Patents Represented by Attorney Ralph G. Medhurst
  • Patent number: 4880550
    Abstract: A method for preparing a carbonate overbased calcium sulfonate, which method comprises the steps of:(1) forming an initial mixture of a lower molecular weight alkanol, an alkyl or alkaryl substituted sulfonic acid or sulfonate compound, a diluent and a solvent; (2) adding a basic calcium compound to the initial mixture to form a second mixture in which the amount of added calcium is at least about ten times the amount necessary to form a neutral calcium sulfonate; (3) heating the second mixture to reflux temperature; (4) carbonating the second mixture at said reflux temperature to form a carbonated product while simultaneously and continuously removing water produced by the carbonation reaction; (5) after carbonation is stopped, heating the carbonated product to an elevated temperature sufficient to remove the alkanol; and (6) removing solids and solvent from the carbonated product.
    Type: Grant
    Filed: August 26, 1988
    Date of Patent: November 14, 1989
    Assignee: Amoco Corporation
    Inventor: Mack W. Hunt