Abstract: Refractory metal nitrides are synthesized during a combustion process utilizing a solid source of nitrogen. For this purpose, a metal azide is employed. The azide is combusted with a transition metal of the IIIB, IVB group, or a rare earth metal, and ignited to produce the refractory material.
Type:
Grant
Filed:
February 28, 1983
Date of Patent:
May 1, 1984
Assignee:
The United States of America as represented by the United States Department of Energy