Patents Represented by Attorney Thomas McDonnell
  • Patent number: 4131609
    Abstract: A silicon-phthalocyanine-siloxy monomer having the formula:PcSi(OSiR'Ph(OSiR".sub.2 ).sub.r X).sub.2wherein X is a hydroxyl group or unreido group having the formula: ##STR1## Pc is a phthalocyanine nucleus, R' and R" are alkyl groups having from 1 to 8 carbon atoms, and r is an integer from 1 to 4. The monomers are useful as dyes and in polymer synthesis as reactive intermediates.
    Type: Grant
    Filed: February 23, 1978
    Date of Patent: December 26, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Kenneth J. Wynne, John B. Davison
  • Patent number: 4131444
    Abstract: Strengthened and densified ceramic bodies are produced by hot pressing lead itanate powder into a lead titanate ceramic at a pressure from 1000 to 5000 psi and at a temperature from 700 to 1100.degree. C if the atmosphere is reducing or from 700 to 1200.degree. C if the atmosphere is oxidizing and by annealing the lead titanate ceramic at a temperature from 600 to 1100.degree. C in an oxidizing atmosphere for at least four hours.
    Type: Grant
    Filed: August 25, 1977
    Date of Patent: December 26, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Basil E. Walker, Robert C. Pohanka, Paul L. Smith, Roy W. Rice
  • Patent number: 4124408
    Abstract: A polymeric residue with one or more metals, salts, and oxides mixed therein, deposited on refrigeration system surfaces by a circulating halogenated hydrocarbon refrigerant, is removed from a surface by contacting the residue with a saturated aqueous solution or slurry with a pH from 2 to 4 of ethylenediaminetetraacetic acid at temperatures from 30.degree. C to 100.degree. C.
    Type: Grant
    Filed: June 2, 1977
    Date of Patent: November 7, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Harold G. Eaton, David L. Venezky
  • Patent number: 4124671
    Abstract: A method for strengthening lead zirconate-lead titanate ceramic transducers hich comprises heating the transducer at a temperature from 900.degree. C to 1000.degree. C in a nonreducing atmosphere containing at least 20 volume percent of oxygen for at least one hour.
    Type: Grant
    Filed: November 25, 1975
    Date of Patent: November 7, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Basil E. Walker, Robert C. Pohanka, Roy W. Rice
  • Patent number: 4119556
    Abstract: Storage of thermal energy in a ternary mixture of salts which comprises from 22.5 to 26.5 weight percent of sodium chloride, from 18.5 to 22.5 weight percent of potassium chloride and from 53.0 to 57.0 weight percent of magnesium chloride.
    Type: Grant
    Filed: June 1, 1977
    Date of Patent: October 10, 1978
    Inventor: Talbot A. Chubb
  • Patent number: 4116945
    Abstract: Compounds of the general formula: ##STR1## wherein R.sub.1 is selected from the class consisting of ##STR2## R.sub.2 is an isomer of an aromatic dialdehyde selected from the class cisting of phthalaldehyde, naphthalene dialdehyde, phenanthrene dialdehyde, anthracene dialdehyde, biphenyl dialdehyde, terphenyl dialdehyde; and mixtures thereof and R.sub.3 is an isomer of an aromatic diamine selected from the class consisting of benzene diamine, naphthalene diamine, phenanthrene diamine, biphenyl diamine, and terphenyl diamine, and the cyano-condensation resins thereof which are useful in preparing semiconductors.
    Type: Grant
    Filed: October 20, 1977
    Date of Patent: September 26, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: James R. Griffith, Jacques G. O'Rear
  • Patent number: 4113646
    Abstract: Air revitalization compositions containing potassium superoxide which furr comprises from about 2 to about 10 weight percent of lithium monoxide, from about 0 to about 2 weight percent of silicon dioxide, and either from 5 to 10 weight percent of lithium metaborate or from 3 to 8 weight percent of calcium sulfate.
    Type: Grant
    Filed: April 25, 1977
    Date of Patent: September 12, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventor: Paul R. Gustafson
  • Patent number: 4104452
    Abstract: A vinyl polymer-fluoroalkylether oligomer composition useful as a structu material, filament, adhesive, or abhesive which comprises:A vinyl polymer selected from the class consisting of polyvinylchloride, polyvinylidene chloride, copolymers of vinylidene chloride and vinyl chloride, copolymers of vinylidene chloride and acrylonitrile in proportions in which vinylidene chloride is at least 70% by weight, polymethylmethacrylate, and polystyrene; and a fluoroalkylether oligomer of the general formula:F[C(CF.sub.3)F--CF.sub.2 --O].sub.m -- C(CF.sub.3)F--CO--Rwherein m is an integer from 4 to 10 and R is further defined by the formulas:OR.sup.1 (OR.sup.2).sub.n OR.sup.2 (1)wherein R.sup.1 is an alkyl radical having from 1 to 3 carbon atoms, R.sup.2 is an alkyl radical having from 1 to 3 carbon atoms, and n is an integer from 3 to 10,OR.sup.3 (2)wherein R.sup.3 is an alkyl having from 1 to 10 carbon atoms,N--(C.sub.p H.sub.2p OH).sub.2 (3)wherein p is an integer from 2 to 4,N (CH.sub.2).sub.q CH.sub.
