Abstract: An improved method for substantially removing potassium from potassium-bearing molybdenum trioxide involves the use of a leach solution in a weight ratio of seven parts of the leach solution to one part molybdenum trioxide at a temperature of at least 90.degree. C.
Abstract: A zinc sulfide precursor material having axially symmetric platelet-type particles for a copper-activated zinc sulfide electroluminescent phosphor is made by reacting zinc- and copper-containing species with hydrogen sulfide and hydrogen chloride gases in a low-temperature vapor state reaction to obtain copper-containing zinc sulfide particles.
Abstract: Metal phosphide used as a raw material in the synthesis of alkaline earth metal halophosphate phosphor activated by antimony and manganese acts as a reducing agent to prevent oxidation of the antimony and manganese. The result is maximum availability of trivalent antimony and divalent manganese for incorporation into the phosphor lattice.
Abstract: A method of forming a partial protective coating on phosphor particles to improve initial power output and maintenance of fluorescent lamps made with the phosphor. The phosphor particles are fluidized in a bed and at least partially enveloped by a coating precursor material. Residence time of the phosphor particles in the fluidized bed is short so that the phosphor particles are only partially coated with the coating precursor material. The coating precursor material is reacted to form a protective coating over at least a portion of the surface of the phosphor particles. The partially-coated phosphor particles are then annealed to cause the protective coating to selectively cover at least a portion of certain sites on the surface of the phosphor particles.
Type:
Grant
Filed:
September 23, 1992
Date of Patent:
November 2, 1993
Inventors:
Robin W. Munn, Dale E. Benjamin, Deborah V. Lutz
Abstract: A fluorescent lamp including a lamp bulb which has been coated with phosphor powder which has been ground in an attritor to reduce the powder weight without loss in light output and light maintenance. A process to produce such a fluorescent lamp utilizes a particular sequence of steps including firing, milling, attritor milling, and washing to produce an improved stir-in alkaline earth halophosphate.
Abstract: A method of making a threaded tungsten metal part having a diameter or thickness greater than two inches. Tungsten metal powder is hot isostatically pressed and sintered and then machined to the desired thread configuration using a single point tungsten carbide cutting tool.
Abstract: A coated electroluminescent phosphor which can be copper activated zinc sulfide, copper and manganese activated zinc sulfide or copper activated zinc sulfide-selenide is disclosed having a particle size of from less than about 5 micrometers in diameter to about 80 micrometers in diameter. The coating is from about 100 to about 400 angstroms in thickness, and consists essentially of aluminum oxide and is resistant to moisture and relatively chemically inert.
Abstract: In a process for reducing the dust content of cobalt metal powder, the starting cobalt powder containing dust is milled for a sufficient period of time to increase the bulk density and decrease the dust content while substantially maintaining the original Fisher Sub Sieve Size.
Type:
Grant
Filed:
November 20, 1990
Date of Patent:
September 14, 1993
Assignee:
GTE Products Corporation
Inventors:
Robert G. Mendenhall, Michael J. Miller
Abstract: A method of making lead-activated barium silicate phosphor involves the use of a lead source which is not lead oxide. More particularly, the lead source may be lead silicate or lead carbonate-lead hydroxide.
Abstract: A stir-in fluorescent lamp phosphor is coated with a 1:1 ratio of latex polymer and fumed silica. The polymer-coated fluorescent lamp phosphor exhibits improved dispersability and wettability in aqueous and organic binder media which are used to apply fluorescent lamp phosphors to the inside walls of a fluorescent lamp envelope.
Type:
Grant
Filed:
February 11, 1991
Date of Patent:
May 4, 1993
Assignee:
GTE Products Corporation
Inventors:
Robert W. Wolfe, Joseph J. Lenox, Theodore J. Tomlinson
Abstract: The initial power output and maintenance of a fluorescent lamp containing europium-activated barium magnesium silicate phosphor is significantly improved by combining the phosphor with a flux and subjecting the phosphor/flux mixture to a refiring and rewashing process before applying the phosphor to the interior of a fluorescent lamp envelope. Surface concentrations of europium and barium are significantly increased, while surface concentrations of magnesium and silicon are decreased.
Abstract: A method of making extrafine pure elemental metal powder from a highly malleable pure elemental metal powder. The pure elemental metal powder is oxidized, ground to a desired average particle size, reduced in a reducing atmosphere to a pure elemental metal powder, and then sieved to obtain the desired fraction of extrafine pure elemental metal powder.
