Patents Assigned to Battelle
  • Publication number: 20190126561
    Abstract: A method for solid state joining of dissimilar materials using a friction stir welding device wherein a pin is inserted through an aperture defined in a first material and a second material to hold the materials together and then held in place by friction stir welding a portion of the pin to a material adjacent said pin, or by friction stir welding a cap or plug that holds the pin in place to the adjacent material. The result is a connection or join wherein the central portion of the pin is not friction stir welded but the portions holding the pin in place (the ends or caps) generally are.
    Type: Application
    Filed: October 26, 2017
    Publication date: May 2, 2019
    Applicant: BATTELLE MEMORIAL INSTITUTE
    Inventors: Scott A. Whalen, MD. Reza-E-Rabby, Kenneth A. Ross, Aashish Rohatgi
  • Publication number: 20190126252
    Abstract: Disclosed herein are catalyst materials and vehicle catalytic converters having platinum atomically dispersed on a ceria support and having a T90 value less than or equal to 150° C., wherein the T90 value represents the temperature required for 90% CO conversion. Also disclosed are methods of making the catalyst material involving hydrothermally treating at a temperature of at least 700° C. a Pt/ceria material comprising atomically dispersed Pt on a ceria support and activating 90% CO conversion at a temperature less than or equal to 150° C. (i.e., T90?150° C.).
    Type: Application
    Filed: October 22, 2018
    Publication date: May 2, 2019
    Applicant: BATTELLE MEMORIAL INSTITUTE
    Inventors: Lei Nie, Yong Wang
  • Patent number: 10274609
    Abstract: A radioactive gas assay system comprises a scintillation cell production assembly, a detector assembly, a computer assembly, and a scintillation cell destruction assembly. The scintillation cell production assembly is configured to produce a scintillation cell comprising a glass scintillator shell containing a volume of radioactive gas. The detector assembly is configured to receive the scintillation cell and to detect photons emitted thereby. The computer assembly is configured to receive data from the detector assembly to automatically calculate an absolute activity of the volume of radioactive gas of the scintillation cell and radiation detection efficiencies of the detector assembly. The scintillation cell destruction assembly is configured to receive the scintillation cell and to rupture the substantially non-porous glass scintillator shell to release the volume of radioactive gas. A method of assaying a radioactive gas, and a scintillation cell are also described.
    Type: Grant
    Filed: May 9, 2017
    Date of Patent: April 30, 2019
    Assignees: Battelle Energy Alliance, LLC, Battelle Memorial Institute
    Inventors: Troy A. Robinson, Martha R. Finck, Matthew W. Cooper, James C. Hayes, Edward L. Reber
  • Patent number: 10274807
    Abstract: Methods of generating second harmonic generation (SHG) signals from interfaces formed with, or formed over, a noncentrosymmetric material, e.g., ?-quartz, are provided. The methods make use of the noncentrosymmetric material as an internal phase reference for the determination of a variety of interfacial electrostatic parameters, including interfacial potential, interfacial charge density, and the sign of the interfacial charge (i.e., net positive or net negative).
    Type: Grant
    Filed: December 7, 2017
    Date of Patent: April 30, 2019
    Assignees: Northwestern University, Battelle Memorial Institute, The Trustees of Columbia University in the City of New York
    Inventors: Franz M. Geiger, Paul E. Ohno, Hong-fei Wang, Kenneth B. Eisenthal
  • Patent number: 10266915
    Abstract: A solid particulate composition useful in extracting a lithium salt from aqueous solutions, the composition comprising lithium, metal atoms, oxygen atoms, and at least one anionic species (X) selected from halide, nitrate, sulfate, carbonate and bicarbonate, all in a framework structure, wherein said metal atoms are selected from at least one of oxophilic main group metal and oxophilic transition metal atoms, provided that, if the metal atoms comprise aluminum atoms, then at least 10 mol % of said aluminum atoms are substituted with at least one metal atom selected from said at least one oxophilic main group and oxophilic transition metal atoms, other than aluminum, and wherein said lithium is present in said composition in an amount less than a saturated amount in order to permit extraction of lithium salt. Methods for extracting and recovering a lithium salt from an aqueous solution by use of the above-described composition are also described.
