Publication number: 20200144594
Abstract: A process for making a cathode active material for a lithium ion battery is described. The process includes (a) a step of synthesizing a mixed oxide of formula Li1+xTM1?xO2 at a temperature ranging from 750 to 1000° C. in an oxidizing atmosphere, where TM is a combination of two or more transition metals of Mn, Co and Ni and, optionally, at least one more metal of Ba, Al, Ti, Zr, W, Fe, Cr, K, Mo, Nb, Mg, Na and V, and x is a number ranging from zero to 0.2, (b) a step of cooling down the material obtained from step (a) to a temperature ranging from 100 to 400° C., (c) a step of adding at least one reactant of BF3, SO2 and SO3 at the temperature of 100 to 400° C., and (d) a step of cooling down to a temperature of 50° C. or below.
Type:
Application
Filed:
June 22, 2018
Publication date:
May 7, 2020
Applicant:
BASF SE
Inventors:
Michael METZGER, Hans BEYER, Johannes SICKLINGER, Daniel PRITZL, Benjamin STREHLE, Hubert GASTEIGER, Hadar SCLAR, Evan ERICKSON, Francis Amalraj SUSAI, Judith GRINBLAT, Doron AURBACH, Boris MARKOVSKY
Patent number: 10633328
Abstract: This invention relates to polyetheramines based on 1,3-dialcohols, in particular to an etheramine mixture comprising at least 90% by weight, based on the total weight of the etheramine mixture, of anamine of Formula (I) and/or (II), wherein R1-R12 are independently selected from H, alkyl, cycloalkyl, aryl, alkylaryl, or arylalkyl, wherein at least one of R1-R6 and at least one of R7-R12 is different from H, wherein A1-A9 are independently selected from linear or branched alkylenes having 2 to 18 carbon atoms, preferably 2-10 carbon atoms, most preferably 2-5 carbon atoms, wherein Z1-Z4 are independently selected from OH or NH2, wherein at least one of Z1-Z2 and at least one of Z3-Z4 is NH2, and wherein the sum of x+y is in the range of from 2 to 200, wherein x?1 and y?1; and x1+y1 is in the range of from 2 to 200, preferably 2-20, most preferably 2-10, wherein x1?1 and y1?1.
Type:
Grant
Filed:
March 27, 2014
Date of Patent:
April 28, 2020
Assignee:
BASF SE
Inventors:
Sophia Ebert, Björn Ludolph, Christof W. Wigbers, Steffen Maas, Frank Huelskoetter, Stefano Scialla, Dieter Boeckh, Kevin Christmas, Amy Eichstadt Waun, Brian J. Loughnane, Darren Rees, Christian Eidamshaus, Monika Charrak, Alexander Panchenko