Abstract: Synthetic procedures to tetraalkyls, tetraacids and dianhydrides substituted 1,1,1-triaryl-2,2,2-trifluoroethanes which comprises: (1) 1,1-bis(dialkylaryl)-1-aryl-2,2,2-trifluoroethane, (2) 1,1-bis(dicarboxyaryl)-1-aryl-2,2,2-trifluoroethane or (3) cyclic dianhydride or diamine of 1,1-bis(dialkylaryl)-1-aryl-2,2,2-trifluoroethanes. The synthesis of (1) is accomplished by the condensation reaction of an aryltrifluoromethyl ketone with a dialkylaryl compound. The synthesis of (2) is accomplished by oxidation of (1). The synthesis dianhydride of (3) is accomplished by the conversion of (2) to its corresponding cyclic dianhydride. The synthesis of the diamine is accomplished by the similar reaction of an aryltrifluoromethyl ketone with aniline or alkyl substituted or disubstituted anilines. Also, other derivatives of the above are formed by nucleophilic displacement reactions.

Abstract: A catalyst for the combination of CO and O.sub.2 to form CO.sub.2 which includes a platinum group metal--e.g., platinum; a reducible metal oxide having multiple valence states--e.g., SnO.sub.2 ; and a compound which can bind water to its structure--e.g., silica gel. This catalyst is ideally suited for application to high-powered, pulsed, CO.sub.2 lasers operating in a sealed or closed-cycle condition.

Abstract: A sensing device 50 comprising an O.sub.2 sensor 22, a pump 37, a compressor 19, and a heater 21 is provided to quickly sense the amount of O.sub.2 in a combustion product gas. A sample of the combustion product gas is compressed to a pressure slightly above one atmosphere by compressor 19. Next, heater 21 heats the sample between 800.degree. C. and 900.degree. C. Next, pump 37 causes the sample to be flushed against electrode 32 located in O.sub.2 sensor 22 6000 to 10,000 times per second. Reference air at approximately one atmosphere is provided to electrode 31 of O.sub.2 sensor 22. Accordingly, O.sub.2 sensor 22 produces a voltage which is proportional to the amount of oxygen in the combustion product gas. This voltage may be used to control the amount of O.sub.2 entering into the combustion chamber 10 which produces the combustion product gas.

Abstract: In a list processing system, small reference counters are maintained in conjunction with memory cells for the purpose of identifying memory cells that become available for re-use. The counters are updated as references to the cells are created and destroyed, and when a counter of a cell is decremented to logical zero the cell is immediately returned to a list of free cells. In those cases where a counter must be incremented beyond the maximum value that can be represented in a small counter, the cell is restructured so that the additional reference count can be represented. The restructuring involves allocating an additional cell, distributing counter, tag, and pointer information among the two cells, and linking both cells appropriately into the existing list structure.

Abstract: The gaseous phase is detected and then separated from a liquid phase in a fluid. This is accomplished by centrifuging the liquid phase while the gaseous phase migrates to the axis. When the expected phase is detected at a predetermined port, a signal is generated to open the liquid or gas valve at the respective outlet ports and to modulate these valves in such a manner as to withdraw fluid at the same volume rate at which it is admitted.

Abstract: A material 11 is protected from acoustic shock waves generated by impacting projectiles by means of a backing 12. Backing 12 has an acoustic impedance that efficiently couples the acoustic energy out of the material 11.

Abstract: The invention described herein relates to an apparatus for providing a selectively humidified gas to a camera canister (12) containing cameras and film used in space. A source of pressurized gas (leak test gas 26 or motive gas 21) is selected by a valve (30), regulated to a desired pressure by a regulator (34), and routed through an ejector (46) (venturi device). A regulated source of water vapor in the form of steam from a heated reservoir (18) is coupled to a low pressure region (50) of the ejector (46) which mixes with high velocity gas flow through the ejector (46). This mixture is sampled by a dew point sensor (14) to obtain dew point thereof (ratio of water vapor to gas) and the apparatus adjusted by varying gas pressure or water vapor to provide a mixture at a connector (78) having selected humidity content.

