Abstract: Hydrocarbon oils such as diesel fuels, turbine fuels and intermediate distillates may be subjected to quantitative analysis of their saturate, aromatic and polar components by supercritical fluid chromatography using carbon dioxide as the solvent. A sample of the oil is passed into a packed column of silica or the like whereby the respective fractions are separated and retained on the column. Supercritical carbon dioxide at selected pressure and temperature conditions is passed through the column to extract, separately, each of the fractions retained on the column. The extracted fraction and solvent are passed through a restrictor and expanded down to a pressure which will allow the solvent to evaporate and to permit retention or collection of the extracted fraction in a collector arrangement including a selector valve and plural collection containers.

Abstract: A combination scratcher-centralizer for use in installing casing in wellbores comprising a single piece of coiled wire or rod having a first hub part for tightly engaging the casing, a radially expanded centralizer and scratcher portion forming a helical wrap of said wire and a second hub part slidable on the casing and formed by a helical wrap of said wire. The first hub part includes serrations and/or a plurality of retaining screws provided so that the first hub part may be secured to the casing in a predetermined position to allow the expanded centralizer coil or wrap portion to undergo some elastic axial excursion during its scratching and scraping operation upon installation in a wellbore. The constricted hub part may be held in a radially expanded position during installation by a retainer engageable with spaced apart portions of the wraps of the hub part.

Abstract: An auger gravel pack assembly for installation in a gravel packed well includes a fluid loss control closure member retained in a body disposed in a tubing assembly or "work string" between the gravel pack screen and a running tool and cup-packer assembly. A ball-type closure member is retained by releasable fingers connected to a piston which is responsive to fluid pressure applied through the work string to effect release of the closure ball to engage a seat and substantially prevent flow of fluid from the work string or the wellbore annulus into and through the gravel pack screen after installation of the screen into the gravel pack. Ports in the assembly above the closure member allow fluid to flow between the wellbore annulus and the work string to prevent pressure buildup between the gravel pack and the cup-packer during installation of the screen.

Abstract: Perforation tunnels and other voids or spaces in earth formations in communication with wells are sealed more effectively by injecting and pre-packing resin-coated particulates (sand) into such tunnels or voids and allowing the sand to consolidate to form a substantially rigid, permeable mass. A lead slurry of relatively fine grained cement is then injected to fill the interstices formed in the permeable material occupying the tunnels or voids. A larger or more coarse grain cement is then injected to form a substantially impermeable, rigid filter cake at the interface of the wellbore and the permeable mass to prevent loss of cement slurry out of the tunnels or voids before the cement is set. Vertical and deviated or generally horizontal wellbores having perforation tunnels or voids which suffer unwanted cement drainage prior to setting of conventional oil well cements are more effectively sealed by the sequential injection of the permeable material followed by injection of settable cement slurries.

Abstract: Oil pollution floating on a body of water is abated or contained by a fire fence generated by a series of devices which are interconnected by cables and anchored to form a barrier line. Each device comprises a buoy connected to a depending, negatively-buoyant tank of pressurized combustion gas and a burner nozzle disposed for providing a pilot flame near the water's surface to ignite an oil slick thereon. The pilot flame Way be controlled to sustain combustion of the floating oil and dissipation of same.

Abstract: A gravel pack screen assembly includes a bit or sub having a flow passage which may accept a wash pipe. The wash pipe may be inserted past a flapper-type closure member which moves to a closed position upon withdrawal of the wash pipe after completion of the installation of the gravel pack assembly. The closure member can be formed of a porous material to permit the flow of liquid through the bit or sub flow passage into the interior of the gravel pack screen but to prevent flow of gravel packing or produced sand into the interior of the screen. The closure member may serve as a backup to a conventional one-way valve and permit additional gravel pack material to be placed in the flow passage upon completion of the gravel pack installation and in the event of early or late failure of the one-way valve.

Abstract: An auger gravel pack screen or other wellbore device is driven by a workstring which includes a torque-limiting device interposed therein to limit the maximum torque exerted on the screen during augering into a gravel packing in a well bore. The torque-limiting device includes driving and driven mandrels with removable shear pin support parts connected to the mandrels, respectively, and supporting plural shear pins through which driving torque is exerted on the device. An alternate embodiment includes a slip clutch with cooperating lobed clutch members. An axially translatable nut is disposed in a fluid-filled chamber between the mandrels and is operable to permit controlled rotation of the mandrels relative to each other when the limit torque is exceeded to absorb torsional deflection energy built up in the workstring without damaging the workstring or the gravel pack screen.

