Patents Assigned to Battelle
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Patent number: 11839852Abstract: Systems and methods for efficient, effective, and safe separation and isolation of multiple isotopes (e.g., Mo, Zr, Ba, Sr, Te, and lanthanide isotopes) from fission products includes use of a plurality of chromatography columns, each containing a chromatographic resin formulated to target one or more particular isotopes. The system is operable in a “series” configuration to load the multiple columns by a single pass of the sample. Then, the system may be transitioned (e.g., using valves) to a “parallel” configuration in which multiple columns of the system may be operated simultaneously to elute targeted isotopes. Additional parallel operations of the columns, using different eluent compositions, may be used to elute different targeted isotopes. The system may be reconditioned in preparation for a subsequent sample.Type: GrantFiled: January 21, 2021Date of Patent: December 12, 2023Assignee: Battelle Energy Alliance, LLCInventors: Mathew S. Snow, Jessica L. Ward
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Patent number: 11826551Abstract: Autoinjectors and methods of injection are described that feature release mechanisms and/or end-of-dose sound which can operate in conjunction with a powered plunger to efficiently inject a controlled dose from a syringe.Type: GrantFiled: April 9, 2020Date of Patent: November 28, 2023Assignee: Battelle Memorial InstituteInventors: William G. Atterbury, Steve Madland, Adam Fox, Steven E. Huckaby, Jake Pyzza
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Patent number: 11826187Abstract: Systems and methods that directly image attenuation-based object grid, use a source grid to improve imaging of the object grid using a high-energy polychromatic source, and use a detector grid having gratings oriented substantially orthogonally to that of the object grid, can address artifacts and beam hardening effects that limit the quality and discriminatory power of high-energy x-ray imaging that includes phase contrast.Type: GrantFiled: March 20, 2020Date of Patent: November 28, 2023Assignee: Battelle Memorial InstituteInventors: Erin A. Miller, Richard E. Jacob, Nikhil S. Deshmukh, Cynthia L. Warner, Richard S. Wittman, Luke W. Campbell
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Patent number: 11827757Abstract: A carbon fiber composite material comprising: (i) a carbon fiber having an outer surface, a thickness of at least 1 micron, and an aspect ratio of at least 1000; (ii) a sizing agent coated on the outer surface of the carbon fiber, wherein the sizing agent has a thickness of up to 200 nm; and (iii) nanoparticles having a size in at least one dimension of up to 100 nm embedded within the sizing agent, wherein the nanoparticles have a metal carbide, metal oxide, metal nitride, and/or metal boride composition. A method for producing the fiber composite material comprises: (a) continuously feeding and coating a continuous carbon fiber with a liquid containing a solvent, sizing agent, and nanoparticles in a continuous feed-through process to result in said sizing agent and nanoparticles coating the surface of the continuous carbon fiber; and (b) removing the solvent from the coated fiber.Type: GrantFiled: February 20, 2019Date of Patent: November 28, 2023Assignee: UT-Battelle, LLCInventors: Christopher C. Bowland, Amit K. Naskar
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Patent number: 11827955Abstract: Nickel alloys, methods of making nickel alloys, articles including the nickel alloys, uses of the alloys, and methods of treating nickel alloys are described. The inventive heat resistant structural materials are suitable for applications requiring high yield stress at room temperature and good creep strength at high temperatures, such as in gas turbines, steam turbines, fossil energy boilers, aero engines, power generation systems using fluids such as supercritical carbon dioxide (e.g., advanced ultra-supercritical power plants), concentrated solar power plants, nuclear power plants, molten salt reactors: turbine blades, casings, valves, heat exchangers and recuperators.Type: GrantFiled: October 27, 2021Date of Patent: November 28, 2023Assignee: Battelle Memorial InstituteInventors: Martin Detrois, Paul D. Jablonski, Jeffrey A. Hawk
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Publication number: 20230378543Abstract: Electrolytes for lithium ion batteries with carbon-based, silicon-based, or carbon- and silicon-based anodes include a lithium salt; a nonaqueous solvent comprising at least one of the following components: (i) an ester, (ii) a sulfur-containing solvent, (iii) a phosphorus-containing solvent, (iv) an ether, (v) a nitrile, or any combination thereof, wherein the lithium salt is soluble in the solvent; a diluent comprising a fluoroalkyl ether, a fluorinated orthoformate, a fluorinated carbonate, a fluorinated borate, a fluorinated phosphate, a fluorinated phosphite, or any combination thereof, wherein the lithium salt has a solubility in the diluent at least 10 times less than a solubility of the lithium salt in the solvent; and an additive having a different composition than the lithium salt, a different composition than the solvent, and a different composition than the diluent. In some electrolytes, the nonaqueous solvent comprises an ester.Type: ApplicationFiled: May 31, 2023Publication date: November 23, 2023Applicant: Battelle Memorial InstituteInventors: Xia Cao, Ji-Guang Zhang, Wu Xu
