Abstract: A modular reactor system and method for synthesizing chemical compounds characterized by a uniform temperature throughout the reaction mixture by use of a continuous flow reactor under high pressure. The apparatus includes a number of generic components such as pumps, flow channels, manifolds, flow restrictors, and valves. Modular reactors, separator and analyzers on an assembly board provide a system where a modular reactor unit has an I.D. of up 100 .mu.m to optimize control of residence time within a reaction zone.

Abstract: A portable microwave instrument for evaluating characteristics of a structural member includes a source of microwave energy, a transmitter coupled to the source of microwave energy for transmitting a microwave signal at the structural member, and a receiver positioned on the same side of the structural member as the transmitter and being disposed to receive a microwave signal reflected by the structural member. A phase angle difference is determined between the transmitted microwave signal and the received microwave signal using a signal splitter and a balanced mixer. The difference in phase angle varies in accordance with differences in size, shape and locations of constituent materials within the structural member.

Abstract: A novel stable inflatable or inflated sail board is provided. The sailboard includes a plurality of discrete, gas-fillable or gas-filled, elongated chambers, each chamber having a top skin and a bottom skin, each chamber, when inflated being sufficiently rigid to maintain its shape without any additional support, and to provide a flat bottom surface for contact with water, the chambers being integrally united to provide an elongated float which is of greater length than width. The sailboard also includes a supporting and stiffening rigid frame comprising a plurality of frame sections which are interconnectable with each other in a longitudinal direction, the frame supporting the floatation member and providing additional stiffness and resistance to fore-and-aft bending and torsion.

Abstract: A liquid photopolymer layer covering a phototool image surface with one surface exposed to air is exposed by radiation through the phototool to partially harden in a pattern defined by the image the photopolymer layer through a part of its thickness. The air exposed surface portion is thus left in liquid form for contacting the surface of a printed wiring board, preferably by scanning along the length of a phototool with a pressurized roll or blade to contact and adhere the preimaged laminate to board surface in an air bubble free lamination where subsequent radiation exposure finishes the curing and bonds the cured portion of the polymer layer to the PWB substrate. After removal of the phototool, the polymer layer is developed by washing out uncured polymer portions as defined by the image pattern.

Abstract: An ultrasonic nozzle includes an atomizing surface for producing an atomized liquid spray; a liquid-feed passageway for supplying the process liquid to the atomizing surface, the passageway having a first diameter section and a second fluidly connected smaller diameter section, with a shoulder defined therebetween; an internal shut-off assembly for preventing the supply of process liquid to the atomizing surface, the shut-off assembly including a shut-off rod slidably positioned within the passageway and having a sealing end adapted to cooperate with the shoulder to prevent the supply of process liquid to the atomizing surface, an actuator piston connected with the opposite end of the shut-off rod and slidable within a cylinder bore that is in fluid communication with the passageway, and a valve actuator for slidably moving the piston and shut-off rod in the passageway between a first closed position in which the supply of liquid to the atomizing surface is prevented and a second open position in which the su

Abstract: A coating applicator is provided for depositing a film on a surface of glass and other substrates by chemical vapor deposition. The applicator includes a pair of opposing coating nozzles for applying a vaporized coating chemical reactant in a carrier gas to the surface at such a concentration and velocity that coating of the surface is achieved under substantially reaction rate controlled conditions. Each coating nozzle is positioned adjacent the surface with a small clearance therebetween which is open to the outside atmosphere. The opposing coating nozzles are directed toward each other at a selected angle with respect to a normal to the surface of the substrate. The angle and the clearance provides a condition where there is substantially no intermixing of coating vapors with the outside atmosphere.

Abstract: Novel chromium plating baths suitable for electrodepositing chromium layers which are bright, adherent, smooth and hard, and are capable of being formed at both high and low current densities, and at high cathodic current efficiencies, consist essentially of chromic acid and sulfoacetic acid in a concentration range of about 40 to 150 g/l., and selenate or tellurate ion. Sulfate ion, if present, is included in low concentrations such that the Cr/SO.sub.4 ratio is high, preferably 300:1 or more.

Abstract: A multiple, parallel packed column vaporizer for vaporizing a chemical having a relatively low decomposition temperature includes a shell; a plurality of parallel, vertically oriented vaporization columns arranged in the shell, each vaporization column having inner walls and upper and lower open ends; a distribution assembly for distributing the chemical substantially equally to the open upper ends of the vaporization columns, which flows downwardly therein; a heat exchanger which heats the vaporization columns to provide the heat needed to vaporize the chemical therein; and a gas supply which supplies the gas to the lower ends of the vaporization columns so that the chemical is vaporized and becomes entrained in the gas and is carried upwardly out of the vaporizer.

Abstract: A surface modified U.V. stabilized article is described which includes a resinous sheet whose sides are both exposed to the air. The surface regions of both sides of the sheet are substantially fully modified in situ with a stabilizing amount of an ingredient such as a ultraviolet light stabilizer material, while the exposed surfaces are substantially free of residual stabilizer and solvent material. The appearance and degree of surface perfection of the modified sides of the sheet are substantially the same as that of an untreated sheet.The U.V. stabilized resin article is made by a continuous process in which the resin body is immersed in a solution of a ultraviolet light stabilizer in a suitable organic solvent, and thereafter, residual stabilizer and solvent are displaced from the modified surface in situ. Both steps in the process are carried out in an environment which are non-evaporative of the solvent.