Abstract: Surface mined lands are reseeded by dispensing grass, forb and shrub seed from a seed drill with seed-dispensing boxes connected to plural dispensing tubes which drop seed on the earth's surface and wherein at least one seed box is operable to dispense cool season grass seed through conventional opener assemblies into furrows formed thereby. An English tine harrow drag is pulled behind the seed drill to cover and distribute seed to provide improved species diversity and desired shrub density on the seeded area. Fine seed shrubs are broadcast by the drill during traversal of the seeded area in a direction generally perpendicular to the first seeding operation. Companion crops of annual grain are seeded with native grass, forb and shrub seed and mowed prior to seedhead maturity to prevent reseeding and to provide cover and protection for native seedlings. Improved species diversity, shrub density and overall revegetation success is provided for semi-arid lands, in particular.

Abstract: Slug flow is substantially prevented in cylindrical pipes and other conduits by placing a generally flat plate partition extending within the pipe and dividing the pipe into a gas flow space and a liquid flow space. The position of the partition and the cross-sectional flow areas of the gas flow space and the liquid flow space are determined by predetermining that the pressure losses of gas flow and liquid flow should be substantially equal.

Abstract: A sand control screen is installed in a well by interposing the screen in a drillstring having a retrievable bit and drive motor. The screen is drilled into place with the distal end of the drillstring and remains in the wellbore. The drillstring may be disconnected from a bottom hole assembly comprising the screen and the distal end of the drillstring and replaced by a tubing string having a packer or other external seal member interposed therein for sealing one portion of the wellbore from another. The sand control screen has a basepipe with plural apertures temporarily closed plugs which are threadedly or force-fit in the apertures. The plugs may be formed of a meltable or dissolvable fiber reinforced wax, for example, or an active metal which may be dissolved by an acid or caustic solution. The screen may also include a temporary plugging medium such as wax in the interstices of the screen sleeve to prevent accumulation of drilling fluid solids during insertion in the wellbore.

Abstract: Formaldehyde and similar biocides are transported in a gelled, semi-solid or solid state by providing formaldehyde in a concentration in methanol of about fifty-five percent (55%) to eighty-five percent (85%) by weight, loading the solution in rail cars or truck transport tanks in a liquid state and cooling the solution to a gelled, semi-solid or solid state for transport to a destination followed by reheating the solution and/or mixing with a solvent for discharge to an application such as the produced water flowstreams from Alaskan North Slope oil fields, for example.

Abstract: An acoustic wave generator for telemetering signals through a drillstem comprises a sub interposed in the drillstem with a central mandrel and a piston mass disposed in sleeved relationship around the mandrel and reciprocable by hydraulic pressure fluid to impose reaction forces on the mandrel and the drillstring at selected frequencies to transmit acoustic waves through the drillstring. A control system for operating the generator includes a hydraulic pump, a control valve and a frequency control circuit which operates the control valve to effect reciprocation of the piston mass at selected frequencies for transmitting serial data from the control system through the drillstring to a receiving system. The generator is coaxially arranged in the drillstring and is operable to generate high-energy acoustic wave signals for propagation through relatively long drillstrings.

Abstract: Lateral vibrations of drillstring bottom hole assemblies are confirmed by sensing longitudinal and torsional accelerations or displacements of the drillstring at or near its top end during rotation and determining the lateral critical speed and displacement of the drillstring from the mode shape of the bottom hole assembly which occurs during forward synchronous whirl and longitudinal shortening of the bottom hole assembly resulting from such whirl. Lateral motion of the bottom hole assembly, while drilling, is estimated based on longitudinal and torsional measurements at the top of the drillstring. Radial displacement of the bottom hole assembly due to impacting of the borehole wall imparts a torsional impulse which, together with considerable radial motion, is repeated each revolution. The lateral or radial motion causes a small axial motion to develop in the bottom hole assembly which results in an axial force on and axial shortening of the drillstring which varies once per revolution.

