Abstract: A preparation method of itaconate-butadiene bio-based engineering rubber belongs to the bio-based engineering rubber area. The bio-based engineering rubber of the present disclosure is formed through chemical crosslinking of copolymers, which are formed by polymerization of itaconate and butadiene emulsion. The number average molecular weight of the itaconate-butadiene copolymer is about 53000-1640000, and weight-average molecular weight is about 110000-2892000. Itaconate-butadiene copolymers are formed by polymerization of itaconate and butadiene emulsion, then and chemical crosslinking of the copolymer is performed to form bio-based engineering rubber using a traditional sulfur vulcanizing system. The bio-based engineering rubber has high molecular weights as well as lower glass-transition temperatures and can be vulcanized using the traditional sulfur vulcanizing system.

Abstract: The present disclosure relates to an adhesive comprising at least one of the following copolymer A: the copolymer A has at least one repeating unit carrying an amide group and a carboxyl and/or its ammonium salt and at least one other repeating unit different from the one carrying an amide group and a carboxyl and/or its ammonium salt. The present disclosure also relates to an artificial board formed of a lignocellulose material and the adhesive and a method for manufacturing the artificial board.

Abstract: The present disclosure relates to an adhesive comprising at least one of the following copolymer A: the copolymer A has at least one repeating unit carrying an amide group and a carboxyl and/or its ammonium salt and at least one other repeating unit different from the one carrying an amide group and a carboxyl and/or its ammonium salt. The present disclosure also relates to an artificial board formed of a lignocellulose material and the adhesive and a method for manufacturing the artificial board.

Abstract: The present disclosure relates to the field of the preparation of high purity sodium and the safe treatment of sodium calcium slag, and discloses a method and apparatus for sodium slag recovery by using gravity separation—controllable combustion—alkaline liquor leaching process for the preparation of high purity sodium and safe treatment of sodium calcium slag. The method comprises the following steps: (1) subjecting a liquid sodium slag to a gravity stratification to obtain pure metallic sodium and high calcium content sodium slag; (2) roasting the high calcium content sodium slag to obtain a roasting slag; and (3) leaching the roasting slag by using an alkaline liquor to obtain the sodium hydroxide solution and calcium hydroxide.

Abstract: The present disclosure relates to the field of non-ferrous metal and chemical industries for the production of metal sodium, and discloses a process for the preparation of high purity metallic sodium and the safe treatment of high calcium content sodium slag, the process comprises the following steps: (1) subjecting a liquid sodium obtained from electrolysis to a supergravity separation to obtain a high purity metallic sodium and a high calcium content sodium slag; (2) subjecting said high calcium content sodium slag to at least one roasting process to obtain a roasting slag; (3) leaching said roasting slag with an alkaline liquor to produce sodium hydroxide solution and calcium hydroxide. The process provided by the present disclosure not only greatly reduces the amount of generated sodium slag, but also implements the safe recovery of calcium and sodium resources from the sodium slag.

Abstract: Cuy/MMgOx interfacial catalyst for selective alkyne hydrogenation and its preparation method are disclosed. The preparation method of the catalyst includes: the mixture of salt and alkali solution is nucleated momentarily by nucleation/crystallization isolation method, preparing the composite metal hydroxide CuyMMg4-LDHs as precursor, which has typical hexagonal morphology of the double hydroxide; the precursor is topologically transformed by heat treatment to produce unsaturated oxide; the catalyst with Cuy-MMgOx interface structure is prepared by separating and electronically modifying Cu particles. By adjusting the ratio of Cu2+/M3+ in LDHs, the electronic and geometric structure of Cuy-MMgOx interface can be flexibly controlled, thus enhancing the reaction activity, product selectivity and stability. The catalyst can be used in the selective hydrogenation of various alkynes in the fields of petrochemical and fine chemical industry, with the outstanding catalytic activity and C?C double bond selectivity.

Abstract: An energy saving and emission reduction system for chemical separation and purification process is disclosed. The chemical separation and purification process includes a synthesis section and/or a distillation section and/or a recovery section. The energy saving and emission reduction system includes an energy comprehensive utilization maximizing energy saving module. The energy comprehensive utilization maximizing energy saving module comprehensively evaluates the chemical separation and purification process, and acquires a lowest energy consumption value according to initial and final material flow parameters. Then energy integration optimization and energy saving technical modification are performed on the synthesis section and/or distillation section and/or recovery section according to the lowest energy consumption value.

