow passage of a fluid through said channel and diffusion of a target material into said adsorbent under a pressure gradient driving force. The targeted molecular species in the fluid mixture diffuses across the porous support retaining layer, contacts the adsorbent, and adsorbs on the adsorbent, while the remaining species in the fluid mixture flows out of the channel.
    Type: Grant
    Filed: June 10, 2008
    Date of Patent: January 25, 2011
    Assignee: Battelle Memorial Institute
    Inventor: Wei Liu
  • Patent number: 7862633
    Abstract: A system and method for creating reformate with decreased carbon deposition. The system is made up of a steam source, a superheater, a fuel injection device, a prereformer, and a reformer with catalyst linings. The system functions to superheat steam while maintaining the fuel at a lower temperature prior to injection and mixing with the steam. After injection and mixing, the steam and fuel mixture is then passed through a prereformer where catalysts treat a portion of the fuel and steam mixture. After these portions are treated with a catalyst, the mixture is passed through to a reformer where further treatment of the material by catalyst takes place.
    Type: Grant
    Filed: April 13, 2007
    Date of Patent: January 4, 2011
    Assignee: Battelle Memorial Institute
    Inventors: Greg A. Whyatt, Christopher M. Fischer, James D. Davis
  • Patent number: 7799299
    Abstract: Reversible acid-gas binding organic liquid systems that permit separation and capture of one or more of several acid gases from a mixed gas stream, transport of the liquid, release of the acid gases from the ionic liquid and reuse of the liquid to bind more acid gas with significant energy savings compared to current aqueous systems. These systems utilize acid gas capture compounds made up of strong bases and weak acids that form salts when reacted with a selected acid gas, and which release these gases when a preselected triggering event occurs. The various new materials that make up this system can also be included in various other applications such as chemical sensors, chemical reactants, scrubbers, and separators that allow for the specific and separate removal of desired materials from a gas stream such as flue gas.
    Type: Grant
    Filed: January 27, 2009
    Date of Patent: September 21, 2010
    Assignee: Batelle Memorial Institute
    Inventors: David J. Heldebrant, Clement R. Yonker
  • Patent number: 7758846
    Abstract: Methods for producing hydrogen via the water-gas shift reaction utilizing a palladium-zinc on alumina catalyst are described.
    Type: Grant
    Filed: December 16, 2005
    Date of Patent: July 20, 2010
    Assignee: Battelle Memorial Institute
    Inventors: Robert A. Dagle, Yong Wang, Jianli Hu
  • Patent number: 7744751
    Abstract: The present invention provides a process for producing reagents for a chemical reaction by introducing a fuel containing hydrocarbons into a flash distillation process wherein the fuel is separated into a first component having a lower average molecular weight and a second component having a higher average molecular weight. The first component is then reformed to produce synthesis gas wherein the synthesis gas is reacted catalytically to produce the desire reagent.
    Type: Grant
    Filed: September 15, 2008
    Date of Patent: June 29, 2010
    Assignee: Battelle Memorial Institute
    Inventors: Darrell R. Herling, Chris L. Aardahl, Robert T. Rozmiarek, Kenneth G. Rappe, Yong Wang, Jamelyn D. Holladay
  • Patent number: 7718957
    Abstract: A method for multiplexed analysis using ion mobility spectrometer in which the effectiveness and efficiency of the multiplexed method is optimized by automatically adjusting rates of passage of analyte materials through an IMS drift tube during operation of the system. This automatic adjustment is performed by the IMS instrument itself after determining the appropriate levels of adjustment according to the method of the present invention. In one example, the adjustment of the rates of passage for these materials is determined by quantifying the total number of analyte molecules delivered to the ion trap in a preselected period of time, comparing this number to the charge capacity of the ion trap, selecting a gate opening sequence; and implementing the selected gate opening sequence to obtain a preselected rate of analytes within said IMS drift tube.
    Type: Grant
    Filed: June 3, 2008
    Date of Patent: May 18, 2010
    Assignee: Battelle Memorial Institute
    Inventor: Mikhail E. Belov
  • Patent number: 7708955
    Abstract: The invention provides methods and systems for alkylating a paraffinic feed stream in a microchannel utilizing the staged addition of olefin.
