Patents Assigned to Chemetall Foote Corporation
  • Patent number: 8057764
    Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.
    Type: Grant
    Filed: December 7, 2010
    Date of Patent: November 15, 2011
    Assignee: Chemetall Foote Corporation
    Inventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
  • Patent number: 7858057
    Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.
    Type: Grant
    Filed: April 17, 2009
    Date of Patent: December 28, 2010
    Assignee: Chemetall Foote Corporation
    Inventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
  • Patent number: 7547426
    Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.
    Type: Grant
    Filed: May 2, 2008
    Date of Patent: June 16, 2009
    Assignee: Chemetall Foote Corporation
    Inventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
  • Patent number: 7449161
    Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.
    Type: Grant
    Filed: February 14, 2007
    Date of Patent: November 11, 2008
    Assignee: Chemetall Foote Corporation
    Inventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
  • Patent number: 7390466
    Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.
    Type: Grant
    Filed: February 14, 2007
    Date of Patent: June 24, 2008
    Assignee: Chemetall Foote Corporation
    Inventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
  • Patent number: 7214355
    Abstract: Metal carbonates that are insoluble in water but that have a corresponding metal biocarbonate salt that is more than 75% by weight soluble in water are purified by preparing an aqueous slurry of the metal carbonate: introducing carbon dioxide gas to form a corresponding metal biocarbonate solution and heating that solution to form a purified metal carbonate and precipitate it.
    Type: Grant
    Filed: January 13, 2006
    Date of Patent: May 8, 2007
    Assignee: Chemetall Foote Corporation
    Inventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
  • Patent number: 7157065
    Abstract: A continuous process for directly preparing high purity lithium carbonate from lithium containing brines by preparing a brine containing about 6.0 wt % lithium and further containing other ions naturally occurring in brines; adding mother liquor containing carbonate to precipitate magnesium; adding a solution of CaO and sodium carbonate to remove calcium and any residual magnesium; precipitating lithium carbonate from the purified brine by adding soda ash solution; filtering to obtain solid lithium carbonate; preparing an aqueous slurry of the lithium carbonate and introducing carbon dioxide gas at a temperature from at least minus 10 to +40° C.; passing the lithium bicarbonate solution through a filter to clarify the solution; introducing said filtered lithium bicarbonate solution into a reactor and adjusting the temperature of the solution to from 60–100° C. to precipitate ultra-pure lithium carbonate.
    Type: Grant
    Filed: March 25, 2003
    Date of Patent: January 2, 2007
    Assignee: Chemetall Foote Corporation
    Inventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
  • Patent number: 6936229
    Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.
    Type: Grant
    Filed: November 7, 2000
    Date of Patent: August 30, 2005
    Assignee: Chemetall Foote Corporation
    Inventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
  • Patent number: 6921522
    Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.
    Type: Grant
    Filed: March 25, 2003
    Date of Patent: July 26, 2005
    Assignee: Chemetall Foote Corporation
    Inventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
  • Patent number: 6861011
    Abstract: Methyllithium is prepared by reacting chloromethane with a dispersion lithium metal in an aromatic organic solvent with methyltetrahydrofuran.
    Type: Grant
    Filed: November 7, 2003
    Date of Patent: March 1, 2005
    Assignee: Chemetall Foote Corporation
    Inventors: Mark J. Hintze, Jing Q. Wen
  • Patent number: 6497850
    Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.
    Type: Grant
    Filed: November 7, 2000
    Date of Patent: December 24, 2002
    Assignee: Chemetall Foote Corporation
    Inventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
  • Patent number: 6307079
    Abstract: Tin lithium compounds of the formula RR′R″SnGM′, wherein R, R′ and R″ may be the same or different and each comprises an alkyl, aryl, aralkyl or alkylaryl having from 1 to 15 carbon atoms and wherein each carbon atom may be unsubstituted or substituted, G is a substituted or unsubstituted branched, cyclic or straight chain hydrocarbon having from 1 to 20 carbon atoms, the substitutions comprising one or more aryl groups, and M′ is an alkali metal comprising Li, Na or K, are prepared. These compounds are useful as initiators in anionic polymerization reactions.
    Type: Grant
    Filed: September 17, 1999
    Date of Patent: October 23, 2001
    Assignee: Chemetall Foote Corporation
    Inventor: Mark J. Hintze
  • Patent number: 6207126
    Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.
    Type: Grant
    Filed: July 14, 1999
    Date of Patent: March 27, 2001
    Assignee: Chemetall Foote Corporation
    Inventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
  • Patent number: 6143260
    Abstract: A method for producing lithium carbonate by precipitating magnesium as the hydroxide from a brine concentrated to a lithium concentration of about 6%. Lithium is then precipitated from the brine by addition of recycled limed mother liquor from a previous lithium precipitation step.
    Type: Grant
    Filed: July 12, 1999
    Date of Patent: November 7, 2000
    Assignee: Chemetall Foote Corporation
    Inventor: Daniel A. Boryta