Abstract: The present invention provides to image processing methods that include a method of selecting an optimal threshold value (to) for an image comprising the steps of: obtaining an image; selecting a test segment of the said image; determining the mean feature size (S) of features appearing in the test segment at each of a plurality of threshold values (t), so as to produce mean feature size data (S(t)); selecting a relevant subset of the mean feature size data (S(t)); and determining an optimal threshold value (to) as a function of said subset of the mean feature size data. The present invention additionally provides methods of thresholding an image to produce a binary image by application of the optimal threshold value (to) determined according to the methods of the present invention.

Abstract: To provide a coating composition of a soluble aromatic polyimide having good heat resistance and mechanical strength. As a soluble polyimide, a compound of the formula (I) in which R's represent independently from one another H, halogen, an alkyl group or an alkoxy group, or a substituted or unsubstituted phenyl group; A is a tetravalent aromatic group or a group of the formula (II) in which B is a covalent bond, a >C(R2)2 group, a carbonyl group, O, S, a >SO2, group, a >Si(CH3)2 group, a >Si(C2H5)2 group, a >NR3 group or a bifunctional ether group in which R2 is a hydrogen atom or —C(R4)3, R3 is H, an alkyl group or an aryl group, and R4 is H, F or Cl; Ar is an aromatic nucleus or a group of the formula (III) in which Ar and B are the same as defined above, and each p is an integer of 0 to 10; m is an integer of 1 to 10 is used. The polyimide has a weight average molecular weight of 150,000 to 1,000,000.

Abstract: A curable melt blended composition and a method of making the composition by melt blending a thermoplastic polymer comprising polyphenylene ether (PPE) polymer and a polystyrene polymer, preferably high impact polystyrene (HIPS), and optionally a compatiblizer, with an uncured epoxy component, comprising a curable epoxy and an epoxy curing agent, at a temperature greater than 150° C. and without addition of solvent wherein the epoxy component of the resulting curable melt blended composition remains substantially uncured.

Abstract: A method and apparatus are provided for peeling a thin film, typically 100 microns or less in thickness, from a liner by use of a rotatable peel rod supported in an air bearing. The air bearing comprises a support plate having arcuate surfaces which are substantially coaxial with a cylindrical film-bearing segment of the peel rod. Air openings in the arcuate surfaces conduct a flow of air into an air bearing gap between the arcuate surfaces and the peel rod.

Abstract: Zwitterionic imide compounds are provided according to the formula: R1—SO2—N?—SO2—R2+, where R1 and R2+ are any suitable groups. Typically R1 is a highly fluorinated alkane and R2+ contains a quaternary ammonium group or a heteroatomic aromatic group having an cationic nitrogen, such as: pyridiniumyl, pyridaziniumyl, pyrimidiniumyl, pyraziniumyl, imidazoliumyl, pyrazoliumyl, thiazoliumyl, oxazoliumyl, or triazoliumyl. Zwitterionic liquids are provided, typically having melting points of less than 100° C. and typically having a solubility in water of less than 5% by weight.

Abstract: Methods are provided to make acid functional fluoropolymers by: a) dehydrofluorinating a starting fluoropolymer with a dehydrofluorinating agent to form an unsaturated fluoropolymer; b) adding an acidifiable nucleophilic functionalizing agent to a double bond of the unsaturated fluoropolymer; and c) acidifying the added acidifiable function. Acid functional fluoropolymers and ion conducting membranes thereof are also provided, including acid functional fluoropolymer having pendent groups according to the formula: —X—Ar—An, wherein X is selected from O, S or NR, where R is selected from H and C1-C30 alkyl or aryl, which are optionally substituted, wherein Ar is a C6-C30 aromatic group, which is optionally substituted, wherein A is an acidic function or salt thereof, wherein a can be independently chosen to be 1, 2 or 3.

Abstract: A curable melt blended composition and a method of making the composition by melt blending a thermoplastic polymer comprising polyphenylene ether (PPE) polymer and a polystyrene polymer, preferably high impact polystyrene (HIPS), and optionally a compatiblizer, with an uncured epoxy component, comprising a curable epoxy and an epoxy curing agent, at a temperature greater than 150° C. and without addition of solvent wherein the epoxy component of the resulting curable melt blended composition remains substantially uncured.

