Abstract: The invention relates to a method for the production of calcium dipropionate by a batch process in a single pressure-resistant reaction vessel. The reaction vessel is charged with calcium oxide, calcium hydroxide, calcium carbonate or a mixture thereof. Then, pure high-concentrated propionic acid, preferably in a concentration of above 99% is added to the solid raw materials. The heat (up to 160° C.) and pressure (up to 10 bar) are retained in the reaction vessel and are subsequently used to discharge the reaction water after the complete amount of acid has been added. After a reaction time of 3 to 6 hours, pure calcium dipropionate with a water content of below 1% is obtained.
Type:
Grant
Filed:
July 6, 2016
Date of Patent:
March 26, 2019
Assignee:
Addcon Europe GMBH
Inventors:
Klaus Ederle-Lerch, Norman Killian, Bernd Kochannek, Hans-Jürgen Stüwe
Abstract: The invention relates to a solid-material method for producing calcium dipropionate in a pressure-resistant solid-state mixing reactor by charging calcium oxide, calcium hydroxide or calcium carbonate or mixtures of these calcium compounds, and adding propionic acid by a reaction directly in the solid phase under a pressure that is increased above normal pressure.
Type:
Application
Filed:
July 6, 2016
Publication date:
July 5, 2018
Applicant:
ADDCON EUROPE GMBH
Inventors:
Klaus EDERLE-LERCH, Norman KILLIAN, Bernd KOCHANNEK, Hans-Jürgen STÜWE