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Patent number: 11815376Abstract: A system for measuring gas flow generally including a passive acoustic wave generator disposed in a gas flow stream to passively generate an audio signal through vortex shedding, a sound capturing instrument disposed outside the gas stream to produce an electrical signal representative of the acoustic signal, a temperature sensor to obtain temperature measurements indicative of the temperature of the gas flow stream and a control system for determining the gas flow, such as velocity or flow rate, as a function of the acquired acoustic and temperature measurements. The acoustic wave generator includes a corrugated flow channel whose geometric design is so tuned to generate an acoustic emission whose frequency signature varies as a function of the gas flow velocity. The control system may acquires time-domain acoustic data, and process that data to obtain a frequency-domain representation from which gas velocity or gas flow rate can be determined.Type: GrantFiled: June 16, 2021Date of Patent: November 14, 2023Assignee: UT-Battelle, LLCInventors: Mustafa S. Cetiner, Trevor K. Howard, Annalisa Manera, Victor Petrov, Jiaxin Mao
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Publication number: 20230356145Abstract: Disclosed herein is a method and system for CO2 removal from a gas stream using a diamine solvent having a Formula I R1(R2)N?L1?NH—R3??Formula I. With respect to Formula I, each of R1 and R2 independently is aliphatic, cycloaliphatic, or R1 and R2 together with the nitrogen to which they are attached, form a heterocyclyl ring; L1 is aliphatic, cycloaliphatic, or L1 and R1 together with the nitrogen to which they are attached form a heterocyclyl ring; and R3 is aliphatic, cycloaliphatic, cycloalkylalkyl, or alkoxyalkyl. And/or the compound may have a viscosity of less than 75 cP at a CO2-loading of 40 mol % and at a temperature of 40° C.Type: ApplicationFiled: July 17, 2023Publication date: November 9, 2023Applicant: Battelle Memorial InstituteInventors: Deepika Malhotra, Phillip K. Koech, David J. Heldebrant, Vassiliki-Alexandra Glezakou, Roger J. Rousseau, Manh Thuong Nguyen, Robert Perry, Jordan P. Page, David C. Cantu
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Publication number: 20230355961Abstract: A system for electrical stimulation may comprise a plurality of electrodes and a processor. The processor may be configured to: define a region of interest (ROI) for electrode activation via a first subset of the plurality of electrodes; and define a second subset of electrodes, wherein each electrode within the second subset of electrodes are positioned away from the ROI such that the average distance between each electrode and the ROI is maximized. The second group of electrodes may be defined via low-discrepancy sequences or an equidistributed sequence. The plurality of electrodes may be part of a wearable garment or an implantable device. The system may be for muscle stimulation or neural simulation.Type: ApplicationFiled: July 17, 2023Publication date: November 9, 2023Applicant: Battelle Memorial InstituteInventors: Collin F. Dunlap, Sam Colachis, Joshua R. Branch, Ian Baumgart
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Patent number: 11807543Abstract: A solid ionically conductive composition (e.g., nanoparticles of less than 1 micron or a continuous film) comprising at least one element selected from alkali metal, alkaline earth metal, aluminum, zinc, copper, and silver in combination with at least two elements selected from oxygen, sulfur, silicon, phosphorus, nitrogen, boron, gallium, indium, tin, germanium, arsenic, antimony, bismuth, transition metals, and lanthanides. Also described is a battery comprising an anode, a cathode, and a solid electrolyte (corresponding to the above ionically conductive composition) in contact with or as part of the anode and/or cathode. Further described is a thermal (e.g., plasma-based) method of producing the ionically conductive composition. Further described is a method for using an additive manufacturing (AM) process to produce an object constructed of the ionically conductive composition by use of particles of the ionically conductive composition as a feed material in the AM process.Type: GrantFiled: July 31, 2020Date of Patent: November 7, 2023Assignee: UT-Battelle, LLCInventors: Andrew K. Kercher, Andrew S. Westover, Michael Naguib Abdelmalak, Nancy J. Dudney
