Patents Represented by Attorney Elmer A. Klavetter
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Patent number: 8288001Abstract: A method of making particles of either spherical or cylindrical geometry with a characteristic diameter less than 50 nanometers by mixing at least one structure directing agent dissolved in a solvent with at least one amphiphilic block copolymer dissolved in a solvent to make a solution containing particles, where the particles can be subsequently separated and dispersed in a solvent of choice.Type: GrantFiled: February 16, 2010Date of Patent: October 16, 2012Assignee: Sandia CorporationInventors: Hongyou Fan, Zaicheng Sun
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Patent number: 8230722Abstract: A system is provided for testing the hermeticity of a package, such as a microelectromechanical systems package containing a sealed gas volume, with a sampling device that has the capability to isolate the package and breach the gas seal connected to a pulse valve that can controllably transmit small volumes down to 2 nanoliters to a gas chamber for analysis using gas chromatography/mass spectroscopy diagnostics.Type: GrantFiled: March 16, 2010Date of Patent: July 31, 2012Assignee: Sandia CorporationInventor: Steven M. Thornberg
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Patent number: 8223472Abstract: A capacitor having at least one electrode pair being separated by a dielectric component, with the dielectric component being made of a polymer such as a norbornylene-containing polymer with a dielectric constant greater than 3 and a dissipation factor less than 0.1 where the capacitor has an operating temperature greater than 100° C. and less than 170° C.Type: GrantFiled: November 14, 2008Date of Patent: July 17, 2012Assignee: Sandia CorporationInventors: Shawn M. Dirk, David R. Wheeler
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Patent number: 8201438Abstract: A method of detecting leaks and measuring volumes as well as an apparatus, the Power-free Pump Module (PPM), that is a self-contained leak test and volume measurement apparatus that requires no external sources of electrical power during leak testing or volume measurement, where the invention is a portable, pneumatically-controlled instrument capable of generating a vacuum, calibrating volumes, and performing quantitative leak tests on a closed test system or device, all without the use of alternating current (AC) power. Capabilities include the ability is to provide a modest vacuum (less than 10 Torr), perform a pressure rise leak test, measure the gas's absolute pressure, and perform volume measurements. All operations are performed through a simple rotary control valve which controls pneumatically-operated manifold valves.Type: GrantFiled: April 16, 2009Date of Patent: June 19, 2012Assignee: Sandia CorporationInventors: Steven Thornberg, Jason Brown
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Patent number: 8137802Abstract: A coated carbon-carbon composite material with multiple ceramic layers to provide oxidation protection from ultra-high-temperatures, where if the carbon-carbon composite material is uninhibited with B4C particles, then the first layer on the composite material is selected from ZrB2 and HfB2, onto which is coated a layer of SiC coated and if the carbon-carbon composite material is inhibited with B4C particles, then protection can be achieved with a layer of SiC and a layer of either ZrB2 and HfB2 in any order.Type: GrantFiled: February 5, 2009Date of Patent: March 20, 2012Assignee: Sandia CorporationInventors: Ronald E. Loehman, Erica L. Corral
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Patent number: 8092595Abstract: A method for forming an ordered array of nanocrystals where a hydrophobic precursor solution with a hydrophobic core material in an organic solvent is added to a solution of a surfactant in water, followed by removal of a least a portion of the organic solvent to form a micellar solution of nanocrystals. A precursor co-assembling material, generally water-soluble, that can co-assemble with individual micelles formed in the micellar solution of nanocrystals can be added to this micellar solution under specified reaction conditions (for example, pH conditions) to form an ordered-array mesophase material. For example, basic conditions are used to precipitate an ordered nanocrystal/silica array material in bulk form and acidic conditions are used to form an ordered nanocrystal/silica array material as a thin film.Type: GrantFiled: February 27, 2008Date of Patent: January 10, 2012Assignee: Sandia CorporationInventors: Hongyou Fan, C. Jeffrey Brinker, Gabriel P. Lopez
