Abstract: An improved process that is commercially practical for forming an oxide film cobalt conversion coating exhibiting corrosion resistance and paint adhesion properties on a substrate, where the substrate is aluminum or aluminum alloy, the process including the steps of: (a) providing an oxide film forming cobalt conversion solution comprising an aqueous reaction solution, containing no triethanolamine (TEA), prepared by reacting the following starting materials: (1) a water soluble cobalt-II salt CoX2 where X=Cl, Br, NO3, CN, SCN, ⅓PO4, ½SO4, ½CO3, formate, or acetate; (2) a water soluble complexing agent selected from the group consisting of MeNO2, MeAc, MeFm, NH4Ac, and NH4Fm where Me is Na, K, or Li; Ac is acetate; and Fm is formate; (3) an accelerator selected from the group consisting of NaClO3, NaBrO3, and NaIO3; (4) water; and (b) contacting the substrate with the aqueous reaction solution for a sufficient amount of time to oxidize the surface of the substrate, whereby the oxid

Abstract: A process for sealing the surface coating formed by anodizing an aluminum or aluminum alloy substrate (for example, aerospace, commercial, and architectural products), the process including the steps of: (a) providing an aluminum or aluminum alloy substrate with a surface coating formed thereon by anodizing the aluminum or aluminum alloy substrate; (b) providing a sealing solution comprising a dilute solution of a rare earth metal salt selected from the group consisting of cerium salts and yttrium salts; and (c) contacting the substrate with the sealing solution for a sufficient amount of time to seal the surface coating on the substrate. Also disclosed is a chemical sealing solution for sealing the surface coating formed by anodizing an aluminum or aluminum alloy substrate, the solution being a dilute solution of a rare earth metal salt selected from the group consisting of cerium salts and yttrium salts.

Abstract: An improved alkaline cleaning solution that has the ability to descale, derust, and completely dissolve machining lubricants coated on steel and other iron alloy objects, the alkaline cleaning solution consisting essentially of: (a) water; (b) about 10% to 95% by volume of a water-soluble descaling and derusting agent; and (c) about 2% to 8% by weight of a water-soluble sequestering agent selected from the group consisting of sodium gluconate and its functional equivalents.

Abstract: A process for making a layered product having a honeycomb core having cells filled with a foam material, the process comprising the steps of: (a) placing a first layer of an uncured, heat-expandable, foamable material on the top side of a central honeycomb core having empty cells, and placing a second layer of an uncured, heat-expandable, foamable material on the bottom side of the central honeycomb core; (b) placing a first layer of an uncured preform material above the first layer of uncured, heat-expandable, foamable material, and placing a second layer of an uncured preform material above the second layer of uncured, heat-expandable, foamable material; (c) placing the charge made by steps (a) and (b) inside a mold and closing the mold; (d) heating the mold to the cure temperature of the heat-expandable, foamable material, and holding the mold at this temperature for sufficient time to expand and cure the heat-expandable, foamable material; (e) reducing the temperature of the mold to the injection temperat

Abstract: An improved method of anodizing an aluminum or aluminum alloy workpiece including the steps of: (a) providing an aqueous anodizing bath consisting essentially by weight of about 3 to 5 percent sulfuric acid, from about 0.5 to 1 percent boric acid, not more than about 5.0 g/L aluminum ion, not more than about 0.2 percent chloride ion, and a fungistat consisting of benzoic acid, a water-soluble salt of benzoic acid selected from the group consisting of sodium benzoate, potassium benzoate, or lithium benzoate, or mixtures thereof, the fungistat having a concentration in the range of about one part per million (1 ppm) to about ten thousand parts per million (10,000 ppm) by weight; (b) maintaining the bath at a temperature from about 70 to about 90 degrees F.

Abstract: An improved panel structure wherein at least one face of the panel is perforated with small holes and where it is desirable to minimize the number of holes that get filled in with adhesive. For example, an improved noise reducing acoustic panel (30) (FIG. 3) constructed of a nonperforated inner skin (14), a perforated outer skin (16) having small holes (18), two sections (12, 12a) of honeycomb core material which are bonded or spliced together by a partially or fully encapsulated foaming adhesive (32e) which has been foamed and expanded, thereby forcing a supported film adhesive (34c) against the walls (24, 24a) of the honeycomb cells in the area of the gap (22) whereby the supported film adhesive (34c) bonds to the walls (24, 24a) of the honeycomb cells in the area of the gap (22). The nonperforated inner skin (14) has been adhesively bonded by a film adhesive to the honeycomb core sections (12, 12a).

