Abstract: A process for monoalkylating diphenylamine using a clay catalyst is disclosed which results in a reaction product having substantial amounts of desirable monoalkylated diphenylamine and minimal amounts of less desirable disubstituted diphenylamine and unsubstituted diphenylamine. The disclosed process uses clay catalysts which favor monoalkylation over dialkylation and specific conditions such as reaction temperature, mole ratios of alkylating olefin to diphenylamine, reaction times, and catalyst amounts. Preferred olefins are diisobutylene and linear alpha olefins having from 6 or 8 to 18 carbon atoms. When more than 1 wt. % residual unreacted diphenylamine is present it may be converted to alkylated diphenylamine by reacting with styrene, alpha-methylstyrene or isobutylene.

Abstract: A composition for use as a de-icing fluid comprising a glycol based aqueous solution thickened with about 0.01 to about 5.0% by weight of a cross-linked hydrophobically modified copolymer of an acrylic acid which has a Brookfield mucilage viscosity of at least 25,000 cP at 0.5% by weight polymer dosage, a holdover time of at least 60 minutes, a shear thinning index of at least 20, and a shear loss of less than 15% and acceptable aerodynamic performance.

Abstract: A method for polymerizing at least one unsaturated monomer in the presence of a latex results in a high solids dispersion of polymer particles with lower viscosities than traditionally observed. A significant wt. % of the polymer from added monomers can be present in large particles, having nonspherical shapes. Some of the original latex particles are retained during the polymerization and these increase the solids content and lower the viscosity by packing in the interstices between large particles. The total polymer solids content can easily be varied from 70 to 92 or more wt. %. The viscosities at very high solids contents become paste-like but the materials still are stable to storage and further handling without causing the dispersion to separate into an agglomerated polymer portion and released water. The dispersions are useful to form sealants, membranes, etc., either with or without other additives.

Abstract: Addition polymers derived from norbornene-functional monomers are terminated with an olefinic moiety derived from a chain transfer agent selected from a compound having a terminal olefinic double bond between adjacent carbon atoms, excluding styrenes, vinyl ethers, and conjugated dienes and at least one of said carbon atoms has two hydrogen atoms attached thereto. The addition polymers of this invention are prepared from a single or multicomponent catalyst system including a Group VIII metal ion source. The catalyst systems are unique in that they catalyze the insertion of the chain transfer agent exclusively at a terminal end of the polymer chain.

Abstract: The invention relates to the field of needling processes for forming fibrous preform structures. The invention is particularly useful in forming fibrous preform structures suitable for subsequent processing into high temperature resistant composite structures such as carbon/carbon aircraft brake disks. The process according to the invention compensates for fiber pull back induced by fiber resilience, and for compaction in previously needled layers induced during subsequent needling passes. According to a further aspect of the invention, Z-fiber distribution throughout the thickness of the fibrous preform structure may be manipulated as necessary to achieve a desired distribution.

Abstract: An inflation system for use in inflating an inflatable foldable escape slide or foldable container for use in evacuating personnel from an aircraft, platform or other device in cases of emergencies. The slide has a gas source such as a bottle member having pressurized fluids therein or as a solid fuel propellant which upon actuation directs pressurized fluids to a turbocharger fastened onto the escape slide or foldable container. The turbocharger has a turbine at one end of a shaft driven by the pressurized fluids to drive such shaft that has a plurality of centrifugal compressors mounted on the other end of the shaft whereby the exhaust fluids from the turbine and the pressurized gas resulting from the driving of the compressors unite to inflate the escape slides or foldable container.

Abstract: A carbon/carbon composite having an oxidation protection outer coating system comprising a coating of a glass, a coating of a ceramic, and a wrap of a ceramic containing fabric.

Abstract: A deployment control for an inflatable escape slide for use in a structure such as an aircraft is disclosed wherein the escape slide has an inboard end and an toe end. The inboard end of the slide is suitably attached to an egress on the structure for deployment and extension of the slide by inflation means whereby the slide extends from an elevated egress to a ground support. The slide has inflatable tubes with a slide surface. The inflation means is operative upon actuation to provide pressurized fluids to the tubes which will inflate and distend the tubes into a longitudinally extending escape slide under the control of a restraining control device (or devices). Such device is operative upon pressurization of the tubes to deploy an outboard portion of the slide to which one end of the device is connected to move relative to the inboard end of the slide to which the other end of the device is connected at a controlled rate for a predetermined length of the slide.

Abstract: A friction disk assembly comprises an annular structural carrier including a plurality of recessed and/or raised regions and torque drive notches spaced around its circumferential direction, and a segmented friction lining mounted on the carrier. Each segment of the friction lining comprises a clamshell-shaped friction cup including a pair of cup members containing a puck of friction material, each pair of cup members being joined by a deformable strap and together defining a U-shaped configuration. The obverse side of each cup member includes projections and/or depressed areas that are complementary in size, shape and location to the recessed and/or raised regions of the associated carrier operatively engaged therewith to prevent movement of the lining relative to the carrier during a braking event. The carrier may be formed of steel or other suitable structural material. The lining may be formed of suitable friction material, e.g. sintered metal.

Abstract: The invention relates to a propeller ice protection system having more evenly distributed sliding contact wear resulting in reduced maintenance, and a method of operating the system. According to the invention, polarity of a DC potential applied to the sliding contacts is periodically reversed in order to more evenly distribute brush wear. Specific hardware embodiments and various polarity reversing schemes are disclosed.

