Abstract: A method for obtaining a nuclear magnetic resonance (NMR) correlation spectrum of heteronuclear spin systems, in particular comprising large molecules, especially biological macromolecules in solution, the spin system being subjected to a homogeneous magnetic field B.sub.0, being irradiated by a sequence of radio frequency (rf) pulses, is characterized in that the spin system comprises at least two kinds of spin 1/2 nuclei I and S being coupled to each other, whereby the sequence of rf pulses is chosen such that line broadening in the observed spectrum due to transverse relaxation (T.sub.2) is significantly reduced because of cross correlation between dipole--dipole (DD) coupling of the spins and chemical shift anisotropy (CSA), giving rise to different relaxation rates of the individual multiplet components of the spin system and chosen such that the relaxation effects of the two different mechanisms cancel each other out to a large degree. Thus, even very large biological macromolecules can be measured.

Abstract: An RF resonator for resonant transmission and/or reception of RF-pulses at a desired resonance frequency into or out of a sample (5) within an investigational region in a homogeneous magnetic field B.sub.0 of an (NMR)-apparatus has at least two spatially separated superconducting components (1, 1a, 1b, 1c, 1d) which do not constitute, either alone or in combination, a closed resonance system capable of resonating at the desired resonant frequency. Normally conducting connection elements (2a, 2b) are therefore provided to connect the superconducting components conductively and/or capacitively in such a fashion that the superconducting components, together with the normally connecting components, form one or a plurality of closed resonance systems capable of resonating at the desired resonant frequency. In this fashion, despite use of flat superconducting materials, a substantially higher fill factor, a very good homogeneity of the B.sub.