Abstract: An improved process that is commercially practical for forming an oxide film cobalt conversion coating exhibiting corrosion resistance and paint adhesion properties on an aluminum or aluminum alloy substrate (for example, aerospace and aircraft parts), the process including the steps of: (a) providing an oxide film forming cobalt conversion solution including an aqueous reaction solution, containing no triethanolamine (TEA), prepared by reacting the following starting materials: (1) a water soluble cobalt-II salt; (2) a water soluble ammonium salt; (3) a water soluble inorganic complexing agent selected from the group consisting of water soluble metal nitrites; (4) a water soluble organic complexing agent; and (5) a water soluble oxidizing agent; and (b) contacting the aluminum or aluminum alloy substrate with the aqueous reaction solution for a sufficient amount of time to oxidize the surface of the substrate, whereby the oxide film cobalt conversion coating is formed, thereby imparting corrosion resistance

Abstract: A process for making a layered product having a honeycomb core having empty cells, the process comprising the steps of: (a) placing a first layer of an uncured adhesive film on the top side of a central honeycomb core having empty cells, and placing a second layer of an uncured adhesive film on the bottom side of the central honeycomb core; (b) placing a first layer of an uncured prepreg material above the first layer of uncured adhesive film, and placing a second layer of an uncured prepreg material below the second layer of uncured adhesive film; (c) placing a first layer of a dry fiber preform above the first layer of uncured prepreg material, and placing a second layer of a dry fiber preform below the second layer of uncured prepreg material; (d) placing the charge made by steps (a)-(c) inside a mold and closing the mold; (e) heating the mold to the cure temperature of the adhesive film and the prepreg material, and holding the mold at this temperature for sufficient time to cure the adhesive film and the

Abstract: A process of forming and shaping a preheated workpiece made of honeycomb core material using a press including complementary male and female dies. The first step of the process is providing a carrier sheet for supporting the workpiece. The carrier sheet is suspended over the female die by two shafts supported by support towers. The next step is loading the preheated workpiece onto the carrier sheet. The next step is applying rotational torque to each of the two shafts whereby the carrier sheet is wrapped around the said shafts thereby applying tension to the carrier sheet and pulling the shafts toward each other and into pressing contact with the sides of the workpiece while said carrier sheet means supports the bottom surface of said workpiece.

Abstract: An improved panel structure wherein at least one face of the panel is perforated with small holes and where it is desirable to minimize the number of holes that get filled in with adhesive. For example, an improved noise reducing acoustic panel (30) (FIG. 3) constructed of a nonperforated inner skin (14), a perforated outer skin (16) having small holes (18), two sections (12, 12a) of honeycomb core material which are bonded or spliced together by a partially or fully encapsulated foaming adhesive (32e) which has been foamed and expanded, thereby forcing a supported film adhesive (34c) against the walls (24, 24a) of the honeycomb cells in the area of the gap (22) whereby the supported film adhesive (34c) bonds to the walls (24, 24a) of the honeycomb cells in the area of the gap (22). The nonperforated inner skin (14) has been adhesively bonded by a film adhesive to the honeycomb core sections (12, 12a).

Abstract: A process for making a layered product having a honeycomb core having cells filled with a foam material, the process comprising the steps of: (a) placing a first layer of an uncured, heat-expandable, foamable material on the top side of a central honeycomb core having empty cells, and placing a second layer of an uncured, heat-expandable, foamable material on the bottom side of the central honeycomb core; (b) placing a first layer of an uncured preform material above the first layer of uncured, heat-expandable, foamable material, and placing a second layer of an uncured preform material above the second layer of uncured, heat-expandable, foamable material; (c) placing the charge made by steps (a) and (b) inside a mold and closing the mold; (d) heating the mold to the cure temperature of the heat-expandable, foamable material, and holding the mold at this temperature for sufficient time to expand and cure the heat-expandable, foamable material; (e) reducing the temperature of the mold to the injection temperat