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Patent number: 8071164Abstract: A method is provided for tribological lubrication of sliding contact surfaces, where two surfaces are in contact and in motion relative to each other, operating in a vapor-phase environment containing at least one alcohol compound at a concentration sufficiently high to provide one monolayer of coverage on at least one of the surfaces, where the alcohol compound continuously reacts at the surface to provide lubrication.Type: GrantFiled: May 7, 2008Date of Patent: December 6, 2011Assignee: Sandia CorporationInventors: Michael T. Dugger, James A. Ohlhausen, David B. Asay, Seong H. Kim
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Patent number: 8003730Abstract: An epoxy resin mixture with at least one epoxy resin of between approximately 60 wt % and 90 wt %, a maleic anhydride of between approximately 1 wt % and approximately 30 wt %, and an imidazole catalyst of less than approximately 2 wt % where the resin mixture is formed from at least one epoxy resin with a 1-30 wt % maleic anhydride compound and an imidazole catalyst at a temperature sufficient to keep the maleic anhydride compound molten, the resin mixture reacting to form a foaming resin which can then be cured at a temperature greater than 50° C. to form an epoxy foam.Type: GrantFiled: December 16, 2008Date of Patent: August 23, 2011Assignee: Sandia CorporationInventor: Mathias C. Celina
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Patent number: 7888397Abstract: A poly(phenylene) compound of copolymers that can be prepared with either random or multiblock structures where a first polymer has a repeat unit with a structure of four sequentially connected phenyl rings with a total of 2 pendant phenyl groups and 4 pendant tolyl groups and the second polymer has a repeat unit with a structure of four sequentially connected phenyl rings with a total of 6 pendant phenyl groups. The second polymer has chemical groups attached to some of the pendant phenyl groups selected from CH3, CH2Br, and CH2N(CH3)3Br groups. When at least one group is CH2N(CH3)3Br, the material functions as an anion exchange membrane.Type: GrantFiled: April 30, 2008Date of Patent: February 15, 2011Assignee: Sandia CorporationInventors: Michael Hibbs, Christopher J. Cornelius, Cy H. Fujimoto
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Patent number: 7880672Abstract: A phase component of a nonlinear frequency modulated (NLFM) chirp radar pulse can be produced by performing digital integration operations over a time interval defined by the pulse width. Each digital integration operation includes applying to a respectively corresponding input parameter value a respectively corresponding number of instances of digital integration.Type: GrantFiled: September 17, 2007Date of Patent: February 1, 2011Assignee: Sandia CorporationInventor: Armin W. Doerry
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Patent number: 7864097Abstract: In radar transponder operation, a variably delayed gating signal is used to gate a received radar pulse and thereby produce a corresponding gated radar pulse for transmission back to the source of the received radar pulse. This compensates for signal distortion due to amplitude modulation on the retransmitted pulse.Type: GrantFiled: January 6, 2009Date of Patent: January 4, 2011Assignee: Sandia CorporationInventors: Richard C. Ormesher, Bertice L. Tise, Robert M. Axline, Jr.
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Patent number: 7767610Abstract: A metal nanocluster composite material for use as a conductive catalyst. The metal nanocluster composite material has metal nanoclusters on a carbon substrate formed within a porous zeolitic material, forming stable metal nanoclusters with a size distribution between 0.6-10 nm and, more particularly, nanoclusters with a size distribution in a range as low as 0.6-0.9 nm.Type: GrantFiled: February 25, 2004Date of Patent: August 3, 2010Assignee: Sandia CorporationInventor: Eric N. Coker
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Patent number: 7741486Abstract: A water soluble, water stable, titanium alkoxide composition represented by the chemical formula (OC6H6N)2Ti(OC6H2(CH2N(CH3)2)3-2,4,6)2 with a theoretical molecular weight of 792.8 and an elemental composition of 63.6% C, 8.1% H, 14.1% N, 8.1% O and 6.0% Ti.Type: GrantFiled: March 18, 2009Date of Patent: June 22, 2010Assignee: Sandia CorporationInventor: Timothy J Boyle
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Patent number: 7591871Abstract: A method for providing a route for the synthesis of a Ge(0) nanometer-sized material from. A Ge(II) precursor is dissolved in a ligand heated to a temperature, generally between approximately 100° C. and 400° C., sufficient to thermally reduce the Ge(II) to Ge(0), where the ligand is a compound that can bond to the surface of the germanium nanomaterials to subsequently prevent agglomeration of the nanomaterials. The ligand encapsulates the surface of the Ge(0) material to prevent agglomeration. The resulting solution is cooled for handling, with the cooling characteristics useful in controlling the size and size distribution of the Ge(0) materials. The characteristics of the Ge(II) precursor determine whether the Ge(0) materials that result will be nanocrystals or nanowires.Type: GrantFiled: February 17, 2005Date of Patent: September 22, 2009Assignee: Sandia CorporationInventors: Henry Gerung, Timothy J. Boyle, Scott D. Bunge
