Abstract: Disclosed are compositions of particulate citric acid or an alkali metal or alkaline earth metal salt thereof prepared by an improved method and an improved method of preparing a detergent builder composition. The method of preparing particulate citric acid or salts thereof involves spray granulating citric acid or a salt thereof from its partially purified fermentation broth to form granules which are freer flowing and less inclined to fracture than is citric acid or its salts prepared by crystallization techniques which properties render the material prepared by the present method suitable for handling in bulk. The same properties may be imparted to detergent builder compositions by adding detergent builders to the partially purified fermentation broth or by introducing a detergent builder solution into a fluidized bed reactor together with appropriate seed particles to thereby form granules which include such detergent builders.
Type:
Grant
Filed:
May 12, 1992
Date of Patent:
December 7, 1993
Assignee:
Miles Inc.
Inventors:
Helmut A. Mothes, Bhalchandra H. Patwardhan, Theo G. Schroeder, David J. Solow
Abstract: Disclosed is a transparency for use in electrostatographic reproduction, particularly in the multi-color mode of such reproduction. The transparency comprises:A) a base of transparent polyester sheet;B) a second layer adherent to the surface of said polyester sheet of a mixture of an acrylic polymer and a copolymer of vinyl acetate and vinyl chloride said second layer having uniformly dispersed therein:I. particulate silica having a particle size range of from about 2 to 70 millimicrons in its longest dimension and being present in an amount of from about 0.25 to 1.5 weight percent of said second layer, andIi. a salt formed from an anion of a carboxylic acid having 1 to 37 carbon atoms or a dimeric fatty acid having 12 to 36 carbon atoms and a cation characterized by the formula: ##STR1## wherein R.sub.