    Type: Grant
    Filed: October 6, 1977
    Date of Patent: August 1, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventor: Marianne K. Bernett
  • Patent number: 4102873
    Abstract: Compounds of the general formula: ##STR1## wherein R.sub.1 is an isomer of phthalaldehyde; R.sub.2 is an isomer of an romatic dialdehyde selected from the class consisting of phthalaldehyde, naphthalene dialdehyde, phenanthrene dialdehyde, anthracene dialdehyde, biphenyl dialdehyde, terphenyl dialdehyde; and mixtures thereof and R.sub.3 is an isomer of an aromatic diamine selected from the class consisting of benzene diamine, naphthalene diamine, phenanthrene diamine, biphenyl diamine, and terphenyl diamine, and the cyano-condensation resins thereof which are useful in preparing semiconductors.
    Type: Grant
    Filed: October 20, 1977
    Date of Patent: July 25, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: James R. Griffith, Jacques G. O'Rear
  • Patent number: 4097317
    Abstract: Increasing the stability of composite energetic compositions containing ctalline high-energy nitrates or nitrites by the inclusion of saligenin into the composition.
    Type: Grant
    Filed: March 25, 1977
    Date of Patent: June 27, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Joel M. Schnur, Richard S. Miller, James P. Sheridan, A. D. Britt
  • Patent number: 4097294
    Abstract: A method for preparing ceramic material from a polymer which comprises selecting a polymer from the class consisting of poly(diorganosilanes), poly(haloorganosilanes), poly(carbosilanes), polysilazanes, polycarbocarboranes, and polyborazines; heating said polymer to a temperature from 700.degree. to 2000.degree. C at a rate of at most 100.degree. C/hr. in an inert atmosphere for at least one hour; and cooling to room temperature at a cooling rate which avoids thermal stresses.
    Type: Grant
    Filed: August 23, 1976
    Date of Patent: June 27, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Roy W. Rice, Kenneth J. Wynne, William B. Fox
  • Patent number: 4087583
    Abstract: Acrylic fibers coated with one or more manganese oxides; the use thereof to remove trace materials from liquids such as water; a method of preparation thereof which comprises soaking the fiber in alkali metal permanganate; and another method of preparation which comprises soaking the fiber in sequence in an alkali metal base, in manganese salt solution, and in an alkali metal base.
    Type: Grant
    Filed: March 5, 1976
    Date of Patent: May 2, 1978
    Inventor: Willard S. Moore
  • Patent number: 4087374
    Abstract: The improvement of the electrolytic and additive methods of coloring alkali fluoride crystals comprising the step of selecting an alkali fluoride crystal having the impurities of between 0 and 5 ppmA of OH; between 0 and 50 ppmA of one or more alkaline earth cations, of which between 0 and 10 ppmA Mg.sup.++ and between 0 and 10 ppmA Ca.sup.++ ; between 0 and 50 ppmA of non-fluorine halide anions; between 0 and 10 ppmA of SiF.sub.6.sup.= ; between 0 and 30 ppmA of other ions; and the method of preparing these crystals which comprises converting the alkali fluoride to alkali hydrofluoride, crystallizing and vacuum drying the alkali hydrofluoride crystals, regenerating the alkali fluoride by expelling hydrogen fluoride, and crystallizing the alkali fluoride.
    Type: Grant
    Filed: April 30, 1975
    Date of Patent: May 2, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Irwin Schneider, William C. Collins, Oscar Imber, Philipp H. Klein
  • Patent number: 4070463
    Abstract: A pharmaceutical composition for the prevention of motion sickness which prises two parts of promethazine hydrochloride and one part of 1-ephedrine sulfate.
    Type: Grant
    Filed: March 3, 1976
    Date of Patent: January 24, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventor: Ashton Graybiel
  • Patent number: 4069059
    Abstract: A dense and high temperature-oxidation-resistant ceramic prepared from silicon nitride and zirconium silicate in an amount from 3 to 15 weight percent of silicon nitride.
