Abstract: A microencapsulated epoxy adhesive system is disclosed comprising in admixture epoxy resin capsules and encapsulated Ancamine TL (Pacific Anchor Chemical Co.) as the curing agent. When applied, for example to a zinc plated bolt and the bolt is tightened, the capsules break and the resin cures and provides good breakaway torques.
Type:
Grant
Filed:
June 15, 1982
Date of Patent:
August 20, 1985
Assignee:
Capsulated Systems, Inc.
Inventors:
Ronald L. Hart, Dale E. Work, Colin E. Davis
Abstract: A highly impermeable encapsulating coating is disclosed prepared from a hydrolyzed ethylene-vinyl ester copolymer prepared by alcoholysis of, for example, ethylene-vinyl acetate using 4 to 9 times the amount of alcohol stoichiometrically required for a predetermined degree of hydrolysis.
Type:
Grant
Filed:
May 29, 1981
Date of Patent:
March 22, 1983
Assignee:
Capsulated Systems, Inc.
Inventors:
Ronald L. Hart, Dale E. Work, Daniel Davis, Robert G. Bayless
Abstract: Microcapsules having a capsule core material surrounded by a relatively impermeable, densified protective wall and a method of producing such microcapsules are disclosed. To produce the microcapsules, an agitated system is provided including a liquid vehicle as a major component of the system and constituting a continuous first phase of the system. A plurality of discrete capsule core material entities are dispersed in the liquid vehicle and constitute a discontinuous second phase. A film-forming, cross-linkable, polymeric base material is also present in the liquid vehicle and, upon induction of phase separation within the agitated system, forms a sheath about the capsule core material entities. The formed sheath also contains entrapped liquid vehicle; however, a major portion of the entrapped liquid vehicle is subsequently extracted from the sheath, and the resulting densified polymeric base material in the sheath is then cross-linked to form a densified protective wall around the capsule core material.