Abstract: A continuous process for the solution polymerization of appropriate polycycloolefins in a ROMP zone to obtain a processable ROMP homo- or copolymer in solution, and subsequent hydrogenation of the ROMP (co)polymer without removing the residual ROMP catalyst and co-catalyst, provides an optical product having a mol wt M.sub.w in the range from 50,000-300,000 and polydispersity M.sub.w /M.sub.n in the range from 1.3-5.0, more preferably from 1.3-3, the lower the polydispersity the more desirable the physical properties of the (co)polymer.

Abstract: A coating composition for use as an overcoat or heat resistant coating having improved heat resistance comprised of an aqueous latex polymer emulsion and a water soluble or water-dispersible resin which containing a sufficient number of either (a) carboxyl groups or (b) carboxyl and amide groups which will form at least one anhydride ring or imide, in the presence of sufficient heat, and release water molecules, with the latex polymer having a particle size of less than about 1600 Angstroms and containing an effective amount of a nitrogen containing volatile base to achieve a pH of greater than about 7.5 to keep the resin solubilized or dispersed.

Abstract: The invention discloses methods of preparing copolymers from norbornene-type monomers and cationically polymerizable monomers or polymers from catalytically polymerizable monomers by employing Group VIII transition metal ion source in a solvent for said monomers at a temperature in the range from -100.degree. C. to 120.degree. C. Also disclosed are copolymers from norbornene-type monomers and catalytically polymerizable monomers.

Abstract: Fibrous substrates for the production of carbon and/or ceramic (including mixtures of these) fiber reinforced carbon and/or ceramic (including mixtures of these) composites and to methods of manufacture of same. A shaped fibrous structure comprising at least a first fibrous tape layer of a width generally corresponding to that of the fibrous structure to be formed, the first fibrous tape layer superposed upon and joined to least one other fibrous layer by needlepunching to produce cross-linking of the layers by fibers displaced out of the layers and extending in a direction generally perpendicular to the faces of the layers, and methods of making same.

Abstract: A de-icing system is provided including a de-icer attached to an aircraft structural member subjected to an impinging airstream during flight, the airstream passing over the structural member in a fore to aft direction. The deicer has a primary heater element disposed beneath a primary shedding zone upon which ice accumulates during flight, the primary heater element being configured to heat the primary shedding zone upon application of an electrical potential across the primary heater element, and a secondary heater element disposed beneath a secondary shedding zone upon which ice accumulates during flight, the secondary heater element being configured to heat the secondary shedding zone upon application of an electrical potential across the secondary heater element, the secondary heater element being disposed immediately aft of the primary heater element.

Abstract: The present invention relates to a method for inhibiting the formation and deposition of silica and silicate compounds in water systems by the use an effective amount of a polymer or copolymer having the following structure: ##STR1## wherein A is the initiator radical from free radical polymerization, such as for example, alkoxy, acyloxy, hydroxyl, alkyl or sulfonate radicals from peroxide initiators, or cyanoalkyl radicals from azonitrile initiators, or n-alkythio or tetrahydrofuranyl radicals from common transfer agents, R.sub.1 and R.sub.2 are alkyl groups which contain a combined total of 2 to 4 carbon atoms or R.sub.1 and R.sub.2 together with the nitrogen atom comprise a ring containing 3 to 5 carbon atoms, R.sub.3 is either H or a C.sub.1 through C.sub.

Abstract: In a marine vessel having a drive shaft that extend rearwardly from its hull, wherein the drive shaft has a coupling and a bearing assembly along its length that are supported by struts, which struts are also secured to the hull of the vessel. A coupling cover encompasses the coupling and is mounted adjacent to a bearing assembly. A fairwater encompasses the coupling cover and is attached to the bearing assembly or the strut associated therewith to define a chamber and a clearance space between the fairwater and the coupling cover for directing fluids therethrough and through the bearing assembly to lubricate such bearing assembly. Vanes are located on the coupling cover or on a separate support located within such chamber to enhance the fluid flow through the bearing assembly.

Abstract: Blends of chlorinated polyvinyl chloride and chlorinated polyethylene and methods for preparing extruded profiles such as a window spacer, a glazing bead, a window lineal, and a track for lighting, having smooth surface characteristics are disclosed. The blends comprise 100 weight parts CPVC containing from 62% to 72% chlorine, preferably 65% to 71% chlorine and from 10 to 30 weight parts, preferably 15 to 25 parts of chlorinated polyethylene containing from 25 to 45% chlorine and extruding the blend. The preferred embodiments of the invention are further defined by a particular combination for the chlorine content of CPVC, the real weight average molecular weight of CPE (M.sub.w) and polydispersity (M.sub.w /M.sub.n), defined as the ratio of the weight average to number average molecular weight, and extrusion shear rate.

Abstract: An improved sliding contact for use with a propeller ice protection system is provided. According to an aspect of the invention, a silver graphite brush forms a sliding contact with a hardened copper alloy slip ring. A sliding contact according to the invention demonstrates improved performance in an oil contaminated environment.

Abstract: An aerodynamic air data sensing probe adapted for mounting to an air vehicle and capable of generating signals related to a fluid flowing relative to the air vehicle. A fluid inlet positioned on a first end of the strut faces generally transverse to the fluid flow selectively admits fluid to an internal strut cavity due to a pressure differential thereacross. In operation, the pressure differential forms between the first end surface of the aerodynamically-shaped, forward-inclined strut and probe exhaust ports. A temperature sensing element disposed in the internal strut cavity registers the temperature of the fluid and the sensed fluid is expelled from the internal strut cavity through the exhaust ports. In another embodiment, a barrel-shaped probe head adapted to sense fluid pressure connects to a portion of the leading edge of the strut to form an aerodynamic multifunction air data sensing probe.