Abstract: A method and devices for the solidification of aqueous substances by the direct evaporation of water from the substance and the sorption of the water vapor in a sorption agent in a vacuum system, wherein the aqueous substance and the sorption agent are evacuated from the surrounding pressure level to a system pressure of below 5 mbar (absolute) by means of a vacuum pump and the nonsorbable gases thereby suctioned by the vacuum pump are suctioned through the sorption agent. The mass of the used sorption agent is at least half the mass of the water fraction in the substance. The solidification process is realized in less than 2 min, particularly less than 20 sec. The aqueous substance is solidified in a solidification container that can be removed from the vacuum system, the vacuum system is subsequently vented, and the solidified substance removed from the vacuum system together with the solidification container.