Patents Assigned to Arkenol, Inc.
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Patent number: 6054611Abstract: A method of producing dehydration products from one more 5-carbon or 6-carbon sugars includes reacting said one or more sugars at 40-240.degree. C. for 1 to 96 hours in the presence of 5-90% sulfuric acid, separating the reaction products, and recovering levulinic acid. The sugars are can be generated from strong acid hydrolysis of biomass, such as rice straw, paper, cotton and other cellulosic materials.Type: GrantFiled: May 13, 1998Date of Patent: April 25, 2000Assignee: Arkenol, Inc.Inventors: William A. Farone, John E. Cuzens
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Patent number: 5892107Abstract: A method of producing dehydration products from one or more 5-carbon or 6-carbon sugars includes reacting said one or more sugars at 40.degree.-240 .degree. C. for 1 to 96 hours in the presence of 10-90% sulfuric acid, separating the reaction products, and recovering levulinic acid. The sugars can be generated from strong acid hydrolysis of biomass, such as rice straw, paper, cotton and other cellulosic materials.Type: GrantFiled: November 8, 1996Date of Patent: April 6, 1999Assignee: Arkenol, Inc.Inventors: William A. Farone, John E. Cuzens
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Patent number: 5820687Abstract: A economically viable method for producing sugars using concentrated acid hydrolysis of biomass containing cellulose and hemicellulose is disclosed. The cellulose and hemicellulose in the biomass is first decrystallized and then hydrolyzed to produce a hydrolysate containing both sugars and acid. Silica present in the biomass can then be removed for further processing. The remaining solids are then subjected to a second decrystallization and hydrolyzation to optimize the sugar yields. An improved method for separating the sugars from the acid in the hydrolysate is also disclosed. The resulting sugar stream can then be fermented, using an improved method which allows both hexose and pentose sugars to be fermented simultaneously.Type: GrantFiled: June 13, 1996Date of Patent: October 13, 1998Assignee: Arkenol, Inc.Inventors: William A. Farone, John E. Cuzens
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Patent number: 5782982Abstract: A method of removing silica or silicates from solids results from the acid hydrolysis of materials containing cellulose and hemicellulose is disclosed. The method includes the steps of treating the solids with a metal hydroxide solution to produce an extract, reducing the pH of the extract to produce silicic acid, and removing the silicic acid from the extract.Type: GrantFiled: June 7, 1995Date of Patent: July 21, 1998Assignee: Arkenol, Inc.Inventors: William A. Farone, John E. Cuzens
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Patent number: 5726046Abstract: A economically viable method for producing sugars using concentrated acid hydrolysis of biomass containing cellulose and hemicellulose is disclosed. The cellulose and hemicellulose in the biomass is first decrystallized and then hydrolyzed to produce a hydrolysate containing both sugars and acid. Silica and silicates present in the biomass can then be removed for further processing. The remaining solids are then subjected to a second decrystallization if necessary and a second hydrolyzation to optimize the sugar yields.Type: GrantFiled: July 2, 1996Date of Patent: March 10, 1998Assignee: Arkenol, Inc.Inventors: William A. Farone, John E. Cuzens
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Patent number: 5620877Abstract: An economically viable method of fermenting a mixture of sugars resulting from the acid hydrolysis of material containing cellulose and hemicellulose allows for the simultaneous fermentation of both pentose and hexose sugars. The sugar solution is mixed with a microbial organism known to produce a useful fermentation product, and the fermentation process is allowed to proceed for 3-5 days, during and after which the fermentation products are removed and purified.Type: GrantFiled: June 6, 1995Date of Patent: April 15, 1997Assignee: Arkenol, Inc.Inventors: William A. Farone, John E. Cuzens
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Patent number: 5597714Abstract: A economically viable method for producing sugars using concentrated acid hydrolysis of biomass containing cellulose and hemicellulose is disclosed. The cellulose and hemicellulose in the biomass is first decrystallized and then hydrolyzed to produce a hydrolysate containing both sugars and acid. Silica and silicates present in the biomass can then be removed for further processing. The remaining solids are then subjected to a second decrystallization if necessary and a second hydrolyzation to optimize the sugar yields.Type: GrantFiled: June 7, 1995Date of Patent: January 28, 1997Assignee: Arkenol, Inc.Inventors: William A. Farone, John E. Cuzens
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Patent number: 5580389Abstract: A economically viable method for producing sugars using concentrated acid hydrolysis of biomass containing cellulose and hemicellulose is disclosed. The cellulose and hemicellulose in the biomass is first decrystallized and then hydrolyzed to produce a hydrolysate containing both sugars and acid. Silica present in the biomass can then be removed for further processing. The remaining solids are then subjected to a second decrystallization and hydrolyzation to optimize the sugar yields. An improved method for separating the sugars from the acid in the hydrolysate is also disclosed. The resulting sugar stream can then be fermented, using an improved method which allows both hexose and pentose sugars to be fermented simultaneously.Type: GrantFiled: June 6, 1995Date of Patent: December 3, 1996Assignee: Arkenol, Inc.Inventors: William A. Farone, John E. Cuzens
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Patent number: 5562777Abstract: A economically viable method for producing sugars using concentrated acid hydrolysis of biomass containing cellulose and hemicellulose is disclosed. The cellulose and hemicellulose in the biomass is first decrystallized and then hydrolyzed to produce a hydrolysate containing both sugars and acid. Silica present in the biomass can then be removed for further processing. The remaining solids are then subjected to a second decrystallization and hydrolyzation to optimize the sugar yields. An improved method for separating the sugars from the acid in the hydrolysate is also disclosed. The resulting sugar stream can then be fermented, using an improved method which allows both hexose and pentose sugars to be fermented simultaneously.Type: GrantFiled: March 26, 1993Date of Patent: October 8, 1996Assignee: Arkenol, Inc.Inventors: William A. Farone, John E. Cuzens