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Patent number: 7567060Abstract: A power management system is provided that includes a power supply means comprising a plurality of power supply strings, a testing means operably connected to said plurality of power supply strings for evaluating performance characteristics of said plurality of power supply strings, and a control means for monitoring power requirements and comprising a switching means for controlling switching of said plurality of power supply strings to said testing means.Type: GrantFiled: June 30, 2005Date of Patent: July 28, 2009Assignee: Sandia CorporationInventors: Stanley Atcitty, Philip C. Symons, Paul C. Butler, Garth P. Corey
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Patent number: 7527671Abstract: A method of making a three-dimensional lattice structure, such as a filter used to remove particulates from a gas stream, where the physical lattice structure is designed utilizing software simulation from pre-defined mass transfer and flow characteristics and the designed lattice structure is fabricated using a free-form fabrication manufacturing technique, where the periodic lattice structure is comprised of individual geometric elements.Type: GrantFiled: November 14, 2006Date of Patent: May 5, 2009Assignee: Sandia CorporationInventors: John N. Stuecker, Joseph Cesarano, III, James E. Miller
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Patent number: 7523582Abstract: A precision laser aiming system comprises a disrupter tool, a reflector, and a laser fixture. The disrupter tool, the reflector and the laser fixture are configurable for iterative alignment and aiming toward an explosive device threat. The invention enables a disrupter to be quickly and accurately set up, aligned, and aimed in order to render safe or to disrupt a target from a standoff position.Type: GrantFiled: August 14, 2007Date of Patent: April 28, 2009Assignee: Sandia CorporationInventors: Brandon R. Ahrens, Steven N. Todd
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Patent number: 7491423Abstract: A method for controllably forming zinc oxide nanostructures on a surface via an organic template, which is formed using a stamp prepared from pre-defined relief structures, inking the stamp with a solution comprising self-assembled monolayer (SAM) molecules, contacting the stamp to the surface, such as Ag sputtered on Si, and immersing the surface with the patterned SAM molecules with a zinc-containing solution with pH control to form zinc oxide nanostructures on the bare Ag surface.Type: GrantFiled: May 1, 2006Date of Patent: February 17, 2009Assignee: Sandia CorporationInventors: Julia Hsu, Jun Liu
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Patent number: 7485343Abstract: A method for preparing a hydrophobic coating by preparing a precursor sol comprising a metal alkoxide, a solvent, a basic catalyst, a fluoroalkyl compound and water, depositing the precursor sol as a film onto a surface, such as a substrate or a pipe, heating, the film and exposing the film to a hydrophobic silane compound to form a hydrophobic coating with a contact angle greater than approximately 150°. The contact angle of the film can be controlled by exposure to ultraviolet radiation to reduce the contact angle and subsequent exposure to a hydrophobic silane compound to increase the contact angle.Type: GrantFiled: April 13, 2005Date of Patent: February 3, 2009Assignee: Sandia CorporationInventors: Eric D. Branson, Pratik B. Shah, Seema Singh, C. Jeffrey Brinker
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Patent number: 7480052Abstract: A method of detecting clouds in a digital image comprising, for an area of the digital image, determining a reflectance value in at least three discrete electromagnetic spectrum bands, computing a first ratio of one reflectance value minus another reflectance value and the same two values added together, computing a second ratio of one reflectance value and another reflectance value, choosing one of the reflectance values, and concluding that an opaque cloud exists in the area if the results of each of the two computing steps and the choosing step fall within three corresponding predetermined ranges.Type: GrantFiled: March 1, 2007Date of Patent: January 20, 2009Assignee: Sandia CorporationInventor: John K. Roskovensky