Abstract: A method and apparatus for purifying acetonitrile from low grade acetonitriles. Low grade acetonitrile from DNA synthesis, HPLC and pharmaceutical drug manufacturing process wastes which comprise acetonitrile, a first set of impurities having a lower boiling temperature than acetonitrile and a second set of impurities having a boiling temperature greater than acetonitrile are processed to produce a purified acetonitrile by first introducing the low grade acetonitrile into a first distillation column and separating the acetonitrile and first set of impurities from the second set of impurities, the acetonitrile and first set of impurities being drawn as a vapor from the first distillation column, the second set of impurities being produced as the first distillation column bottoms.
Type:
Grant
Filed:
May 24, 2002
Date of Patent:
January 21, 2003
Assignee:
ChemCycles, Inc.
Inventors:
Heather K. Miles, Donald H. Westermann, Glenn F. Cunningham
Abstract: A method and apparatus for purifying acetonitrile from low grade acetonitriles. Low grade acetonitrile from DNA synthesis, HPLC and pharmaceutical drug manufacturing process wastes which comprise acetonitrile, a first set of impurities having a lower boiling temperature than acetonitrile and a second set of impurities having a boiling temperature greater than acetonitrile are processed to produce a purified acetonitrile by first introducing the low grade acetonitrile into a first distillation column and separating the acetonitrile and first set of impurities from the second set of impurities, the acetonitrile and first set of impurities being drawn as a vapor from the first distillation column, the second set of impurities being produced as the first distillation column bottoms.
Type:
Grant
Filed:
October 14, 1999
Date of Patent:
May 28, 2002
Assignee:
ChemCycles, Inc.
Inventors:
Heather K. Miles, Donald H. Westermann, Glenn F. Cunningham