Type:
Grant
Filed:
December 20, 1991
Date of Patent:
February 9, 1993
Assignee:
GTE Products Corporation
Inventors:
Michael J. Miller, James N. Christini, Eric F. Husted
Abstract: The initial power output and maintenance of a fluorescent lamp containing europium-activated barium magnesium silicate phosphor is significantly improved by combining the phosphor with a flux and subjecting the phosphor/flux mixture to a refiring and rewashing process before applying the phosphor to the interior of a fluorescent lamp envelope. Surface concentrations of europium and barium are significantly increased, while surface concentrations of magnesium and silicon are decreased.
Abstract: A wire plating cell comprises an enclosed housing into which plating solution is pumped at a high velocity so as to create substantial fluid pressure therein. The plating cell contains a plurality of consumable anodes through which a wire passes axially and through which plating solution flows transversely. Current densities of at least 200 amps per square foot are obtained. Use of a highly concentrated plating solution in the cell results in high-speed, high quality wire plating. The invention particularly applies to the plating of nickel onto steel wire at current densities of up to 14,500 amps per square foot.
Type:
Grant
Filed:
November 6, 1989
Date of Patent:
January 5, 1993
Assignee:
GTE Products Corporation
Inventors:
Tom E. Byler, Robert S. Orbanic, Kimberly J. Suchar
Abstract: A method is disclosed for producing an agglomerated molybdenum plasma spray powder with a controlled level of oxygen which comprises forming a relatively uniform mixture of agglomerated powders containing molybdenum dioxide and one or more ammonium-containing compounds of molybdenum wherein the mixture has an oxygen content of greater than about 25% by weight and reducing the mixture in a moving bed furnace at a temperature of from about 700.degree. C. to about 1000.degree. C. for a sufficient time to remove a portion of the oxygen therefrom and form reduced molybdenum powder agglomerates having an oxygen content of no greater than about 25% by weight. The reduction takes place in the direction from the outside surface of the agglometates to the inside surface.
Abstract: A lanthanum cerium terbium gadolinium phosphate phosphor has the composition La.sub.1-x-y-z Ce.sub.x Tb.sub.y Gd.sub.z PO.sub.4, where x=0.2 to 0.45, y=0.127 to 0.137, and z=0.001 to 0.1. The phosphor has improved brightness and/or maintenance over a lanthanum cerium terbium phosphate phosphor without gadolinium. The phosphor can be prepared by reacting a lanthanum cerium terbium gadolinium oxide with boron phosphate in the presence of a flux forming compound containing lithium in an inert or reducing atmosphere.
Abstract: A method for producing pure cobalt metal powder involves the removal of divalent cationic impurities from a trivalent hexamine cobalt chloride solution. This solution is then decomposed to an insoluble cobalt oxide-containing material, from which pure cobalt metal powder is obtained through a chemical reduction process.
Type:
Grant
Filed:
October 28, 1991
Date of Patent:
October 13, 1992
Assignee:
GTE Products Corporation
Inventors:
Michael J. Miller, Thomas A. Wolfe, Michael J. Cheresnowsky, Tai K. Kim
Abstract: A consolidated tungsten alloy body consisting essentially of from about 88% to about 98% by weight of tungsten, balance, nickel and iron, produced by liquid phase sintering, containing a continuous phase of a tungsten, nickel and iron alloy and a discontinuous phase of elongated grains of tungsten having an aspect ratio of at least 4:1 relatively uniformly distributed throughout the continuous phase and wherein said body has a recrystallization temperature of from about 1000.degree. C. to about 1200.degree. C. A process for producing the consolidated bodies comprises working and annealing at controlled temperatures to achieve the desired properties. The working temperatures are from about 700.degree. C. to about 900.degree. C. and the annealing temperature is preferably 1200.degree. C.
Abstract: A method of making a lanthanum cerium terbium phosphate phosphor involves the single-step reaction of single-phase, mixed valence state lanthanum cerium terbium oxide with boron phosphate in the presence of a flux-forming compound containing lithium. The resulting phosphor is up to 5% brighter than the same phosphor prepared without the lithium-containing compound.
Type:
Grant
Filed:
May 14, 1990
Date of Patent:
July 21, 1992
Assignee:
GTE Products Corporation
Inventors:
Chung N. Chau, Anthony F. Kasenga, Charles F. Chenot, Leslie F. Gray