Patents Represented by Attorney Steven A. Owen
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Patent number: 7880032Abstract: Disclosed is a process and apparatus for treating a purge stream in a carboxylic acid production process. The process employs a purge process that allows for the separation of oxidation byproducts into benzoic acid and non-benzoic acid oxidation byproducts, thus providing flexibility in the treatment and use of such oxidation byproducts.Type: GrantFiled: January 19, 2007Date of Patent: February 1, 2011Assignee: Eastman Chemical CompanyInventors: Kenny Randolph Parker, Philip Edward Gibson
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Patent number: 7863481Abstract: Disclosed is a process and apparatus for treating a purge stream in a carboxylic acid production process. The process employs a purge process that allows for the separation of oxidation byproducts into benzoic acid and non-benzoic acid oxidation byproducts, thus providing flexibility in the treatment and use of such oxidation byproducts.Type: GrantFiled: August 16, 2007Date of Patent: January 4, 2011Assignee: Eastman Chemical CompanyInventors: Philip Edward Gibson, Kenny Randolph Parker
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Patent number: 7863483Abstract: Disclosed are processes and apparatus for producing a carboxylic acid. The processes employ a concentration section disposed before and/or after a product isolation section, which allows for oxidation byproducts produced in the process to exit the product isolation section with the isolated carboxylic acid product and/or to be combined with the isolated carboxylic acid product downstream of the product isolation section at a rate of at least about 15 percent of the net make rate of the oxidation byproducts in the production process.Type: GrantFiled: February 12, 2007Date of Patent: January 4, 2011Assignee: Eastman Chemical CompanyInventors: Philip Edward Gibson, Kenny Randolph Parker
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Patent number: 7855305Abstract: A process is provided for producing an enriched carboxylic acid compositions produced by contacting composition comprising a carboxylic acid with an enrichment feed in an enrichment zone to form an enriched carboxylic acid composition. This invention also relates to a process and the resulting compositions for removing catalyst from a carboxylic acid composition to produce a post catalyst removal composition.Type: GrantFiled: October 2, 2008Date of Patent: December 21, 2010Assignee: Eastman Chemical CompanyInventors: Kenny Randolph Parker, Philip Edward Gibson, Ruairi Seosamh O'Meadhra
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Patent number: 7847121Abstract: Disclosed are processes and apparatus for producing a carboxylic acid. The processes employ a concentration section disposed before and/or after a product isolation section, which allows for oxidation byproducts produced in the process to exit the product isolation section with the isolated carboxylic acid product and/or to be combined with the isolated carboxylic acid product downstream of the product isolation section at a rate of at least about 15 percent of the net make rate of the oxidation byproducts in the production process.Type: GrantFiled: February 12, 2007Date of Patent: December 7, 2010Assignee: Eastman Chemical CompanyInventors: Philip Edward Gibson, Kenny Randolph Parker
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Patent number: 7842778Abstract: The invention is directed to polyester processes where the esterification process at utilizes a vapor removing device, wherein the vapor removing device is substantially horizontally oriented, wherein the esterification effluent forms a two-phase laminar, stratified, non-circular vapor/liquid flow in at least a portion of said vapor removing device.Type: GrantFiled: August 6, 2008Date of Patent: November 30, 2010Assignee: Eastman Chemical CompanyInventor: Bruce Roger DeBruin
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Patent number: 7834208Abstract: A process is provided for producing an enriched carboxylic acid compositions produced by contacting composition comprising a carboxylic acid with an enrichment feed in an enrichment zone to form an enriched carboxylic acid composition. This invention also relates to a process and the resulting compositions for removing catalyst from a carboxylic acid composition to produce a post catalyst removal composition.Type: GrantFiled: March 1, 2006Date of Patent: November 16, 2010Assignee: Eastman Chemical CompanyInventors: Kenny Randolph Parker, Philip Edward Gibson, Ruairi Seosamh O'Meadhra
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Patent number: 7829037Abstract: Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.Type: GrantFiled: August 29, 2007Date of Patent: November 9, 2010Assignee: Eastman Chemical CompanyInventors: Thomas Earl Woodruff, Alan George Wonders
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Patent number: 7816556Abstract: Disclosed is an optimized system for more efficiently and economically producing terephthalic acid. The system includes a multi-stage oxidative digestion system for processing an improved initial slurry from primary oxidation. The multi-stage digestion system is capable of adequately purifying the improved initial slurry without requiring significant liquor exchange between primary oxidation and oxidative digestion.Type: GrantFiled: March 1, 2006Date of Patent: October 19, 2010Assignee: Eastman Chemical CompanyInventors: Alan George Wonders, Ronald Buford Sheppard, Thomas Earl Woodruff, Martin De Boer, Raymond Elbert Fogle