    Type: Grant
    Filed: April 14, 2016
    Date of Patent: April 23, 2019
    Assignees: UT-Battelle, LLC, Alger Alternative Energy, LLC
    Inventors: Mariappan Parans Paranthaman, Ramesh R. Bhave, Bruce A. Moyer, Stephen Harrison
  • Patent number: 10269525
    Abstract: A liquid sampling, atmospheric pressure, glow discharge (LS-APGD) device as well as systems that incorporate the device and methods for using the device and systems are described. The LS-APGD includes a hollow capillary for delivering an electrolyte solution to a glow discharge space. The device also includes a counter electrode in the form of a second hollow capillary that can deliver the analyte into the glow discharge space. A voltage across the electrolyte solution and the counter electrode creates the microplasma within the glow discharge space that interacts with the analyte to move it to a higher energy state (vaporization, excitation, and/or ionization of the analyte).
    Type: Grant
    Filed: November 23, 2016
    Date of Patent: April 23, 2019
    Assignees: Clemson University Research Foundation, Battelle Memorial Institute on behalf of Pacific Northwest National Laboratory, The Regents of the University of California—Lawrence Berkeley National Laboratory
    Inventors: R. Kenneth Marcus, Charles Derrick Quarles, Jr., Richard E. Russo, David W. Koppenaal, Charles J. Barinaga, Anthony J. Carado
  • Patent number: 10270787
    Abstract: A method and system for administering an interactive computer network and more particularly to performing security in a network of interactive electronic components, such as a computer network using a currency-based transactional economy model where scarcity serves as a limiting factor to accessing and engaging in various activities within the system.
    Type: Grant
    Filed: May 23, 2016
    Date of Patent: April 23, 2019
    Assignee: Battelle Memorial Institute
    Inventors: Jeremy R. Teuton, Jeromy M. Markwort
  • Patent number: 10265660
    Abstract: Zeolite membrane sheets for separation of mixtures containing water are provided, as well as methods for making the same. Thin, but robust, zeolite membrane sheets having an inter-grown zeolite crystal film directly on a thin, less than 200 micron thick, porous support sheet free of any surface pores with a size above 10 microns. The zeolite membrane film thickness is less than about 10 microns above the support surface and less than about 5 microns below the support surface. Methods of preparing the membrane are disclosed which include coating of the support sheet surface with a seed coating solution containing the parent zeolite crystals with mean particle sizes from about 0.5 to 2.0 microns at loading of 0.05-0.5 mg/cm2 and subsequent growth of the seeded sheet in a growth reactor loaded with a growth solution over a temperature range of about 45° C. to about 120° C.
    Type: Grant
    Filed: June 8, 2015
    Date of Patent: April 23, 2019
    Assignee: Battelle Memorial Institute
    Inventor: Wei Liu
  • Publication number: 20190110468
    Abstract: This invention relates to a liquid herbicidal composition comprising a non-aqueous solvent system, at least one sulfonylurea herbicide and at least one inorganic or C1-C12 organic lithium salt. The invention also relates to the use of an inorganic or C1-C12 organic lithium salt to improve chemical stabilisation of a sulfonylurea herbicide in a liquid composition comprising a non-aqueous solvent system.
    Type: Application
    Filed: June 21, 2017
    Publication date: April 18, 2019
    Applicants: Battelle UK Limited, Mitsui AgrScience International S.A./N.V.
    Inventors: Andrew Goldsmith, John Groome
  • Patent number: 10263246
    Abstract: An electrode material includes a lithium active material composition. The lithium active material composition includes lithium and an active anode material. The lithium active material composition is coated with a lithium ion conducting passivating material, such that the electrode material is lithiated and pre-passivated. An electrode and a battery are also disclosed. Methods of making an electrode material, electrode and battery that are lithiated and pre-passivated are also disclosed.
