Abstract: A process separates a multicomponent feed by distillation into at least one stream enriched in the most volatile component, one stream enriched in the least volatile component, and one stream enriched in a component of intermediate volatility. In one embodiment, the process produces an argon-enriched stream from a cryogenic air separation process. The distillation system includes at least one distillation column that produces a nitrogen-enriched stream from the top of the column, an oxygen product stream from the bottom of the column, and an argon-enriched stream from a partitioned section. The geometry of the partitioned section minimizes vapor and liquid distribution, and includes a vertical separating element and an end separating element to isolate the partitioned section from the intermediate distillation section.