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Patent number: 7772424Abstract: Disclosed is an optimized system for more efficiently and economically producing terephthalic acid. The system employs an evaporative removal step downstream of oxidative digestion. The evaporative removal step removes a portion of the liquid phase and promotes precipitation of certain aromatic impurities. By promoting precipitation of certain aromatic impurities, the amount of the precipitated impurities in the recycled solvent is advantageously reduced.Type: GrantFiled: March 1, 2006Date of Patent: August 10, 2010Assignee: Eastman Chemical CompanyInventors: Alan George Wonders, Ronald Buford Sheppard, Thomas Earl Woodruff, Martin De Boer, Raymond Elbert Fogle, Philip Edward Gibson, Kenny Randolph Parker
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Patent number: 7759516Abstract: Disclosed is a process and apparatus for treating a purge stream in a carboxylic acid production process. The process employs a purge process that allows for the separation of oxidation byproducts into benzoic acid and non-benzoic acid oxidation byproducts, thus providing flexibility in the treatment and use of such oxidation byproducts.Type: GrantFiled: August 16, 2007Date of Patent: July 20, 2010Assignee: Eastman Chemical CompanyInventors: Philip Edward Gibson, Kenny Randolph Parker
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Patent number: 7741515Abstract: Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.Type: GrantFiled: June 16, 2005Date of Patent: June 22, 2010Assignee: Eastman Chemical CompanyInventors: Alan George Wonders, Wayne Scott Strasser, Marcel de Vreede, J Thomas Tidwell
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Patent number: 7741516Abstract: A process is provided for producing an enriched carboxylic acid compositions produced by contacting composition comprising a carboxylic acid with an enrichment feed in an enrichment zone to form an enriched carboxylic acid composition. This invention also relates to a process and the resulting compositions for removing catalyst from a carboxylic acid composition to produce a post catalyst removal composition.Type: GrantFiled: March 1, 2006Date of Patent: June 22, 2010Assignee: Eastman Chemical CompanyInventors: Philip Edward Gibson, Kenny Randolph Parker, Ruairi Seosamh O'Meadhra
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Patent number: 7718759Abstract: The invention is directed to polyester processes that utilizes a pipe reactor in the esterification, polycondensation, or both esterification and polycondensation processes. Pipe reactor processes of the present invention have a multitude of advantages over prior art processes including improved heat transfer, volume control, agitation and disengagement functions.Type: GrantFiled: July 15, 2008Date of Patent: May 18, 2010Assignee: Eastman Chemical CompanyInventor: Roger Bruce DeBruin
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Patent number: 7692037Abstract: Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.Type: GrantFiled: June 16, 2005Date of Patent: April 6, 2010Assignee: Eastman Chemical CompanyInventors: Alan George Wonders, Marcel de Vreede, Lee Reynolds Partin, Wayne Scott Strasser
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Patent number: 7659427Abstract: Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.Type: GrantFiled: May 7, 2008Date of Patent: February 9, 2010Assignee: Eastman Chemical CompanyInventors: Alan George Wonders, Wayne Scott Strasser, Marcel de Vreede, J. Thomas Tidwell
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Patent number: 7601795Abstract: The present invention relates to a process by which a carboxylic acid/diol mixture is obtained from a slurry or cake carboxylic acid product without isolation of a substantially dry carboxylic acid solid. More specifically, the present invention relates to a process by which a terephthalic acid/ethylene glycol mixture suitable as a starting material for polyester or co-polyester production is obtained from a slurry or cake terephthalic acid product without isolation of a substantially dry terephthalic acid solid.Type: GrantFiled: March 10, 2005Date of Patent: October 13, 2009Assignee: Eastman Chemical CompanyInventors: Kenny Randolph Parker, Robert Lin, Philip Edward Gibson
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Patent number: 7589231Abstract: Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.Type: GrantFiled: June 16, 2005Date of Patent: September 15, 2009Assignee: Eastman Chemical CompanyInventors: Alan George Wonders, Howard Wood Jenkins, Jr., Lee Reynolds Partin, Wayne Scott Strasser, Marcel de Vreede
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Patent number: 7586000Abstract: Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.Type: GrantFiled: June 16, 2005Date of Patent: September 8, 2009Assignee: Eastman Chemical CompanyInventors: Alan George Wonders, Thomas Young Lightfoot, Charles Edwan Sumner, Jr., Thomas Earl Woodruff, Ernest William Arnold, III, Eric Jackson Fugate, Charles Helton Hitchcock, Brent Alan Tennant, John David Aycock
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Patent number: 7582793Abstract: Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.Type: GrantFiled: June 16, 2005Date of Patent: September 1, 2009Assignee: Eastman Chemical CompanyInventors: Alan George Wonders, Gino Georges Lavoie, Charles Edwan Sumner, Jr.