    Type: Grant
    Filed: October 9, 2007
    Date of Patent: May 4, 2010
    Assignee: Battelle Memorial Institute
    Inventors: Yong Wang, James F. White
  • Patent number: 7700518
    Abstract: The present invention includes Fischer-Tropsch catalysts, reactions using Fischer-Tropsch catalysts, methods of making Fischer-Tropsch catalysts, processes of hydrogenating carbon monoxide, and fuels made using these processes. The invention provides the ability to hydrogenate carbon monoxide with low contact times, good conversion rates and low methane selectivities. In a preferred method, the catalyst is made using a metal foam support.
    Type: Grant
    Filed: September 20, 2005
    Date of Patent: April 20, 2010
    Assignee: Battelle Memorial Institute
    Inventors: Yong Wang, David P. Vanderwiel, Anna Lee Y. Tonkovich, Yufei Gao, Eddie G. Baker
  • Patent number: 7632320
    Abstract: The present invention is a chemical reactor and method for catalytic chemical reactions having gas phase reactants. The chemical reactor has reactor microchannels for flow of at least one reactant and at least one product, and a catalyst material wherein the at least one reactant contacts the catalyst material and reacts to form the at least one product. The improvement, according to the present invention is: the catalyst material is on a porous material having a porosity that resists bulk flow therethrough and permits molecular diffusion therein. The porous material further has a length, a width and a thickness, the porous material defining at least a portion of one wall of a bulk flow path through which the at least one reactant passes.
    Type: Grant
    Filed: November 18, 2005
    Date of Patent: December 15, 2009
    Assignee: Battelle Memorial Institute
    Inventors: Anna Lee Y. Tonkovich, Yong Wang, Sean P. Fitzgerald, Jennifer L. Marco, Gary L. Roberts, David P. Vanderwiel, Robert S. Wegeng
  • Patent number: 7604781
    Abstract: Multiphasic reactions, especially those reactions using a phase transfer catalyst, are conducted in microchannel apparatus. Advantageously, these reactions can be conducted with two, planar microlayers of reactants in adjacent laminar flow streams. Microchannel apparatus and methods for conducting unit operations such as reactions and separations in microchannel apparatus is also described. Microchannel apparatus can provide advantages for controlling reactions and separating products, solvents or reactants in multiphase reactions.
    Type: Grant
    Filed: July 26, 2006
    Date of Patent: October 20, 2009
    Assignee: Battelle Memorial Institute
    Inventors: John H. Brophy, Bruce F. Monzyk
  • Patent number: 7585899
    Abstract: The present invention includes a catalyst structure and method of making the catalyst structure for Fischer-Tropsch synthesis that both rely upon the catalyst structure having a first porous structure with a first pore surface area and a first pore size of at least about 0.1 ?m, preferably from about 10 ?m to about 300 ?m. A porous interfacial layer with a second pore surface area and a second pore size less than the first pore size is placed upon the first pore surface area. Finally, a Fischer-Tropsch catalyst selected from the group consisting of cobalt, ruthenium, iron and combinations thereof is placed upon the second pore surface area. Further improvement is achieved by using a microchannel reactor wherein the reaction chamber walls define a microchannel with the catalyst structure placed therein through which pass reactants. The walls may separate the reaction chamber from at least one cooling chamber. The present invention also includes a method of Fischer-Tropsch synthesis.
    Type: Grant
    Filed: February 27, 2006
    Date of Patent: September 8, 2009
    Assignee: Battelle Memorial Institute
    Inventors: Yong Wang, David P. Vanderwiel, Anna Lee Y. Tonkovich, Yufei Gao, Eddie G. Baker
  • Patent number: 7585472
    Abstract: The invention describes combustors and steam reformers and methods of combustion and steam reforming. For example, integrated combustion reactors are described in which heat from combustion is transferred to an endothermic reaction. Thermally efficient reactors and methods of alcohol steam reforming are also described. Also described is an integrated combustor/reformer containing a methanation catalyst.
    Type: Grant
    Filed: May 7, 2003
    Date of Patent: September 8, 2009
    Assignee: Battelle Memorial Institute
    Inventors: Jamelyn D. Holladay, Yong Wang, Jianli Hu, Ya-Huei Chin, Robert A. Dagle, Guanguang Xia, Eddie G. Baker, Daniel R. Palo, Max Phelps, Heon Jung