Patents Represented by Attorney Eugene O. Palazzo
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Patent number: 6455219Abstract: A process for making silica-containing latex particles involves polymerizing monomer in an emulsion comprising the monomer, water, silica particles, and optionally at least one surfactant, by adding at least one free radical initiator to the emulsion to form the silica-containing latex particles. In a preferred method, semicontinuous polymerization employing a seed latex is used to form the latex resin. The process achieves a silica-containing latex in which the silica is chemically incorporated therein that is ideally suited for use in the manufacture of toner and developer for xerographic use.Type: GrantFiled: June 22, 2001Date of Patent: September 24, 2002Assignee: Xerox CorporationInventors: Allan K. Chen, Tie Hwee Ng, Arthur Helbrecht, Kimberly D. Nosella, Danielle C. Boils-Boissier, Paul J. Gerroir, Rosa M. Duque
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Patent number: 6456273Abstract: A bistable flap array display in which flaps selectively cover portions of a background substrate in response to fluid flow and a flap catchment mechanism, each flap rendering at least one pixel of the display. The catchment mechanism can be electrostatically based and the fluid can reduce the charge required to operate the catchment mechanism by creating a partial vacuum that lifts the flaps until the flow can impinge on the flap directly.Type: GrantFiled: December 6, 1999Date of Patent: September 24, 2002Assignee: Xerox CorporationInventors: Roy Want, David Goldberg, Anthony G. LaMarca, Todd A. Cass
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Patent number: 6450712Abstract: A printer control apparatus and an algorithm for determining the peak instantaneous speed of a substrate through a thermal ink jet printer and a printer apparatus are disclosed herein. The printer includes a dryer module, a print head module, and a controller. The method includes determining the tolerable peak instantaneous speeds of the substrate through the print head and dryer modules, which by their sequential nature, operate out of phase from one another. The lower of the two speeds is then selected as the optimum instantaneous speed of the substrate through the printer. A controller in the printer carries out methods disclosed herein.Type: GrantFiled: January 29, 2001Date of Patent: September 17, 2002Assignee: Xerox CorporationInventors: Dinesh S. Shah, Frederick A. Donahue, John F. Moreland, Thomas N. Taylor
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Patent number: 6445490Abstract: A particulate encapsulated Gyricon element includes a Gyricon sphere encapsulated within a shell that also contains a dielectric fluid in which the Gyricon sphere is able to rotate. The shell is preferably formed around the Gyricon sphere and the dielectric fluid by interfacial condensation polymerization. Display elements such as electric paper can be readily derived by coating the encapsulated Gyricon elements upon a substrate. Display elements can thus be readily achieved without the need for an expensive elastomer binder sheet or the need to have the sheet in contact with a dielectric fluid.Type: GrantFiled: November 28, 2000Date of Patent: September 3, 2002Assignee: Xerox CorporationInventors: Naveen Chopra, Peter M. Kazmaier, Karen A. Moffat, Paul J. Gerroir
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Patent number: 6416916Abstract: A toner of toner particles containing at least one binder, at least one color ant, and an external additive package comprised of zinc stearate and at. least one of silicon dioxide or titanium dioxide, wherein the amount of zinc stearate is limited to about 0.10 percent by weight or less of the toner. It has been surprisingly found that when the amount of zinc stearate is so limited, a developer formed from the toner exhibits excellent triboelectric charging and stability and excellent developer flow. When the developer is used in a magnetic brush development system, consistent, high quality copy images are formed substantially without any depletion defects over time.Type: GrantFiled: September 25, 2000Date of Patent: July 9, 2002Assignee: Xerox CorporationInventors: Scott M. Silence, Edward J. Gutman, James M. Proper, Frank O. Reitze, Brian S. Giannetto, Brian E. Moore, Joo T. Chung, James G. Stenzel, Jeffrey L. DeBarr, Morris M. DeYoung, Jr.
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Patent number: 6410196Abstract: A charge transport layer for a photoreceptor includes at least a bisphenol A-phthallic acid dichloride ester copolymer polycarbonate binder and at least one charge transport material. The charge transport layer exhibits excellent wear resistance, excellent electrical performance, and delivers superior print quality.Type: GrantFiled: September 28, 2001Date of Patent: June 25, 2002Assignee: Xerox CorporationInventors: Kathleen M. Carmichael, Stephan V. Drappel, David J. Maty, John A. Bergfjord, Sr.