Abstract: A process for making a layered product having a honeycomb core having empty cells, the process comprising the steps of: (a) placing a first layer of an uncured adhesive film on the top side of a central honeycomb core having empty cells, and placing a second layer of an uncured adhesive film on the bottom side of the central honeycomb core; (b) placing a first layer of an uncured prepreg material above the first layer of uncured adhesive film, and placing a second layer of an uncured prepreg material below the second layer of uncured adhesive film; (c) placing a first layer of a dry fiber preform above the first layer of uncured prepreg material, and placing a second layer of a dry fiber preform below the second layer of uncured prepreg material; (d) placing the charge made by steps (a)-(c) inside a mold and closing the mold; (e) heating the mold to the cure temperature of the adhesive film and the prepreg material, and holding the mold at this temperature for sufficient time to cure the adhesive film and the

Abstract: An improved process that is commercially practical for forming an oxide film cobalt conversion coating exhibiting corrosion resistance and paint adhesion properties on an aluminum or aluminum alloy substrate for use in aircraft/aerospace applications (for example, an aluminmn or aluminum alloy commercial airplane part), the process comprising the steps of: (a) providing an oxide film forming cobalt conversion solution comprising an aqueous reaction solution prepared by reacting the following starting materials:(1) a cobalt-II salt;(2) an ammonium salt;(3) one or more inorganic complexing agents selected from a soluble metal carboxylate, a soluble metal nitrite, or ammonia;(4) a water soluble amine; and(5) an oxidizing agent; and(b) contacting the substrate with the aqueous reaction solution for a sufficient amount of time to oxidize the surface of the substrate, whereby the oxide film cobalt conversion coating is formed, thereby imparting corrosion resistance and paint adhesion properties to the substrate.

Abstract: A portable version of a honeycomb core forming restricter (20) for forming and shaping a workpiece made of stiff honeycomb core material, the apparatus (20) to be used in combination with a press including a male die (70) and a female die (72), the apparatus (20) including: (a) a base plate (62); (b) four support tower assemblies (24a, 24b, 24c, 24d) supported by the base plate (62); (c) two shafts (22a, 22b) supported by the support tower assemblies (24a, 24b, 24c, 24d), the shafts (2a, 22b) being arranged in a generally parallel relationship to each other and to the longitudinal axis of the female die 72; (d) a carrier sheet (74) for supporting the workpiece, the carrier sheet (74) being attached to the two shafts (22a, 22b); (e) four air motors (26a, 26b, 26c, 26d) for applying rotational torque to the shafts ( 22a, 22b); and (f) the support tower assemblies including a double acting air cylinder (36a) for moving the shaft (22a) in a transverse direction with respect to the longitudinal axis of the female

Abstract: (A.) A process for forming a cobalt conversion coating on a metal substrate, thereby imparting corrosion resistance and paint adhesion properties. The invention was developed as a replacement for the prior art chromic acid process. The substrate may be aluminum or aluminum alloy, as well as magnesium and its alloys, Cd plated substrates, and Zn plated substrates. The cobalt-III hexacoordinated complex may be present in the form of Me.sub.3 [Co(NO.sub.2).sub.6 ] wherein Me is one or more of Na, K, and Li. (B.) A chemical conversion coating solution for producing the cobalt conversion coating on a metal substrate, the solution being an aqueous solution having a pH of about 7.0 to 7.2 and containing a soluble cobalt-III hexacoordinated complex, the concentration of the cobalt-III hexacoordinated complex being from about 0.1 mole per gallon of solution to the saturation limit of the cobalt-III hexacoordinated complex.

Abstract: (A.) A process for forming a cobalt conversion coating on a metal substrate, thereby imparting corrosion resistance and paint adhesion properties. The invention was developed as a replacement for the prior art chromic acid process. The process includes the steps of: (a) providing a cobalt conversion solution comprising an aqueous reaction solution containing a soluble cobalt-III hexacoordinated complex, the concentration of the cobalt-III hexacoordinated complex being from about 0.01 mole per liter of solution to the saturation limit of the cobalt-III hexacoordinated complex, and acetic acid; and (b) contacting the substrate with the aqueous solution solution for a sufficient amount of time, whereby the cobalt conversion coating is formed. The substrate may be aluminum or aluminum alloy, as well as Cd plating, Zn plating, Zn--Ni plating, and steel. The cobalt-III hexacoordinated complex may be present in the form of [Co(NH.sub.3).sub.6 ]X.sub.3 wherein X is Cl, Br, NO.sub.3, CN, SCN, 1/3PO.sub.4, 1/2SO.sub.

