Abstract: A process for preparing polyol fatty acid polyesters having levels of triglyceride below 0.5% is described. Methyl esters having a level of monoglycerides below 500 ppm, a nondetectable level of di- and triglyceride and a glycerine level of less than about 200 ppm are prepared and then used in a two-stage, solvent-free transesterification reaction to prepare the polyol fatty acid polyesters.
Abstract: Polyol polyesters are purified by a process comprising bleaching with a specific silica gel and/or heat treatment and removal of volatile products by steam deodorization. Any steam deodorization is at reduced temperatures or in admixture with triglycerides to minimize thermal degradation of the polyol polyesters.
Type:
Grant
Filed:
April 22, 1992
Date of Patent:
June 7, 1994
Assignee:
The Procter & Gamble Company
Inventors:
Robert Houston, Robert J. Sarama, Paul Seiden, Keith D. Adams, Gregory M. McCabe