Abstract: An apparatus and method for lamination are provided, which are advantageously used in intermittent lamination and fixed-gap lamination, the apparatus comprising first and second laminating rollers defining a laminating gap therebetween and at least one gapping block positioned between the first and second rollers such that the gapping block determines and maintains a minimum gap width. The gapping block comprises a rigid gapping block body, which may be adjustable in width, and four or more load wheels rotatably attached to the gapping block body which ride on a portion of the first and second rollers.

Abstract: Flow field designs are provided, as well as flow field devices employing the subject flow field designs. A fluid distribution assembly is provided comprising a flow field device and a fluid transport layer disposed between the flow field device and a target area, where, for at least one finite non-zero flow rate and at least one use rate of an active component of the fluid in the fluid transport layer, lateral flux of the active component varies by no more than 35% through at least 90% of all overland portions of said fluid transport layer. In one embodiment, the flow field device comprises a flow field comprising a serpentine channel, comprising non-parallel sequential major segments. In a further embodiment, the angles between successive major segments of the serpentine channel vary progressively.

Abstract: Stacking porous and non-porous material layers involves applying vacuum to a first porous layer to stabilize same relative to a support structure. The support structure and/or a non-porous layer are moved to establish contact between the non-porous layer and the first porous layer. The first porous and non-porous layers define a sub-assembly. While applying vacuum to the sub-assembly, one or both of the support structure and a second layer are moved to establish contact between the second layer and the non-porous layer. Vacuum applied to the sub-assembly maintains positional stability of the sub-assembly layers relative to the support structure while the second layer is moved into contact with the non-porous layer. Vacuum is subsequently removed to facilitate transporting of the material layer stack. Material layers of a fuel cell, including first and second fluid transport layers and a membrane, are well suited for automated stacking.

Abstract: A method and apparatus for separating a membrane electrode assembly (MEA) from a fixture assembly subsequent to MEA bonding within the fixture assembly involves stabilizing the first fixture of the fixture assembly. The second fixture of the fixture assembly is stabilized. While the second fixture is stabilized, the first fixture is pressurized to cause the first surface of the MEA to separate from the first fixture. While the first fixture is stabilized, the second fixture is pressurized to cause the second surface of the MEA to separate from the second fixture. The second fixture is then moved out of proximity with the first fixture to permit removal of the MEA from the first fixture.

Abstract: An apparatus and method provide for automated converting of a web of a thin patterned catalyst-coated membrane to separate membrane sheets for fuel cell assembly. The membrane typically has a thickness of about one thousandth of an inch. Automated web converting involves transporting, with use of a movable vacuum, an end portion of the membrane web from a first location to a second location. With use of respective first and second vacuums at the first and second locations, and after removal of the movable vacuum, the end portion of the membrane web is releasably secured at the first and second locations. The membrane web is cut within a gap defined between a single catalyst pattern of the membrane web end portion and an adjacent catalyst pattern to produce a membrane sheet. The membrane sheet is precisely positioned to a desired orientation to facilitate subsequent processing of the membrane sheet.

Abstract: A method is provided for making a hydrophilic carbon fiber construction comprising the steps of: a) immersing a carbon fiber construction in an aqueous dispersion of one or more metal oxides, comprising: i) 1-15% by weight metal oxide; ii) 0.01%-5% by weight dispersant; and b) subsequently heating the carbon fiber construction sufficiently to remove substantially all of the dispersant. Typically the entire method can be completed in less than 20 minutes. In addition, a hydrophilic carbon fiber construction made according to the method of the present invention is provided, typically having a loading of metal oxide equivalent to 20-50 mg metal per gram of carbon.

Abstract: A first fixture of a transportable fixture apparatus incorporates a substantially porous first region adapted to receive one or more porous and/or non-porous first material layers, such as fuel cell layers, and to facilitate formation of a vacuum between the first fixture and the first material layers. A second fixture incorporates a substantially porous second region adapted to receive one or more porous and/or non-porous second material layers and to facilitate formation of a vacuum between the second fixture and the second material layers. A stop arrangement protrudes from one or both of the first and second fixtures, and is situated peripheral to the first and second material layers when the first and second fixtures are brought into contact. The stop arrangement defines a cavity adapted to effect compression of the first and second material layers when the first and second fixtures are brought into contact.

