Abstract: A method for fabricating a homogenous and uniformly sized mixture of alkaline earth metal carbonates found to be especially useful as an emission type coating material for application to a cathodic element of a thermionic vacuum tube.
Abstract: A method for treating hydrazine-fuel contaminated wastewater in which hydrazine, monomethyl hydrazine, unsymmetrical dimethyl hydrazine and dimethylnitrosamine pollutants are effectively decomposed at a controlled pH of about 5 by an ultraviolet induced chlorination treatment of the wastewater.
Type:
Grant
Filed:
December 1, 1982
Date of Patent:
September 6, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Inventors:
Edward G. Fochtman, Roger L. Koch, Forrest S. Forbes
Abstract: A method for delineating defects in the <111> surface of an indium antimonide crystal wafer by treating said surface with a 5 percent solution of iodine in N,N-dimethylacetamide to form triangularly shaped etch pits in the defect area.
Type:
Grant
Filed:
September 16, 1982
Date of Patent:
August 2, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: A high char yielding matrix resin for use in fabricating carbon-carbon composites comprised of a polymerizable mixture of a diethynylbenzene monomer and an ethynylpyrene monomer.
Type:
Grant
Filed:
June 11, 1982
Date of Patent:
July 12, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: A technique for monitoring the ablation symmetry of a reentry vehicle by implanting a boundary layer trip material into the nose-tip surfaces of the re-entry vehicle's nose cone. The implantation material is characterized by a density that is usually greater and surface roughness that is greater than that which characterizes the material forming the main portion of the nose cone.
Type:
Grant
Filed:
February 6, 1981
Date of Patent:
July 12, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: A method for polymerizing octafluoronaphthalene and the resulting perfluorocompounds prepared therefrom. Polymerization is accomplished by reacting the octafluoronaphthalene monomer with a mono or difluoroxyperfluoroalkane.
Type:
Grant
Filed:
September 30, 1981
Date of Patent:
July 12, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: This invention concerns itself with the addition of certain copper salts and chelates to solid propellant formulations as burning rate modifiers. The additives increase the burning rate of the propellant while simultaneously decreasing its pressure exponent.
Type:
Grant
Filed:
September 10, 1981
Date of Patent:
July 5, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Inventors:
Robert C. Corley, Frederick F. Myers, Jr.
Abstract: A solvent solution for dissolving and removing cured polyurethane formulations composed of a mixture of dichloromethane, dimethyl formamide and methanol as essential components.
Type:
Grant
Filed:
June 30, 1981
Date of Patent:
May 17, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: A polymeric composition comprised of a mixture of an acetylene-terminated polymer and an hydroxy-substituted, polynuclear, aromatic derivative as a cure retarding additive.
Type:
Grant
Filed:
September 10, 1981
Date of Patent:
April 26, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: New, easily processable, polyaromatic esters were prepared from 2,2'-diiododiphenyl-4,4'-dicarbonyl dichloride, isophthaloyl chloride and/or terephthaloyl chloride in combination with 4,4'-isopropylidene diphenol, 4,4'-sulfonyldiphenol, or resorcinol by interfacial condensation. In these polymers, phenylacetylenyl groups can be easily introduced into the polymer chain by replacing the iodine. This process leads to soluble and curable polymers from which films can be prepared. After curing the polymers are insoluble and show excellent thermal and chemical resistance. The curing process increases the polymers' softening temperature about 20.degree. C.
Type:
Grant
Filed:
March 3, 1981
Date of Patent:
April 26, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: A novel method is taught for preparing polymeric alloys composed of a mixture of an aromatic heterocyclic rod-like reinforcing polymer and an aromatic heterocyclic coil-like amorphous mixture with vastly improved mechanical properties.
Type:
Grant
Filed:
August 11, 1981
Date of Patent:
March 22, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Inventors:
Thaddeus E. Helminiak, Charles L. Benner, Fred E. Arnold, George Husman
Abstract: A method for preparing a stable sodium carbonate micro dispersion in hexane by subjecting a starting material composed of a colloidal sodium carbonate dispersion in oil to the steps of flocculation, redispersion, centrifugation and vacuum distillation.
Type:
Grant
Filed:
July 18, 1974
Date of Patent:
March 15, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: An improved method for synthesizing poly (carbonyl fluoride) oligomers by using bis(trifluoromethyl)trioxide as a reaction initiator in the photo-oxidation of F-3 methylbutene-1.
Type:
Grant
Filed:
June 17, 1981
Date of Patent:
February 22, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: A high char yielding matrix resin for use in fabricating carbon-carbon composites comprised of a polymerizable mixture of a diethynylbenzene monomer and an ethynylpyrene monomer.
Type:
Grant
Filed:
September 30, 1981
Date of Patent:
January 18, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: New processable polyaromatic amides were prepared from the acid chloride of bis-m-carboxyphenyl acetylene and several aromatic diamines. The polyamides containing the acetylene units were cured by Diels-Alder cycloaddition reaction with 1,4-diphenyl-1,3-butadiene. Cured polyamides showed increase in Tg. thermal and heat stabilities. The polyamides can be cast into films and give good glass fiber laminates.
Type:
Grant
Filed:
May 20, 1981
Date of Patent:
January 4, 1983
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: A composition of matter comprising an acetylene-terminated polyimide oligomer and a cure rate inhibitor selected from the group consisting of hydroquinone, maleic acid, glutaric acid, dibetanapthyl para-phenylene diamine. The composition has a retarded cure rate, thereby facilitating the fabrication of void-free molded objects and composites.
Type:
Grant
Filed:
September 21, 1981
Date of Patent:
December 21, 1982
Assignee:
The United States of America as represented by the Secretary of the Air Force
Inventors:
Mark F. Grimes, Theodore J. Reinhart, Jr.
Abstract: A solvent for dissolving and removing polysulfide and polysilicone rubber coatings from a metal substrate. The solvent is composed of a mixture of dichloromethane and a minor amount of a chlorotrimethylsilane.
Type:
Grant
Filed:
October 13, 1981
Date of Patent:
December 7, 1982
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: A process for synthesizing novel polyaromatic amides containing 1,3-butadiene groups along the polymer chain by effecting a reaction between the acid chloride of 1,4-bis-p-carboxyphenyl-1,3-butadiene and an aromatic diamine. These polyamides have been found to be especially useful as laminating resins for a variety of laminating applications.
Type:
Grant
Filed:
May 20, 1981
Date of Patent:
November 16, 1982
Assignee:
The United States of America as represented by the Secretary of the Air Force
Abstract: A method for fabricating a homogenous and uniformily sized mixture of alkaline earth metal carbonates found to be especially useful as an emission type coating material for application to a cathodic element of a thermionic vacuum tube.
Abstract: A color-coded taggant for the post-detonation identification of explosive material. Retrieval of the taggnt after detonation of an explosive is facilitated by the addition of nickel formate to the taggant. The additive renders the taggant magnetically susceptible only after detonation. This eliminates the possiblity of the unauthorized removal of the taggant by a magnet before detonation but retains the advantages of facile retrieval by means of a magnet subsequent to detonation.
Type:
Grant
Filed:
August 27, 1980
Date of Patent:
November 16, 1982
Assignee:
The United States of America as represented by the Secretary of the Air Force