Abstract: (A.) A process for forming a cobalt conversion coating on a metal substrate, thereby imparting corrosion resistance and paint adhesion properties. The invention was developed as a replacement for the prior art chromic acid process. The process includes the steps of: (a) providing a cobalt conversion reaction solution comprising an aqueous, alkaline solution containing a soluble cobalt-III hexacoordinated complex, the concentration of the cobalt-III hexacoordinated complex being from about 0.1 mole per gallon of solution to the saturation limit of the cobalt-III hexacoordinated complex; and (b) contacting the substrate with the aqueous reaction solution for a sufficient amount of time, whereby the cobalt conversion coating is formed. The substrate may be aluminum or aluminum alloy, as well as Cd plating, Zn plating, Zn--Ni plating, and steel. The cobalt-III hexacoordinated complex may be present in the form of [Co(NH.sub.3).sub.6 ]X.sub.3 wherein X is Cl, Br, NO.sub.3, CN, SCN, 1/3PO.sub.4, 1/2SO.sub.4, C.sub.

Abstract: (A) A process for forming an oxide film cobalt conversion coating on a metal substrate, thereby imparting corrosion resistance and paint adhesion properties. The invention was developed as a replacement for the prior art chromic acid process. The process includes the steps of: (a) providing a cobalt conversion solution comprising an aqueous reaction solution containing a soluble cobalt-III hexacoordinated complex, the concentration of the cobalt-III hexacoordinated complex being from about 0.01 mole per liter of solution to the solubility limit of the cobalt-III hexacoordinated complex; and (b) contacting the substrate with the aqueous reaction solution for a sufficient amount of time, whereby the cobalt conversion coating is formed. The substrate may be aluminum or aluminum alloy, as well as Cd plated, Zn plated, Zn--Ni plated, and steel. The cobalt-III hexacoordinated complex may be present in the form of Me.sub.m [Co(R).sub.6 ].sub.

Abstract: (A.) A process for forming a cobalt conversion coating on a metal substrate, thereby imparting corrosion resistance and paint adhesion properties. The invention was developed as a replacement for the prior art chromic acid process. The process includes the steps of: (a) providing a cobalt conversion solution comprising an aqueous reaction solution containing a soluble cobalt-III hexacoordinated complex, the concentration of the cobalt-III hexacoordinated complex being from about 0.01 mole per liter of solution to the saturation limit of the cobalt-III hexacoordinated complex, and acetic acid; and (b) contacting the substrate with the aqueous reaction solution for a sufficient amount of time, whereby the cobalt conversion coating is formed. The substrate may be aluminum or aluminum alloy, as well as Cd plating, Zn plating, Zn--Ni plating, and steel. The cobalt-III hexacoordinated complex may be present in the form of [Co(NH.sub.3).sub.6 ]X.sub.3 wherein X is Cl, Br, NO.sub.3, CN, SCN, 1/3PO.sub.4, 1/2SO.sub.

Abstract: (A.) A process for forming a cobalt conversion coating on a metal substrate, thereby imparting corrosion resistance and paint adhesion properties. The invention was developed as a replacement for the prior art chromic acid process. The process includes the steps of: (a) providing a cobalt conversion reaction solution comprising an aqueous, alkaline solution containing a soluble cobalt-III hexacoordinated complex, the concentration of the cobalt-III hexacoordinated complex being from about 0.1 mole per gallon of solution to the saturation limit of the cobalt-III hexacoordinated complex; and (b) contacting the substrate with the aqueous reaction solution for a sufficient amount of time, whereby the cobalt conversion coating is formed. The substrate may be aluminum or aluminum alloy, as well as Cd plating, Zn plating, Zn-Ni plating, and steel. The cobalt-III hexacoordinated complex may be present in the form of [Co(NH.sub.3).sub.6 ]X.sub.3 wherein X is Cl, Br, NO.sub.3, CN, SCN, Y.sub.3 PO.sub.4, SO.sub.4, C.