Abstract: A method is provided for making aromatic-imide and aromatic-methylidynetrissulfonyl species by reaction of aromatic species with a reactant according to formula (I): (X—SO2—)m—QH—(—SO2—R1)n  (I) wherein Q is C or N; wherein each X is independently selected from the group consisting of halogens, typically F or Cl; wherein each R1 is independently selected from the group consisting of aliphatic and aromatic groups, which may or may not be saturated, unsaturated, straight-chain, branched, cyclic, heteroatomic, polymeric, halogenated, fluorinated or substituted; wherein m is greater than 0; wherein m+n=2 when Q is N; and wherein m+n=3 when Q is C. Ar may be derived from an aromatic polymeric compound.

Abstract: A method and apparatus for identifying the orientation and positions of the elements of a grid in an image. The elements of the grid need not be parallel to the sides of the image, and the image need not contain all of the elements of the grid. The method can be applied to multi-sided grids, whether rectilinear or distorted. The addresses of identified grid elements can be used to control, e.g., analytical procedures directed to individual elements.

Abstract: The present invention provides a compound according to the formula: CH2═C(R1)—C(O)—R6—NHCO2(CH2)p(CF2)q—O—((CF2)8CFXO)m(CF2)r—Z wherein each R1 is independently selected from —H, —CH3, —F and —Cl, wherein each R6 is independently selected from substituted or unsubstituted C1-C10 alkyl, cyclic alkyl, or aryl groups, wherein each a is independently selected from 0-3, wherein each X is independently selected from —F, —CF3 or —CF2CF3, wherein each p is independently selected from 1-4, each q is independently selected from 1-5, each r is independently selected from 1-5, each m is independently selected from 1-50, each Z is independently selected from —F and —(CH2)5OH, and each s is independently selected from 1-4. The present invention also provides for the use of this compound as a surfactant in highly fluorinated liquid solvents. Latexes of dispersed particles utilizing this surfactant are provided.

Abstract: An aqueous coating composition is provided comprising carbon particles, one or more highly fluorinated polymers and one or more amine oxide surfactants, typically an amine oxide surfactant according to formula I: where n is 9 to 19. The coating composition is advantageously used in a method of making a gas diffusion layer for an electrochemical cell comprising the steps of: a) coating a electrically conductive porous substrate with the aqueous coating composition, and b) heating the electrically conductive porous substrate to a temperature sufficient to decompose the amine oxide surfactants. In another aspect, a gas diffusion layer for an electrochemical cell is provided which is advantageously free of surfactant.

Abstract: A supported catalyst is provided comprising catalyst metal nanoparticles having an average particle size of 3.0 nm or less, or more typically 2.0 nm or less, and typically having a standard deviation of particle size of 0.5 nm or less, which are supported on support particles at a loading of 30% or more. Typical catalyst metals are selected from platinum, palladium, ruthenium, rhodium, iridium, osmium, molybdenum, tungsten, iron, nickel and tin. Typical support particles are carbon. A method of making a supported catalyst is provided comprising the steps of: a) providing a solution of metal chlorides of one or more catalyst metals in solvent system containing at least one polyalcohol, typically ethylene glycol containing less than 2% water; b) forming a colloidal suspension of unprotected catalyst metal nanoparticles by raising the pH of the solution, typically to a pH of 10 or higher, and heating said solution, typically to 125 ° C.

Abstract: A method is provided for making aromatic-imide and aromatic-methylidynetrissulfonyl species by reaction of aromatic species with a reactant according to formula (I): (X—SO2—)m—QH—(—SO2—R1)n  (I) wherein Q is C or N; wherein each X is independently selected from the group consisting of halogens, typically F or Cl; wherein each R1 is independently selected from the group consisting of aliphatic and aromatic groups, which may or may not be saturated, unsaturated, straight-chain, branched, cyclic, heteroatomic, polymeric, halogenated, fluorinated or substituted; wherein m is greater than 0; wherein m+n=2 when Q is N; and wherein m+n=3 when Q is C. Ar may be derived from an aromatic polymeric compound.