    Type: Grant
    Filed: June 11, 1976
    Date of Patent: January 17, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: William J. McDonough, Roy W. Rice
  • Patent number: 4067860
    Abstract: N,N'-bis(3,4-dicyanophenyl) alkanediamides of the general formula: ##STR1## wherein R = (CH.sub.2).sub.n-2 and (CH.sub.2).sub.x CH(CH.sub.3)(CH.sub.2).sub.y ; n = 3 to 20; x = 1 to 8; and y = 1 to 8, prepared by reacting 4-aminophthalonitrile with a saturated aliphatic dicarboxylic acid halide. These dinitriles readily polymerize through heating by themselves or with a metal or with a salt to form polyphthalocyanine resins, of the infinite molecular weight type which are useful as coatings, laminates, adhesives, filament windings, and castings. The general formulas for these polyphthalocyanine resins are: ##STR2## wherein R = (CH.sub.2).sub.n-2 and (CH.sub.2).sub.x CH(CH.sub.3)(CH.sub.2).sub.y ; n = 3 to 20; x = 1 to 8; and y = 1 to 8.
    Type: Grant
    Filed: July 23, 1976
    Date of Patent: January 10, 1978
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: James R. Griffith, Jacques G. O'Rear
  • Patent number: 4065509
    Abstract: The .beta.-methylation of 2,4-dicarba-closo-heptaborane-7 through the reaon of methyl chloride with the parent carborane in the presence of metal trichloride selected from the group consisting of aluminum chloride and ferric chloride in a methyl chloride-to-carborane mole ratio from 1:1 to 6:1 and a metal trichloride-to-carborane from 0.3:1 to 5:1 at a temperature from about 30.degree. C to about 60.degree. C and at a pressure of at least 50 psig.
    Type: Grant
    Filed: May 25, 1976
    Date of Patent: December 27, 1977
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Jerome F. Ditter, Eugene B. Klusmann
  • Patent number: 4057569
    Abstract: Compounds of the general formula: ##STR1## wherein R.sub.1 is selected from the class consisting of ##STR2## R.sub.2 is an isomer of an aromatic dialdehyde selected from the class cisting of phthalaldehyde, naphthalene dialdehyde, phenanthrene dialdehyde, anthracene dialdehyde, biphenyl dialdehyde, terphenyl dialdehyde; and mixtures thereof and R.sub.3 is an isomer of an aromatic diamine selected from the class consisting of benzene diamine, naphthalene diamine, phenanthrene diamine, biphenyl diamine, and terphenyl diamine, and the cyano-condensation resins thereof which are useful in preparing semiconductors.
    Type: Grant
    Filed: April 28, 1976
    Date of Patent: November 8, 1977
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: James R. Griffith, Jacques G. O'Rear
  • Patent number: 4056560
    Abstract: N,N'-bis(3,4-dicyanophenyl) alkanediamides of the general formula: ##STR1## wherein R = (CH.sub.2).sub.n-2 and (CH.sub.2).sub.x CH(CH.sub.3)(CH.sub.sub.y ; n = 3 to 20; x = 1 to 8; and y = 1 to 8, prepared by reacting 4-aminophthalonitrile with a saturated aliphatic dicarboxylic acid halide. These dinitriles readily polymerize through heating by themselves or with a metal or with a salt to form polyphthalocyanine resins, of the infinite molecular weight type which are useful as coatings, laminates, adhesives, filament windings, and castings. The general formulas for these polyphthalocyanine resins are: ##STR2## wherein R = (CH.sub.2).sub.n-2 and (CH.sub.2).sub.x CH(CH.sub.3)(CH.sub.2).sub.y ; n = 3 to 20; x = 1 to 8; and y = 1 to 8.
    Type: Grant
    Filed: July 23, 1976
    Date of Patent: November 1, 1977
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: James R. Griffith, Jacques G. O'Rear
  • Patent number: 4045408
    Abstract: Fluoro-anhydride curing agents for fluorinated epoxy resins, especially for highly fluorinated epoxy resins selected from the class consisting of hydroxyperfluoroalkyl phthalic anhydride, hydroxyperfluoroalkyl pyromellitic dianhydride, and mixtures thereof; a fluoro-anhydride curing agent for fluorinated epoxy resins that is the toluene-soluble mixture prepared by heating a hydroxyperfluoroalkyl benzenepentacarboxylic acid at about 240.degree. C; precursors for all of the curing agents; and the epoxy resins prepared therefrom.
    Type: Grant
    Filed: March 19, 1976
    Date of Patent: August 30, 1977
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: James R. Griffith, Jacques G. O'Rear