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Patent number: 6406822Abstract: At least three differently colored toners, designed for use together in forming a color image in an image developing device, have substantially the same melt flow index value. By substantially matching the melt flow index values of at least three toners of a set of toners, it has been found that the resultant color image has an overall excellent image quality, i.e., an excellent overall gloss level without any gloss banding.Type: GrantFiled: September 29, 2000Date of Patent: June 18, 2002Assignee: Xerox CorporationInventors: Scott M. Silence, Joo T. Chung, James M. Proper, Edward J. Gutman, James G. Stenzel, Kip L. Jugle, Yelena Shapiro, James A. Winters, Maria M. Barden, John S. Walters
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Patent number: 6399701Abstract: Submicron sized particles of poly(methyl methacrylate) are prepared by a surfactant-free semi-continuous emulsion polymerization process that involves (i) preparing an aqueous phase containing a free radical initiator in water by heating and stirring, (ii) preparing a monomer composition containing at least 80% by weight methyl methacrylate and 1 to 10% by weight of a crosslinking agent, (iii) adding the monomer composition to the aqueous phase to initiate emulsion polymerization of the monomer composition, the adding being done at a rate such that from 0.05% to 5% by weight of the total weight of the monomer composition is added per minute, (iv) continuing heating and stirring following completion of the adding of the monomer composition for an amount of time, and (v) drying and recovering the submicron sized particles of poly(methyl methacrylate). The submicron sized particles of poly(methyl methacrylate are used in forming a coating of carrier particles for a two-component developer composition.Type: GrantFiled: May 15, 2000Date of Patent: June 4, 2002Assignee: Xerox CorporationInventors: Thomas E. Enright, Anthony James Paine, George Liebermann, Kenneth Derek Henderson, Scott M. Silence, Bernard A. Kelly
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Patent number: 6395445Abstract: A process for forming toner particles includes aggregating the toner particles by adding an aggregating agent to a latex emulsion of resin having a colorant mixed therein, the adding being done under adding conditions of agitation and a temperature above a glass transition temperature of the resin, wherein the adding of the aggregating agent comprises first introducing at least about 40% by weight of a total amount of aggregating agent to be added at a rapid introduction rate and subsequently adding a remaining portion of the aggregating agent at a continuous addition rate slower than the rapid introduction rate. The particles are subsequently cooled to a temperature below the glass transition temperature of the resin when particles have been grown to the desired size.Type: GrantFiled: March 27, 2001Date of Patent: May 28, 2002Assignee: Xerox CorporationInventors: Alan John Toth, Milan Maric, Armin R. Völkel, Marko D. Saban, Thomas Edward Enright
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Patent number: 6392250Abstract: An organic light emitting device includes a mixed region composed of a mixture of a hole transport material, an electron transport material and at least one dopant material. The hole transport material and/or the electron transport material can optionally be an emitter. The materials of the mixed region can be selected to provide various emission colors from the organic light emitting device. The organic light emitting device also includes at least one of a hole transport material region and an electron transport material region on the mixed region. The hole transport material region, the electron transfer material region, and/or the mixed region can be formed with a plurality of layers.Type: GrantFiled: June 30, 2000Date of Patent: May 21, 2002Assignee: Xerox CorporationInventors: Hany M. Aziz, Zoran D. Popovic, Nan-Xing Hu
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Patent number: 6392339Abstract: An organic light emitting device includes a mixed region composed of a mixture of a hole transport material and an electron transport material, one of which is an emitter. The organic light emitting device also includes at least one of a hole transport material region and an electron transport material region on the mixed region. An anode contacts the hole transport material region or the mixed region. A cathode contacts the electron transport material region or the mixed region. The hole transport material region and/or the electron transfer material region can be formed with a plurality of layers.Type: GrantFiled: July 20, 1999Date of Patent: May 21, 2002Assignee: Xerox CorporationInventors: Hany M. Aziz, Zoran D. Popovic, Nan-Xing Hu, Ah-Mee Hor
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Patent number: 6384108Abstract: An ink for ink jet printing includes submicron-sized particles in a liquid vehicle, with the submicron-sized particles including a colorant dispersed in an emulsifiable polymer resin. The polymer resin may contain a base chain, such as polyester, having hydrophilic groups, such as alkali sulfonated groups, for emulsifying the resin in water.Type: GrantFiled: September 29, 1995Date of Patent: May 7, 2002Assignee: Xerox CorporationInventors: Marcel P. Breton, Guerino G. Sacripante, Harvey Bruce Goodbrand, Carol A. Jennings, Susanne Birkel
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Patent number: 6379856Abstract: A toner composition comprised of binder, colorant, and a surface additive of a coated silica and wherein said silica possesses a BET surface area, in m2/g of from about 35 to about 65, a bulk density, in grams/liter, of from about 40 to about 60, and and wherein the size diameter determined from the BET measurement is from about 20 to about 100 nanometers.Type: GrantFiled: February 2, 2001Date of Patent: April 30, 2002Assignee: Xerox CorporationInventors: Jeffrey H. Sokol, Edward J. Gutman