    Type: Grant
    Filed: November 20, 2015
    Date of Patent: April 16, 2019
    Assignee: UT-BATTELLE, LLC
    Inventors: Nancy J. Dudney, Edward W. Hagaman, Gabriel M. Veith, Lance W. Gill, Robert L. Sacci
  • Patent number: 10263786
    Abstract: Disclosed below are representative embodiments of methods, apparatus, and systems for monitoring and using data in an electric power grid. For example, one disclosed embodiment comprises a sensor for measuring an electrical characteristic of a power line, electrical generator, or electrical device; a network interface; a processor; and one or more computer-readable storage media storing computer-executable instructions.
    Type: Grant
    Filed: January 19, 2018
    Date of Patent: April 16, 2019
    Assignee: Battelle Memorial Institute
    Inventors: Bora A. Akyol, Jereme Nathan Haack, Philip Allen Craig, Jr., Cody William Tews, Anand V. Kulkarni, Brandon J. Carpenter, Wendy M. Maiden, Selim Ciraci
  • Patent number: 10260156
    Abstract: A system and process are disclosed for electrochemically upgrading bio-oils and bio-crudes that enhance yields of selected reduction products for subsequent production of bio-based fuels.
    Type: Grant
    Filed: March 23, 2016
    Date of Patent: April 16, 2019
    Assignee: BATTELLE MEMORIAL INSTITUTE
    Inventors: Michael A. Lilga, Asanga B. Padmaperuma, Tedd E. Lister, Eric J. Dufek, Lucia M. Petkovic, Luis A. Diaz-Aldana
  • Publication number: 20190106799
    Abstract: An ionic liquid composition comprising a complex of a trihalo aluminum (III) species with at least one organic uncharged ligand comprising a ring structure having at least three ring carbon atoms and at least one ring heteroatom selected from nitrogen and sulfur, wherein the complex is a liquid at a temperature of 100° C. or less. Methods of electroplating aluminum onto a metallic substrate using the above-described ionic liquid composition are also described.
    Type: Application
    Filed: December 10, 2018
    Publication date: April 11, 2019
    Applicant: UT-Battelle, LLC
    Inventors: Sheng Dai, Xiao-Guang Sun
  • Publication number: 20190108990
    Abstract: A method of manipulating ions comprises injecting ions between a first surface and a second surface positioned parallel to and spaced apart from each other and defining a central axis therebetween, wherein the first surface comprises first outer electrodes coupled to the first surface and a first inner array of electrodes coupled to the first surface and positioned between the first outer electrodes, wherein the second surface comprises second outer electrodes coupled to the second surface and a second inner array of electrodes coupled to the second surface and positioned between the second outer electrodes, and applying a frequency modulated RF voltage to at least one electrode of the first inner array of electrodes or the second inner array of electrodes to confine ions between the first surface and the second surface and to guide ions between the first surface and the second surface along the central axis.
    Type: Application
    Filed: November 16, 2018
    Publication date: April 11, 2019
    Applicant: Battelle Memorial Institute
    Inventors: Aneesh Prabhakaran, Yehia M. Ibrahim, Sandilya V. B. Garimella
  • Publication number: 20190105710
    Abstract: An apparatus and device for building an article by additive manufacturing or 3-D printing. The method includes feeding a supply of particulate slurry to and through a nozzle, such as including an integrated pump, to form a plurality of beads and layers of the slurry on a deposition surface, and ultimately forming a desirable article from the layers of deposited material. The liquid phase of the slurry is desirably removed by heat, and the deposited layers can be sintered or otherwise fused as needed.
    Type: Application
    Filed: October 5, 2018
    Publication date: April 11, 2019
    Applicant: UT-BATTELLE, LLC
    Inventors: James W. Klett, Amelia M. ELLIOTT, Makayla S. EDWARDS, Kelsey L. HEDRICK, Ryan K. DUNCAN, Alex G. HESSLER, Corson L. CRAMER
  • Patent number: 10256072
    Abstract: Disclosed are methods for optimized sub-sampling in an electron microscope. With regard at least to utilization of electron dose budgets, of time for acquisition of measurements, and of computing/processing capabilities, very high efficiencies can be achieved by informing and/or adapting subsequent sub-sampling measurements according to one or more earlier-acquired sparse datasets and/or according to analyzes thereof.