Abstract: Paste-consistency photopolymer is imaged onto printed wiring boards by coating the board overall and positioning the photographic film over the board in register and off-contact. A resilient blade is pressed against the phototool at one end of the board and drawn across the surface, thus forcing the photographic film into intimate contact with the photopolymer and purging all air therebetween. Mounted on the resilient blade aft of leading edge is a shuttered tubular lamp which hardens the photopolymer where the photographic film is clear, so that in a single pass the photographic film is sequentially mated and photopolymer exposed, to produce line widths unmatched by competing dry film systems and at speeds of 0.5 feet per second.

Abstract: A coating hood for applying uniform protective coatings to glass containers, while minimizing the escape of noxious fumes from the hood to the ambient atmosphere, which includes a pair of spaced side walls having inclined end surfaces adjacent the entrance and exit ends to reduce the amount of stagnant ambient air thereat; coating air supply slots in the side walls for supplying process air to the containers; and finish air supply slots positioned at a height above the coating air supply slots for supplying coating free air.

Abstract: Aqueous alkaline developable, UV curable urethane acrylate compounds and compositions are particularly useful for making flexible, 100% solids, solvent-free solder mask coatings which are characterized by having screen-printable viscosities, rapid developability and advantageous performance characteristics.

Abstract: An improvement in the process of incorporating a modifier ingredient into the surface region of a resinous article is described herein. The basic process includes immersing the article in a liquid such as water and contacting the immersed article with a solution of a modifier ingredient in a solvent which is immiscible with the liquid. The improvement herein comprises removing a substantial amount of air dissolved in the water layer to prevent droplets of solution from rising to the surface of the water layer during the process, thereby preventing solid modifier material from accumulating on the water surface.

Abstract: A composition and method are disclosed for electroplating microporous chromium layers without the requirement that microparticles be present either in the chromium layer or in a sublayer. A composition used contains chromic acid and sulfoacetic acid and, optionally, dichromate ion, sulfate ion and/or fluoride ion but being substantially free of iodide, selenide or bromide ions. A deposit having at least 20,000 micropores per square inch results. The process may be used to make multiple layer articles having an outer layer of microporous chromium.

Abstract: A surface modified, U.V. stabilized opaque polyvinyl chloride resin article and process for making same is described. The article includes a white pigment, such as titanium dioxide, in low amounts. The modified surface is substantially free of residual stabilizer and solvent, and its appearance and degree of surface perfection is substantially the same as an unmodified side of the article.The process of the invention is characterized by the steps of immersing the polyvinyl chloride article is immersed in a suitable liquid media, then contacted with a solution of an ultraviolet light stabilizer in a suitable organic solvent, and residual stabilizer and solvent are displaced in situ, i.e. in a non-evaporative environment without contacting the air.

Abstract: A submersible positive displacement piston pump includes a cylinder for insertion within a body of liquid, the cylinder including a working end and an opposite end, an inlet port, an outlet port and a working chamber bounded by the outlet port and the working end; a piston rotatably and reciprocably movable in the cylinder between a retracted positon and an extended position for pumping liquid from the inlet port to the outlet port, the piston including a free end having a recessed section alternately in fluid communication with the inlet port and the outlet port; a pivoting assembly pivotally connected to a drive motor which rotatably and reciprocably drives the piston in the cylinder; and an extension assembly for connecting the pivoting assembly to the piston and for ensuring that the pivoting assembly and the drive motor are positioned out of the body of liquid when the piston and cylinder are positioned in the body of liquid, the extension assembly including a shaft extension for connecting the pivoting

Abstract: A composition including a mixture of UV curable urethane acrylate and a urethane diacrylate compounds provides an aqueous alkaline developable, flexible solder mask having excellent electrical insulation resistance under hydrolytic testing conditions at elevated temperatures.

Abstract: Corrosion resistant electrodeposited chromium layers, processes for their electrodepositions and plating baths suitable for use therein are disclosed. The corrosion resistant chromium layers also are bright, adherent, smooth, hard, wear resistant, and exhibit a low coefficient of friction. Electrodeposition is carried out at both high and low currrent densities. The baths used comprise 450-650 g/l of chromic acid, 40-100 g/l of sulfoacetic acid and 0-4.5 g/l of sulfate ion and are substantially free of other carboxylic acids, fluoride ions, iodide ions, bromide ions and selenium ions. The baths used comprise 400-650 g/l of chromic acid, 40-100 g/l of sulfoacetic acid and 0-4.5 g/l of sulfate ion and are substantially free of other carboxylic acids, flouride ions, iodide ions, bromide ions and selenium ions.

Abstract: A chromium plating bath which consists essentially of chromic acid and 40-100 g/l of sulfoacetic acid, and which is substantially free of carboxylic acid, fluoride, iodide, bromide and selenium ions, is described herein.

Abstract: A functional chromium electroplating bath and process is disclosed. The bath comprises chromic acid, sulfoacetic acid, iodate and a nitrogen organic compound. Such a bath gives chromium deposits which are both bright and adherent.