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Patent number: 6376147Abstract: A liquid toner includes a carrier liquid, and toner particles including a thermoplastic resin and a metallic colorant dispersed in said thermoplastic resin, the toner particles being dispersed in the carrier liquid. The liquid toner enables formation of printed images having a metallic sheen using a liquid toner imaging process.Type: GrantFiled: November 27, 2000Date of Patent: April 23, 2002Assignee: Xerox CorporationInventors: Frank J. Bonsignore, George A. Gibson
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Patent number: 6365316Abstract: A toner for particular use in devices utilizing hybrid scavengeless development includes toner particles of at least one binder, at least one colorant, and optionally one or more additives, the toner exhibiting a charge per particle diameter (Q/D) of from −0.1 to −1.0 fC/&mgr;m with a variation during development of from 0 to 0.25 fC/&mgr;m and the distribution is substantially unimodal and possesses a peak width of less than 0.5 fC/&mgr;m, and the toner has a triboelectric charge of from −25 to −70 &mgr;C/g with a variation during development of from 0 to 15 &mgr;C/g following triboelectric contact with carrier particles. Use of a toner with such properties in a hybrid scavengeless development apparatus enables images to be achieved with properties similar to that achieved in offset lithography.Type: GrantFiled: March 7, 2000Date of Patent: April 2, 2002Assignee: Xerox CorporationInventors: Amy L. Stamp, William H. Hollenbaugh, Jr., Susan J. Lafica, Timothy J. Key, Scott M. Silence, Michael J. Duggan, Merrilee A. Galloway, Dennis A. Mattison, Jr., William T. Delelys, Kenneth D. Henderson, Gerardo Leute
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Patent number: 6361915Abstract: A process for manufacturing a conductive micro-powder includes the steps of: (i) forming an aqueous dispersion of conductive material and the first surfactant, (ii) mixing a latex emulsion of a polymer and a second surfactant into the aqueous dispersion to form a suspension and (iii) recovering the conductive micro-powder from the suspension. The first and second surfactants are of the same class and polarity. The conductive micro-powder finds particular utility as a coating for carrier core particles, and as a conductive coating component of carrier particle coatings.Type: GrantFiled: November 28, 2000Date of Patent: March 26, 2002Assignee: Xerox CorporationInventors: John G. Van Dusen, Frederick J. Good, Vladislav Skorokhod, Suresh K. Ahuja, Michael S. Hawkins
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Patent number: 6359105Abstract: Cross-linked toner resin having linear portions and cross-linked portions of high density microgel particles, where the toner resin is an unsaturated polyester resin, is prepared using a liquid chemical initiator such as 1,1-bis(t-butyl peroxy)-3,3,5-trimethylcyclohexane so that the cross-linked resin achieved contains less than 0.20 percent by weight of acids. In particular, the cross-linked toner resin is free of benzoic acid. The method of making the cross-linked toner resin includes (a) spraying the liquid chemical initiator onto the unsaturated polyester resin prior to, during or subsequent to melting of the unsaturated polyester resin to form a polymer melt; and (b) subsequently cross-linking the polymer melt under high shear to form the cross-linked toner resin.Type: GrantFiled: October 26, 2000Date of Patent: March 19, 2002Assignee: Xerox CorporationInventors: John James Ianni, J. Stephen Kittelberger, Daniel Andrew Harrington, Eugene Frederick Young, Hui Chang, Nilmarie Santos-Roman, Dennis J. O'Keefe, Joseph Louis Leonardo, Paul Lynn Jacobs, Kiran B. Sheth, Dongming Li, Louis Joseph Kurtic, Jr., Robert Edward Lutz, Yelena Lipovetskaya
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Patent number: 6358657Abstract: A toner having a high colorant concentration and a binder resin that includes a polyester resin having linear portions and crosslinked portions of high density crosslinked microgel particles has a melt flow index value of about 11±MFI units. The binder resin may also include a mixture of two polyester resins having different MFI values.Type: GrantFiled: August 16, 2001Date of Patent: March 19, 2002Assignee: Xerox CorporationInventors: Scott M. Silence, Joo T. Chung, James M. Proper, John J. Ianni, Jeffrey H. Sokol, Hui Chang
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Patent number: 6355391Abstract: A micro-powder includes: (i) a sub-micron sized powder recovered from a synthetic latex emulsion of polymer and surfactant; (ii) a conductive filler incorporated into the powder; and (iii) optional charge enhancing additives incorporated into the powder. The conductive micro-powder finds particular utility as a coating for carrier core particles of toner and developer compositions.Type: GrantFiled: November 28, 2000Date of Patent: March 12, 2002Assignee: Xerox CorporationInventors: John Gregory Van Dusen, Thomas R. Hoffend, Vladislav Skorokhod, Richard Phillip Nelson Veregin, Deepak R. Maniar, Mary L. McStravick
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Patent number: 6326119Abstract: A method of forming a toner having controlled properties for use in a developer composition finding particular use in a hybrid scavengeless development scheme includes feeding at least one binder and at least one colorant into a mixing device at a feed ratio, upon exit of the mixture from the mixing device, monitoring one or more properties of the mixture with at least one monitoring device, wherein if the monitoring indicates that the one or more properties being monitored is out of specification, removing the monitored mixture from the method and adjusting the feed ratio by adjusting the feeding of the at least one binder or of the at least one colorant, thereby retaining in-specification mixture in the method. The in-specification toner is ground, optionally together with a portion of one or more external additives, classified, and mixed with one or more external additives to obtain the toner having controlled properties.Type: GrantFiled: March 7, 2000Date of Patent: December 4, 2001Assignee: Xerox CorporationInventors: William H. Hollenbaugh, Jr., Hui Chang, Samir Kumar, Scott M. Silence, Amy L. Stamp, Susan J. Lafica, Gerardo Leute, Juan A. Morales-Tirado, Dongming Li