Abstract: Disclosed is an interdigitated plate-type heat exchanger interface. The interface includes a modular interconnect to thermally connect a pair or pairs of plate-type heat exchangers to a second single or multiple plate-type heat exchanger. The modular interconnect comprises a series of parallel, plate-type heat exchangers arranged in pairs to form a slot therebetween. The plate-type heat exchangers of the second heat exchanger insert into the slots of the modular interconnect. Bellows are provided between the pairs of fins of the modular interconnect so that when the bellows are pressurized, they drive the plate-type heat exchangers of the modular interconnect toward one another, thus closing upon the second heat exchanger plates. Each end of the bellows has as a part thereof a thin, membrane diaphragm which readily conforms to the contours of the heat exchanger plates of the modular interconnect when the bellows is pressurized.

Abstract: The invention is an improvement in a lightweight carbon-carbon composite piston, the improvement comprehending the use of near-net shape knitted or warp-interlock pre-forms to improve the structural qualitites of the piston. In its preferred embodiment, a one piece, tubular, closed-ended, knitted pre-form (a sock) of carbon fibers (11) embedded within the matrix of the piston structure forms the crown (12), side wall (15), skirt (16) and inner surface (18) of the piston, and wrap-interlock pre-forms strengthen the piston crown and wrist pin bosses.

Abstract: A steam reformer is disclosed having an annular steam reforming catalyst bed formed by concentric cylinders and having a catalytic combustor located at the center of the innermost cylinder. Fuel is fed into the interior of the catalytic combustor and air is directed at the top of the combustor, creating a catalytic reaction which provides sufficient heat so as to maintain the catalytic reaction in the steam reforming catalyst bed. Alternatively, air is fed into the interior of the catalytic combustor and a fuel mixture is directed at the top. The catalytic combustor provides enhanced radiant and convective heat transfer to the reformer catalyst bed.

Abstract: The invention relates to a process for crosslinking aromatic polymers containing radiation-sensitive methylene groups (--CH.sub.2 --) by exposing the polymers to ionizing radiation thereby causing crosslinking of the polymers through the methylene groups. Crosslinked polymers are resistant to most organic solvents such as acetone, alcohols, hydrocarbons, methylene, chloride, chloroform, and other halogenated hydrocarbon, to common fuels and to hydraulic fluids in contrast to readily soluble uncrosslinked polymers. In addition, the degree of crosslinking of the polymers depends upon the percentage of the connecting groups which are methylene which ranges from 5 to 50% and preferably from 25 to 50% of the connecting groups and is also controlled by the level of irradiation which ranges from 25 to 1000 Mrads and preferably from 25 to 250 Mrads. The temperature of the reaction conditions ranges from 25.degree. to 200.degree. C. and preferably at or slightly above the glass transition temperature of the polymer.

Abstract: A yeast strain with high power to produce alcohol by fermentation is produced by a method comprising directly conjugating the haploid of the strain No. 909-1 with each tetrad of the ascospores of the strain No. 180 by spore-to-cell mating, acclimating the resultant zygote in the medium of waste after alcohol fermentation, and acclimating the surviving cells of the zygote in the medium of the beet molasses containing 2-deoxyglucose. The yeast strain produced is designated as Strain M-9 (FERM BP 1481) of genus Saccharomyces cerevisiae. Alcohol is produced by culturing the Strain M-9 in a medium of beet molasses.

Abstract: An apparatus is disclosed for allowing mixing of solutions in low gravity environments so as to carry out crystallization of proteins and other small molecules or other chemical syntheses, under conditions that maximize crystal growth and minimize disruptive turbulent effects. The apparatus is comprised of a housing, a plurality of chambers, and a cylindrical rotatable valve disposed between at least two of the chambers, said valve having an internal passageway so as to allow fluid movement between the chambers by rotation of the valve. In an alternate embodiment of the invention, a valve is provided having an additional internal passageway so that fluid from a third chamber can be mixed with the fluids of the first two chambers. This alternate embodiment of the invention is particularly desirable when it is necessary to provide a termination step to the crystal growth, or if a second synthetic step is required.

Abstract: Polyphenylquinoxalines are prepared by the nucleophilic displacement reaction of di(hydroxyphenyl)quinoxaline monomers with activated aromatic dihalides or dinitro compounds. The reactions are carried out in polar aprotic solvents using alkali metal bases at elevated temperatures under nitrogen. The di(hydroxyphenyl)quinoxaline monomers are prepared either by reacting stoichiometric quantities of aromatic bis(o-diamines) with a hydroxybenzil or by reacting o-phenylenediamine with a dihydroxybenzil or bis(hydroxyphenylglyoxylyl)benzene.

