Abstract: Purified dibenzylidene sorbitol is prepared by mixing crude dibenzylidene sorbitol containing monobenzylidene sorbitol and tribenzylidene sorbitol as by-product impurities with a lower aliphatic alcohol to dissolve the impurities, and separating and recovering the undissolved dibenzylidene sorbitol. This process affords dibenzylidene sorbitol having a purity of at least 98% from crude dibenzylidene sorbitol with a purity of about 95%.
Type:
Grant
Filed:
May 9, 1977
Date of Patent:
December 26, 1978
Assignees:
E. C. Chemical Ind. Co., Ltd., C. Itoh & Co.