    Type: Grant
    Filed: August 1, 2017
    Date of Patent: April 9, 2019
    Assignee: Battelle Memorial Institute
    Inventors: Andrew J. Stevens, Libor Kovarik, Andrey V. Liyu, Nigel D. Browning
  • Patent number: 10255355
    Abstract: The visual analytic system enables information retrieval within large text collections. Typically, users have to directly and explicitly query information to retrieve it. With this system and process, the reasoning of the user is inferred from the user interaction they perform in a visual analytic tool, and the appropriate information to query, process, and visualize is systematically determined.
    Type: Grant
    Filed: May 27, 2015
    Date of Patent: April 9, 2019
    Assignee: Battelle Memorial Institute
    Inventors: Alexander Endert, Nicholas O. Cramer, Ralph J. Perko, III, Shawn D. Hampton, Edwin R. Burtner, Kristin A. Cook
  • Patent number: 10254562
    Abstract: Methods and devices for altering the power of a lens, such as an intraocular lens, are disclosed. In one method, the lens comprises a single polymer matrix containing crosslinkable pendant groups, wherein the polymer matrix increases in volume when crosslinked. The lens does not contain free monomer. Upon exposure to ultraviolet radiation, crosslinking causes the exposed portion of the lens to increase in volume, causing an increase in the refractive index. In another method, the lens comprises a polymer matrix containing photobleachable chromophores. Upon exposure to ultraviolet radiation, photobleaching causes a decrease in refractive index in the exposed portion without any change in lens thickness. These methods avoid the need to wait for diffusion to occur to change the lens shape and avoid the need for a second exposure to radiation to lock in the changes to the lens.
    Type: Grant
    Filed: March 11, 2016
    Date of Patent: April 9, 2019
    Assignee: BATTELLE MEMORIAL INSTITUTE
    Inventors: Herbert S. Bresler, Erik Edwards, Amy M. Heintz, John S. Laudo, Alexander C. Morrow, Steven M. Risser
  • Patent number: 10253261
    Abstract: Liquid crystalline network compositions comprising azo-containing aromatic epoxy units cross-linked with alkylene diacid units having alkylene segments containing at least one methylene unit, wherein the azo-containing aromatic epoxy units and alkylene diacid units are connected by ester linkages resulting from ring-opening esterification between the epoxy units and alkylene diacids, and wherein the azo-containing aromatic epoxy units and alkylene diacid units are in a molar ratio that results in the liquid crystalline network composition exhibiting a glass transition temperature (Tg) of at least 25° C. Methods for producing these compositions and their use in light- or thermal-activated physical deformation, shape memory applications, and self-healing, as well as their ability to be recycled and used in additive manufacturing processes are also described.
    Type: Grant
    Filed: January 19, 2017
    Date of Patent: April 9, 2019
    Assignees: UT-BATTELLE, LLC, WASHINGTON STATE UNIVERSITY
    Inventors: Yuzhan Li, Orlando Rios, Michael Richard Kessler
  • Patent number: 10254248
    Abstract: A unique fiber core sampler composition, related systems, and techniques for designing, making, and using the same are described. The sampler is used to interface with existing field instrumentation, such as Ion Mobility Spectrometer (IMS) equipment. Desired sampler characteristics include its: stiffness/flexibility; thermal mass and conductivity; specific heat; trace substance collection/release dependability, sensitivity and repeatability; thickness; reusability; durability; stability for thermal cleaning; and the like. In one form the sampler has a glass fiber core with a thickness less than 0.3 millimeter that is coated with a polymer including one or more of: polymeric organofluorine, polyimide, polyamide, PolyBenzlmidazole (PBI), PolyDiMethylSiloxane (PDMS), sulfonated tetrafluoroethylene (PFSA) and Poly(2,6-diphenyl-p-phenylene Oxide) (PPPO).
    Type: Grant
    Filed: April 21, 2015
    Date of Patent: April 9, 2019
    Assignee: Battelle Memorial Institute
    Inventors: Raymond S Addleman, Xiaohong Shari Li, Wilaiwan Chouyyok, David A Atkinson