Abstract: The subject invention provides polyurethane foam and a method of purifying polyether polyols of non-volatile impurities for use in forming the polyurethane foam. The method includes the step of providing a crude polyether polyol having a non-volatile impurity present therein. The crude polyether polyol is contacted with an adsorbent selected from at least one of activated carbon, diatomaceous earth, charcoal, attapulgite, and clay to remove the impurity and filtered to form a purified polyether polyol. The filtering of the crude polyether polyol is carried out through a filter media that is used both in a pre-filtering step prior to adding the adsorbent and the filtering step to remove the adsorbent to reduce losses of the purified polyether polyol because of its high viscosity. The purified polyether polyol is then used to form a polyurethane foam having improved stability.
Type:
Grant
Filed:
March 31, 2004
Date of Patent:
November 8, 2005
Assignee:
BASF Corporation
Inventors:
David D. Peters, Jon S. Speier, Alexander Gershanovich
Abstract: An improved method for synthesizing a double metal cyanide (DMC) catalyst combines and sonicates aqueous and non-aqueous solutions of a first metal salt, such as Zn(OAc)2, of a second metal salt, such as CoCl2, and of an alkali metal cyanide, such as NaCN, to synthesize the DMC catalyst, Zn3[Co(CN)6]2. An improved method of producing a polyether polyol uses the DMC catalyst to produce the polyol.
Type:
Grant
Filed:
May 26, 2004
Date of Patent:
July 26, 2005
Assignee:
BASF Corporation
Inventors:
Edward M. Dexheimer, Jacob Wildeson, Werner Hinz
Abstract: Starting material streams are mixed in a mixer (13) for the phosgenation of amines by a process in which the reaction product (3) is removed in a closed loop and the starting material streams (1.2) contain organic solvents. The main streams (1.1, 2.1) and/or part-streams (1.2, 2.2) of the starting materials (1, 2) come into contact with one another according to the countercurrent principle.
Abstract: In multimetal cyanide complexes, more than 30% by weight of the primary particles have a platelet-like habit, i.e. the length and width of the primary particles is at least three times the thickness of the particles.
Type:
Grant
Filed:
May 29, 2003
Date of Patent:
October 19, 2004
Assignee:
BASF Aktiengesellschaft
Inventors:
Georg Heinrich Grosch, Kathrin Harre, Jörg Erbes, Reinhard Lorenz, Stephan Bauer, Thomas Ostrowski, Eva Baum, Dieter Junge
Abstract: A device for retaining a visored cap upon a wearer's head under high wind conditions includes a strap member and a pair of clamp members that directly engage the strap member and a portion of a visor on a cap. The direct coupling between the strap member and the visor on the cap, which is maintained by the clamp members, is particularly advantageous for maintaining a cap in a desired position on a wearer's head under high wind conditions. The retaining device of this invention also includes an adjustment member that allows a wearer to vary the effective length of the strap member to ensure a snug fit. Each of the clamp members and the adjustment member include a housing having a cavity and an opening formed therein, a pin member slidable in the cavity and having an opening formed therein and a spring to bias the pin member thereby clamping the strap member in the openings.