Abstract: This invention provides a method for efficiently separating magnesium and lithium from salt lake brine, and simultaneously preparing high-purity magnesium oxide and battery-grade lithium carbonate. The detailed processing steps are as follows: (1) adding urea into the brine to dissolve, (2) placing the solution into the reactor for hydrothermal reaction, the magnesium ion will precipitate and enter the solid phase; (3) filtering and drying the production to get the magnesium carbonate solid, while the lithium ion remains in the liquid phase; (4) after directly concentration and precipitation, the battery-grade lithium carbonate can be obtained, while the calcination of solid-phase product results in the high-purity magnesium oxide. In this method, urea is used as the precipitant to separate magnesium and lithium in salt lake without introducing any new metal ion, and the brine solution is not diluted. The solid product is white and fluffy powder, which is easy to filter and separate.

Abstract: The present disclosure discloses a butenediol-based polyester elastomer and a method for preparing same. In the present disclosure, 1,4-butenediol containing high-stability double-bond is used to replace itaconic acid, and a series of butenediol-based polyester elastomers with high molecular weight and narrow distribution are synthesized, which have high relative molecular weight and narrow relative molecular weight distribution. The crosslinking in subsequent processing is more controllable, and the dosage of a vulcanizing agent is equivalent to that of traditional rubber.

Abstract: The present disclosure relates to a fault diagnosis method of a reciprocating machinery based on a keyphasor-free complete-cycle signal. The method includes the following steps: 1) building a complete-cycle vibration signal image library; 2) training an image recognition model; 3) acquiring a complete-cycle data on a keyphasor-free basis; 4) building an automatic feature extraction model; and 5) inputting a hidden layer feature of an autoencoder into a support vector machine (SVM) classifier to obtain a diagnosis result. By using a deep cascade convolutional neural network (CNN), the present disclosure achieves the goal of complete-cycle data acquisition on a keyphasor-free basis, solves the problems that traditional intelligent fault diagnosis relies on a keyphasor signal and real-time diagnosis fails due to insufficient installation space. In addition, by using an autoencoder for automatic feature extraction, the present disclosure avoids manual feature selection, reduces labor costs.

Abstract: The invention discloses a composition for fiber surface treatment and a process for treating a fiber. The fiber surface treatment composition of the invention includes maleic anhydride polymer, epoxy resin, blocked isocyanate, curing agent, rubber latex, solvent and optional filler. The fiber treated by the invention has excellent adhesion effects, reaching or even exceeding the adhesion level of RFL treatment.

Abstract: Described is a method for extracting lithium from salt lake brine and simultaneously preparing aluminum hydroxide. This method includes a. adding an aluminum salt to the brine, adding an alkali solution, then subjecting to crystallization reaction and solid-liquid separation to obtain lithium-containing brine; b. evaporating and concentrating the lithium-containing brine, adding an aluminum salt, adding an alkali solution dropwise to perform a co-precipitation reaction and solid-liquid separation to obtain a lithium-containing layered material filter cake, wherein in steps a and b, the alkali solution is an alkali solution free of carbonate ion; c. dispersing the lithium-containing layered material filter cake in deionized water to form a suspension slurry, then adjusting the pH value of the suspension slurry so as to carry out a lithium deintercalation reaction; d. filtering to obtain aluminum hydroxide filter cake; e. washing the aluminum hydroxide filter cake with deionized water and drying.

Abstract: An electromagnetic automatic balancing device based on radial excitation includes a shell, a rotatory ring, a stationary ring, a pair of connecting bearings and a controller. The rotatory ring includes two bilaterally symmetrical outer excitation magnetic rings, two bilaterally symmetrical inner excitation magnetic rings, two bilaterally symmetrical counterweight discs, two bilaterally symmetrical first counterweight blocks, two bilaterally symmetrical second counterweight blocks and a pair of rotatory-ring bearings. The stationary ring includes a stator, two bilaterally symmetrical excitation frameworks and two bilaterally symmetrical coils. The rotatory ring and the stationary ring are installed in the shell and connected through a pair of connecting bearings. The stator is installed in the center of the shell. The excitation frameworks are respectively fixed at both ends of the stator.

Abstract: Disclosed is a production device and production method of electronic grade hydrofluoric acid. The method includes vaporizing the raw material industrial anhydrous hydrogen fluoride by an evaporator, transporting the vaporized hydrogen fluoride to a purification tower, obtaining a high purity hydrogen fluoride gas through rectification, transporting the high purity hydrogen fluoride gas to an absorption tower for absorption by a certain concentration of hydrofluoric acid in the liquid phase, obtaining the crude electronic grade hydrofluoric acid, and obtaining the electronic grade hydrofluoric acid product through ultrapure filtration. The disclosure overcomes the technical problems of small yield and low purity of the prior art. The production process meets the requirements of environmental protection. The disclosure is suitable for industrialized large-scale production.