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Patent number: 11810208Abstract: Apparatus and methods for a market-based control framework to coordinate a group of autonomous thermostatically controlled loads (TCL) to achieve system-level objectives with pricing incentives is disclosed. In one example of the disclosed technology, a method of providing power to a load via a power grid by submitting bids to a coordinator includes determining an energy response relating price data for one or more energy prices to quantity data for power to be consumed by the load, sending a bid for power for a finite time period based on the energy response to the coordinator, and receiving a clearing price based on: the bid, on bids received from a plurality of additional loads, and a feeder power constraint. In some examples, the energy response is based at least in part on an equivalent thermal parameter model and a control policy indicating one or more power states for the load.Type: GrantFiled: February 20, 2020Date of Patent: November 7, 2023Assignees: Battelle Memorial Institute, Ohio State Innovation FoundationInventors: Jianming Lian, Karanjit Kalsi, Sen Li, Wei Zhang
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Patent number: 11808297Abstract: A fastener for use in joining dissimilar materials manufactured by the process of producing the fastener with an external surface that forms an electrically insulating oxide layer when subjected to oxidation and, after manufacture and prior to use, subjecting the fastener to a pre-oxidation process to grow the desired oxide layer in situ on the external surface of the fastener. The present invention also provides a dissimilar material joint in which the pre-oxidized fastener is used to mechanically join dissimilar materials with the oxide layer electrically insulating the fastener from at least one of the dissimilar materials. The fastener may be a rivet used in friction self-piercing riveting (F-SPR). The fastener may be fabricated from an alloy capable of forming Al2O3 or Cr2O3 by thermal oxidation. The fastener may be pre-coated with Al or Cr that functions as a seed layer to form Al2O3 or Cr2O3.Type: GrantFiled: January 29, 2021Date of Patent: November 7, 2023Assignee: UT-Battelle, LLCInventors: Yong Chae Lim, Ji Heon Jun, Michael P. Brady, Zhili Feng
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Patent number: 11808753Abstract: Systems for determining GW/SW interaction are provided. The systems can include: a sensing assembly comprising sensors for pressure, fluid conductivity, temperature, and transfer resistance; processing circuitry operatively coupled to the sensing assembly and configured to receive data from the sensing assembly and process the data to provide a GW/SW interaction, wherein the data includes pressure, fluid conductivity, temperature, transfer resistance data. Methods for determining GW/SW interaction are provided. The methods can include: receiving real time data including pressure, fluid conductivity, temperature, and transfer resistance; from at least some of the data received simulating the SW/GW interaction; and fitting the real time data with the simulated data to provide actual SW/GW interaction.Type: GrantFiled: November 16, 2022Date of Patent: November 7, 2023Assignee: Battelle Memorial InstituteInventors: Timothy C. Johnson, Christopher E. Strickland, Yue Zhu, Jonathan N. Thomle, James C. Stegen
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Patent number: 11808750Abstract: Sampling devices for sampling an aqueous source (e.g., field testing of ground water) for multiple different analytes are described. Devices include a solid phase extraction component for retention of a wide variety of targeted analytes. Devices include analyte derivatization capability for improved extraction of targeted analytes. Thus, a single device can be utilized to examine a sample source for a wide variety of analytes. Devices also include an isotope dilution capability that can prevent error introduction to the sample analysis and can correct for sample loss and degradation from the point of sampling until analysis as well as correction for incomplete or poor derivatization reactions. The devices can be field-deployable and rechargeable.Type: GrantFiled: April 29, 2021Date of Patent: November 7, 2023Assignee: Battelle Savannah River Alliance, LLCInventors: Andrew J. Boggess, Stephen L. Crump, Thomas L. White
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Publication number: 20230353351Abstract: Methods of quantum key distribution include receiving a frequency bin photon at a location, selecting a frequency bin photon quantum key distribution measurement basis, with a quantum frequency processor, performing a measurement basis transformation on the received frequency bin photon so that the frequency bin photon is measurable in the selected frequency bin photon quantum key distribution measurement basis, and detecting the frequency bin photon in the selected quantum key distribution measurement basis and assigning a quantum key distribution key value based on the detection to a portion of a quantum key distribution key. Apparatus and methods for encoding, decoding, transmitting, and receiving frequency bin photons are disclosed.Type: ApplicationFiled: June 29, 2023Publication date: November 2, 2023Applicant: UT-Battelle, LLCInventors: Joseph M. Lukens, Pavel Lougovski