Abstract: An image difference detection system is described, of the type wherein two created image representations such as transparencies representing the images to be compared lie coplanar, while light passes through the two transparencies and is formed into coincident images at the image plane for comparison. The two transparencies are formed by portions of a polarization rotation spacial light modulator display such as a multi-pixel liquid crystal display or a magneto optical rotation type. In a system where light passing through the two transparencies is polarized in transverse directions to enable the use of a Wollaston prism to bring the images into coincidence, a liquid crystal display can be used which is devoid of polarizing sheets that would interfere with transverse polarizing of the light passing through the two transparencies.

Abstract: A concatenated coding system consisting of a (255,223) Reed-Solomon outer code and a convolutional inner code is provided with either a block of preinterleaved frames or an interleaver of frames in a block of data symbols to be coded in the outer decoder. By interleaving, errors are constrained to occur in only one symbol in a frame, which can be corrected by the Reed-Solomon outer decoder. After transmission and inner decoding, the data symbols are deinterleaved for outer decoding. Instead of preinterleaving at the source, or interleaving before inner encoding, the frames of data symbols may be interleaved at the receiver after inner decoding and then combined with the inner decoded check symbols for outer decoding. The outer encoder is a bit-serial Reed-Solomon encoder with programmable interleaving, and the inner decoder is a Viterbi decoder.

Abstract: A simple electrostatically enhanced fabric filtration system for removing fine particulate matter or dust entrained in a gas flow, has a single, elongate, central, corona-generating electrode positioned within a cylindrical fabric filter, closed at one end, into which the particulate bearing gas flow is directed. In one embodiment, a grid-like cylindrical grounded electrode is disposed proximately outside the filter element and establishes a radially directed electrostatic field with the corona electrode. Particles passing through the corona acquire charges of like polarity and are subjected immediately to Coulombic forces driving them radially outward toward the filter fabric where they collect prominently near the filter element inlet, thus allowing easier passage to the gas further downstream. Other embodiments have a plurality of grounded electrodes attached to the inside of the filter element or as wires woven therethrough. Corona concentration near the filter element entrance by known techniques, e.g.

Abstract: A single step is relied on in the canning process for hot isostatic pressing powder metallurgy composites. The binders are totally removed while the HIP can of compatible refractory metal is sealed at high vacuum and temperature. This eliminates out-gassing during hot isostatic pressing.

Abstract: An aerobraking orbital transfer vehicle (AOTV) (80) has aerobrake (82) with a blunted raked-off circular-cone configuration. The other components of the AOTV, including command/control module (95), fuel tanks (86, 88, 89 and 91), rocket engines (94) and afterbody (84), are positioned substantially along resultant force axis (104) of the AOTV (80). The axis (104) coincides with the resultant (sum of lift and drag) force vector. Afterbody (84) is mounted behind the aerobrake (82) with its length extending rearwardly from the aerobrake. The base flow clearance angle .phi. of the aerobrake (80) is 25.degree., thus allowing the afterbody (84) to extend rearwardly from the aerobrake (82) to a much greater extent than possible with a raked-off elliptic-cone aerobraking shield configuration.

Abstract: An octapeptide of the formula: ##STR1## wherein each A.sub.1 and A.sub.2, independently, is H, C.sub.1-12 alkyl, C.sub.7-10 phenylalkyl, R.sub.1 CO (where R.sub.1 is C.sub.1-20 alkyl, C.sub.3-20 alkenyl, C.sub.3-20 alkinyl, phenyl, naphthyl, or C.sub.7-10 phenylalkyl), or R.sub.2 OCO (where R.sub.2 is C.sub.1-10 alkyl or C.sub.7-10 phenylalkyl), provided that when one of A.sub.1 or A.sub.2 is R.sub.1 CO or R.sub.2 OCO, the other must be H; A.sub.3 is CH.sub.2 -A.sub.6 (where A.sub.6 is pentafluorophenyl, naphthyl, pyridyl, or phenyl); A.sub.4 is o- m- or p-substituted X-Phe (where X is a halogen, H, NO.sub.2, OH, NH.sub.2, or C.sub.1-3 alkyl), pentafluoro-Phe, or .beta.-Nal; A.sub.5 is Thr, Ser, Phe, Val, .alpha.-aminobutyric acid, or Ile, provided that when A.sub.3 is phenyl, A.sub.1 is H, and A.sub.2 is H, A.sub.5 cannot be Val; and A.sub.7 is Thr, Trp, or .beta.-Nal; or a pharmaceutically acceptable salt thereof.