Abstract: A novel polycyano compound and method for the synthesis thereof comprising the reaction of triaminoguanidine with potassium cyanoformate in the presence of a mineral acid.
Type:
Grant
Filed:
July 25, 1968
Date of Patent:
September 21, 1976
Assignee:
The United States of America as represented by the Secretary of the Army
Abstract: A method for producing high density and high energy solid propellants conting of a solid inorganic oxidizing salt, a binder and a granular organic explosive comprising, the suspension of said ingredients in an organic solvent with agitation at ambient temperature to form a colloid, extruding the colloid, and raising the temperature to cure the grain, and the mixing of said propellant ingredients under vacuum, raising the temperature until a bulk viscosity of approximately 60,000 to 70,000 centipoises is reached, pouring said ingredients into a mold under vacuum, and curing the grains until the charge solidifies.
Type:
Grant
Filed:
January 11, 1968
Date of Patent:
March 9, 1976
Assignee:
The United States of America as represented by the Secretary of the Army
Abstract: The unidirectional solidification of a metal-ceramic composite in a system omprising the positioning of a seed crystal in a crucible, adding a portion of premelted ceramic material, a metallic material, and the remainder of the premelted ceramic. The temperature of the ceramic material is raised to about 50.degree.C above its melting point and then slowly decreased with a corresponding increase in the flow of an inert coolant gas through the system thereby unidirectionally solidifying the material to produce a single crystal having the orientation of the seed.
Type:
Grant
Filed:
February 15, 1974
Date of Patent:
February 17, 1976
Assignee:
The United States of America as represented by the Secretary of the Army
Inventors:
James W. McCauley, Dennis J. Viechnicki, Frederick Schmid