Abstract: A process is provided for the preparation of a compound having the structure of Formula I
The process includes reacting a heterocyclic amine with a monoaldehyde or a dialdehyde in a pH range of from about 8 to 14 and then quaternizing the so-reacted heterocyclic amine with an alkylating agent at a pH of not less than about 2. The use of pH control substantially prevents formation of an undesirable protonated reaction intermediate.
Type:
Grant
Filed:
November 19, 1999
Date of Patent:
May 22, 2001
Assignee:
The Clorox Company
Inventors:
Ulrich Annen, James E. Deline, Lafayette D. Foland, Kevin A. Klotter, Josef Müller, Michael Müller, Klaus Mundinger, Martin A. Phillippi, Alfred Ruland, Wolfgang Schäfer, Gregor Schürmann, Rudi Widder, Alfred G. Zielske