Abstract: Slurries of relatively fine particles of solids wastes and similar materials are disposed of through injection wells which penetrate earth formation disposal zones which have a minimum in situ compressive stress generally less than an overburden zone and an underburden zone adjacent to the disposal zone. The disposal zone preferably has a permeability greater than the overburden and underburden zones. The slurry is injected through a disposal well intersecting all of the zones and having perforations preferably communicating the slurry with the underburden zone to provide for lateral growth of the hydraulically fractured disposal zone as the solids filter cake plates out on the fracture faces of the disposal zone without substantially penetrating the overburden zone.

Abstract: Drill cuttings and similar earth materials are reduced in particle size, slurried and disposed of from a system which includes a ball mill, a reduced particle receiving tank, a grinder pump in communication with the receiving tank and separator screens for receiving a slurry of particles which have been reduced in size through the ball mill and the grinder pump. The underflow of the separator is suitable for discharge for final disposal, oversized particles are returned to the ball mill and the underflow discharged from the separator is controlled to maintain a certain level in the primary receiving tank. A secondary tank may receive a portion of the underflow to be mixed with viscosifiers and dispersants to maintain a suitable slurry composition for discharge. The system may be mounted on a semi-trailer and in weather-proof enclosures with the ball mill, receiving tanks and grinder pump on a first level and the separators on a second level.

Abstract: Aged and/or colored diesel fuels and similar petroleum distillates may be analyzed for the presence of an anthraquinone marker dye such as DuPont Chemicals Oil Blue B Liquid dye by passing a sample of the fuel through an unbonded silica solid phase extraction column which retains the color-forming agents on the column and which will provide for visual detection of the substantially nonretained marker dye in the column. A sufficiently nonpolar elution solvent such as dichloromethane or toluene may be passed through the column to elute the marker dye without removing the color-forming agents from the column. The solvent may be spectrophotometrically analyzed to detect presence of the dye.

Abstract: Offshore well slots are recovered by cutting off old drive or surface pipe below the mud line to form a stub end. A new drivepipe is installed with a guide and shield device disposed on the scarfed lower end or "mule shoe" of the new drivepipe. The guide and shield device includes a saddle contiguous with the lower end of the new drivepipe having one or more hooks formed on the outer surface thereof for engagement with the stub end to locate the device and the new drivepipe. Shear pins interconnect the new drivepipe with the device and are sheared in response to downward driving action on the new drivepipe or allowing the full weight of the drivepipe to be exerted on the shield device after engagement with the old drivepipe.

Abstract: A tubing conveyed straddle packer system includes two inflatable packers interconnected with each other and spaced apart to provide for isolating a wellbore space for communicating pressure fluids between a formation zone of interest and the surface through the tubing string. An electrical cable extends within the tubing string and is operable to provide control signals to electrically controlled valves for inflation and deflation of the packers and for conveying fluids between the formation zone of interest and the tubing string and between the tubing string and the wellbore above and below the straddle packer system. A logging tool is interposed in the tubing string for precisely locating the straddle packer system in the well.

Abstract: An oil recovery and storage ship having a general tank configuration of a conventional crude oil carrier is modified by providing inlet doors along opposite sides of the ship and a deployable floating boom arrangement for maximizing the floating oil gathering swath. The side inlet doors open into sluice or sea-calming compartments which have adjustable weir doors opening into primary separation tanks on port and starboard sides. Adjustable weir doors open from the primary separation tanks into a secondary separation tank. A selected number of cargo tanks are interconnected by conduits which permit the flow of liquid from one tank to the next in a series or cascade manner to decant oil from oily water and to discharge substantially oil-free water overboard from the last tank in the cascade. The ship may be used as a conventional liquids carrier when not required for oil spill recovery operations.

Abstract: Sand control screens temporarily plugged with paraffin wax are installed in deep open hole wells wherein the wax has a melting temperature slightly greater or less than the nominal formation temperature in the zone from which well fluids are to be produced. Drilling fluids and other solids-laden wellbore fluids are removed from the wellbore by flowing the well up through a section of tubing disposed distal of the screen, through the interior of the screen and through the tubing string to the surface until the wellbore is cleaned. The wax is then melted due to the temperature of the produced fluid, is dissolved by the produced fluid or a solvent pumped down through the tubing string or is heated by a heater inserted into the interior of the screen such as a wireline conveyed electric heater. The distal tubing section is plugged so that production fluids are forced to flow through the sand control screen in a conventional manner.