Abstract: The selectivity of ion exchange processes for the removal of lithium from acids is improved when weak acids such as citric and acetic, are used in the wash step. An added improvement is realized by a two stage process of contacting the acid solution first with an ion exchange resin functional to remove the nickel and aluminum compounds from the acid solution; and then contacting the acid solution with an ion exchange resin which is more selective to remove the alkali metal compound from the acid solution.
Abstract: This invention relates to the novel recycle of a slipstream of product gas from the reactor outlet train, the slipstream having been cooled to a lower temperature, back into the outlet head. The recycled cooled gas immediately reduces the temperature of the product gas as the product gas exits the reactor tubes.
Type:
Grant
Filed:
May 21, 1997
Date of Patent:
November 24, 1998
Assignee:
Shell Oil Company
Inventors:
Wayne Errol Evans, Thomas Records Keller, III
Abstract: Problems with pressure in a catalyst bed contained within a vessel arise where there is some sort of blockage in the bed such as a crust formed by a layer of catalyst particles sticking together. To overcome this problem control means is provided to coordinate the flow of nitrogen gas into the vessel and the resulting gas pressure build up and maintenance in the catalyst bed and in the bottom of the vessel as well as in the vapor space of the vessel above the catalyst bed.
Type:
Grant
Filed:
December 27, 1996
Date of Patent:
August 11, 1998
Assignee:
Catalyst Technology
Inventors:
Thomas Peyton Easterly, William Ogle Jones
Abstract: A process for preparing a polymer cement which is relatively free of alkali metal salt by preparing the polymer cement with a polymerization terminating agent which is a diketone which leaves alkali metal salt in the cement which is readily removable by centrifugation.
Abstract: A method for producing an epoxy polyetherpolyol having 15 to 75 wt. % epoxy comprising heating a polyol and catalyst to initiate condensation, removing water, introducing sufficient epoxy into the reaction mixture to give 15 to 75 wt. % epoxy in the product. Generally, between 0.5 and 1.19 moles of water per mole of polyol are removed. In one embodiment at least 95 wt. % of all of the polyol is introduced initially into the reaction zone. In another embodiment the condensation is terminated prior to 93 percent completion. Also provided are novel compositions suitable for drilling fluids, adhesives and coatings.
Type:
Grant
Filed:
June 19, 1996
Date of Patent:
May 26, 1998
Assignee:
Shell Oil Company
Inventors:
George Constantine Blytas, Arthur Herman Hale
Abstract: Reduction of the adhesion of polyethercyclicpolyol (PECP) to metals by preparing the PECP by condensing polyol molecules by reactive distillation and replacing part of the polyol with an alcohol of lower hydroxyl content than the polyol.
Type:
Grant
Filed:
January 28, 1997
Date of Patent:
May 26, 1998
Assignee:
Shell Oil Company
Inventors:
George Constantine Blytas, Arthur Herman Hale
Abstract: Process for removing an alkali metal compound from an acid solution also containing nickel and aluminum compounds, which requires contacting the acid solution first with an ion exchange resin functional to remove the nickel and aluminum compounds from the acid solution; and then contacting the acid solution with an ion exchange resin which is more selective to remove the alkali metal compound from the acid solution.
Abstract: A composition and process for improving the osmotic efficiency of a shale during the drilling of a well with a drilling fluid containing polyglyerol with other additives.