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Patent number: 11801346Abstract: An autoinjector and method of injection are described. A power spring causes rotation of a drive nut about the central axis of the autoinjector that, in turn, causes a middle screw to rotate in the same direction as the drive nut and also to move in the distal direction while pushing a center screw in the distal direction that pushes the syringe and needle. The center screw also pushes a plunger that pushes the fluid out of the syringe. After injection, a locked retract screw is freed and rotates in the same direction as the middle screw causing the syringe to retract the syringe into the housing.Type: GrantFiled: April 9, 2020Date of Patent: October 31, 2023Assignee: Battelle Memorial InstituteInventors: William G. Atterbury, Timothy M. Blum, David A. Holley, John P. Tallarico, Steven M. Madland
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Patent number: 11805104Abstract: Computing system operational methods and apparatus are described. According to one aspect, a computing system operational method includes accessing user information regarding a user logging onto a computing device of the computing system, processing the user information to determine if the user information is authentic, as a result of the processing determining that the user information is authentic, first enabling the computing device to execute an application segment, and as a result of the processing determining that the user information is authentic, second enabling the application segment to communicate data externally of the computing device via one of a plurality of network segments of the computing system.Type: GrantFiled: December 14, 2018Date of Patent: October 31, 2023Assignee: Battelle Memorial InstituteInventors: Thomas W. Edgar, Thomas E. Carroll, Garret E. Seppala
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Patent number: 11802357Abstract: The present subject matter relates to systems, devices, and methods of enhancing carbon fiber dispersion in wet-laid nonwovens. A quantity of fibers is deposited in a medium, and each of one or more stirring elements is moved in a pattern to mechanically agitate the medium. In some embodiments, moving each of the one or more stirring elements includes moving the one or more stirring elements in complementary patterns to induce a chaotic advection current within the medium.Type: GrantFiled: September 10, 2019Date of Patent: October 31, 2023Assignees: University of Tennessee Research Foundation, UT-Battelle, LLCInventors: Hicham Kheir Ghossein, Lonnie J. Love, Uday Kumar Vaidya
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Publication number: 20230341409Abstract: Provided herein are methods and systems for proteome analysis that are at least partially automated and/or performed robotically. In some aspects, the methods and systems described herein can rapidly and efficiently provide protein identification of each of the proteins from a proteome, or a complement of proteins, obtained from extremely small amounts of biological samples. The identified proteins can be imaged quantitatively over a spatial region. Automation and robotics facilitates the throughput of the methods and systems, which enables protein imaging and/or rapid proteome analysis.Type: ApplicationFiled: June 14, 2023Publication date: October 26, 2023Applicant: Battelle Memorial InstituteInventors: Paul D. Piehowski, Ying Zhu, Ryan T. Kelly, Kristin E. Burnum-Johnson, Ronald J. Moore
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Patent number: 11795583Abstract: A method for producing polyacrylonitrile (PAN) fiber, the method comprising: (i) mixing PAN with an ionic liquid in which the PAN is soluble to produce a PAN composite melt in which the PAN is dissolved in the ionic liquid; (ii) melt spinning the PAN composite melt to produce the PAN fiber; and (iii) washing the PAN fiber with a solvent in which the ionic liquid is soluble to substantially remove the ionic liquid from the PAN fiber. Also described herein is a method for producing carbon fiber from the PAN fiber as produced above, the method comprising oxidatively stabilizing the PAN fiber produced in step (iii), followed by carbonizing the stabilized PAN fiber to produce the carbon fiber. The initially produced PAN fiber, stabilized PAN fiber, resulting carbon fiber, and articles made thereof are also described.Type: GrantFiled: January 21, 2022Date of Patent: October 24, 2023Assignees: UT-Battelle, LLC, University of Tennessee Research FoundationInventors: Sheng Dai, Huimin Luo, Halie J. Martin