Abstract: A load identification method for reciprocating machinery based on information entropy and envelope features of an axis trajectory of a piston rod. According to the present disclosure, firstly, the position of an axial center is calculated according to a triangle similarity theorem to obtain an axial center distribution; secondly, features are extracted from the axial center distribution of the piston rod by means of an improved envelope method for discrete points as well as an information entropy evaluation method; thirdly, a dimensionality reduction is carried out on the features by means of manifold learning to form a set of sensitive features of the load; and finally, a neural network is trained to obtain a load identification classifier to fulfill automatic identification on the operating load of the reciprocating machinery. The advantages of the present disclosure are verified by means of actual data of a piston rod of a reciprocating compressor.

Abstract: The present invention discloses an efficient mass-transfer separation bulk filler structure, which includes a bulk filler body with closely-fit multilayer structures, wherein an annular wall surface of the bulk, filler body has a corrugated angle group. A lower portion of the bulk filler body is of a bell-mouth shape. Three passages with a same sectional area are formed inside the bulk filler body. The present invention has the characteristics of small pressure drop, large specific surface area, low liquid holdup and large void ratio. The annular wall surface is provided with the corrugated angle group to increase the disturbance and reduce a double-membrane thickness of vapor and liquid phase mass-transfer resistance, thereby improving the mass-transfer coefficient and separation efficiency. Meanwhile, by adopting the bell-mouth shape, the stability and natural stacking regularity of the bulk filler can be improved.

Abstract: A method for efficiently catalyzing furfural to prepare cyclopentanone, and a catalyst and preparation method therefor, are disclosed, in the field of biomass catalytic conversion. The catalyst comprises uniformly dispersed metal active center nanoparticles and oxides obtained by LDHs calcination. The metal active center is single atom Pt/Cu alloy; the LDHs is used as a precursor to prepare a Cu-containing catalyst precursor; after a reduction in H2 atmosphere, small amount of Pt2+ is used for reacting with the Cu-containing catalyst precursor to obtain a monoatomic Pt/Cu catalyst; said catalyst is used to catalyze hydrogenation of an aqueous phase of furfural to prepare cyclopentanone, wherein the reaction temperature is 120-250° C., the reaction pressure is 0.1-5 MPa, the reaction time is 0.5-24 hours, and the reaction solvent is ultrapure water. Low-cost and efficient, the catalyst catalyzes the hydrogenation of an aqueous phase of furfural to prepare cyclopentanone.

Abstract: The present disclosure relates to a fault diagnosis method of a reciprocating machinery based on a keyphasor-free complete-cycle signal. The method includes the following steps: 1) building a complete-cycle vibration signal image library; 2) training an image recognition model; 3) acquiring a complete-cycle data on a keyphasor-free basis; 4) building an automatic feature extraction model; and 5) inputting a hidden layer feature of an autoencoder into a support vector machine (SVM) classifier to obtain a diagnosis result. By using a deep cascade convolutional neural network (CNN), the present disclosure achieves the goal of complete-cycle data acquisition on a keyphasor-free basis, solves the problems that traditional intelligent fault diagnosis relies on a keyphasor signal and real-time diagnosis fails due to insufficient installation space. In addition, by using an autoencoder for automatic feature extraction, the present disclosure avoids manual feature selection, reduces labor costs.

Abstract: The embodiments of the present disclosure disclose a scroll type micro-compressor, and a method for machining a fixed scroll plate and an orbit scroll plate thereof. The scroll type micro-compressor comprises a fixed scroll plate and an orbit scroll plate each integrally made with a monocrystalline silicon substrate; the compressor device has an Oldham ring structure, and reduces a mass of the orbit scroll plate by optimizing a design of a substrate of the orbit scroll plate; a cross-sectional shape of a plurality of micropores provided on a lower surface of the fixed scroll plate is set as of a fan ring, in which an electrode material is accommodated to maintain an electric field uniformity and reduce an electric field loss; and hydrophilia of inner surfaces is changed to prevent a top leakage and facilitate capillary filling of a compression chamber.

Abstract: A method for calibrating phase-frequency characteristics of low frequency accelerometer based on time-spatial synchronization, comprises: measuring excitation displacement of the low frequency accelerometer to realize excitation acceleration measurement of the low frequency accelerometer; realizing alignment of the excitation acceleration signal of the low frequency accelerometer with output voltage signal of the low frequency accelerometer in the spatial domain based on TSS technology, fitting the excitation acceleration signal and the output voltage signal respectively by SAM, and calculating phase ?F of the excitation acceleration signal at a zero position of horizontal long-stroke shaker and phase ?Z of the output voltage signal at the time when a zero encoder on the shaker outputs pulse; and calculating the sensitivity phase of the low frequency accelerometer with ?Z and ?F, and determining phase-frequency characteristics of the low frequency accelerometer by calibrating the sensitivity phases at differe