Patents Assigned to Chemetall Foote Corporation
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Patent number: 8057764Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.Type: GrantFiled: December 7, 2010Date of Patent: November 15, 2011Assignee: Chemetall Foote CorporationInventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
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Patent number: 7858057Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.Type: GrantFiled: April 17, 2009Date of Patent: December 28, 2010Assignee: Chemetall Foote CorporationInventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
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Patent number: 7547426Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.Type: GrantFiled: May 2, 2008Date of Patent: June 16, 2009Assignee: Chemetall Foote CorporationInventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
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Patent number: 7449161Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.Type: GrantFiled: February 14, 2007Date of Patent: November 11, 2008Assignee: Chemetall Foote CorporationInventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
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Patent number: 7390466Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.Type: GrantFiled: February 14, 2007Date of Patent: June 24, 2008Assignee: Chemetall Foote CorporationInventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
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Patent number: 7214355Abstract: Metal carbonates that are insoluble in water but that have a corresponding metal biocarbonate salt that is more than 75% by weight soluble in water are purified by preparing an aqueous slurry of the metal carbonate: introducing carbon dioxide gas to form a corresponding metal biocarbonate solution and heating that solution to form a purified metal carbonate and precipitate it.Type: GrantFiled: January 13, 2006Date of Patent: May 8, 2007Assignee: Chemetall Foote CorporationInventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
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Patent number: 7157065Abstract: A continuous process for directly preparing high purity lithium carbonate from lithium containing brines by preparing a brine containing about 6.0 wt % lithium and further containing other ions naturally occurring in brines; adding mother liquor containing carbonate to precipitate magnesium; adding a solution of CaO and sodium carbonate to remove calcium and any residual magnesium; precipitating lithium carbonate from the purified brine by adding soda ash solution; filtering to obtain solid lithium carbonate; preparing an aqueous slurry of the lithium carbonate and introducing carbon dioxide gas at a temperature from at least minus 10 to +40° C.; passing the lithium bicarbonate solution through a filter to clarify the solution; introducing said filtered lithium bicarbonate solution into a reactor and adjusting the temperature of the solution to from 60–100° C. to precipitate ultra-pure lithium carbonate.Type: GrantFiled: March 25, 2003Date of Patent: January 2, 2007Assignee: Chemetall Foote CorporationInventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
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Patent number: 6936229Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.Type: GrantFiled: November 7, 2000Date of Patent: August 30, 2005Assignee: Chemetall Foote CorporationInventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
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Patent number: 6921522Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.Type: GrantFiled: March 25, 2003Date of Patent: July 26, 2005Assignee: Chemetall Foote CorporationInventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
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Patent number: 6861011Abstract: Methyllithium is prepared by reacting chloromethane with a dispersion lithium metal in an aromatic organic solvent with methyltetrahydrofuran.Type: GrantFiled: November 7, 2003Date of Patent: March 1, 2005Assignee: Chemetall Foote CorporationInventors: Mark J. Hintze, Jing Q. Wen
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Patent number: 6497850Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.Type: GrantFiled: November 7, 2000Date of Patent: December 24, 2002Assignee: Chemetall Foote CorporationInventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
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Patent number: 6307079Abstract: Tin lithium compounds of the formula RR′R″SnGM′, wherein R, R′ and R″ may be the same or different and each comprises an alkyl, aryl, aralkyl or alkylaryl having from 1 to 15 carbon atoms and wherein each carbon atom may be unsubstituted or substituted, G is a substituted or unsubstituted branched, cyclic or straight chain hydrocarbon having from 1 to 20 carbon atoms, the substitutions comprising one or more aryl groups, and M′ is an alkali metal comprising Li, Na or K, are prepared. These compounds are useful as initiators in anionic polymerization reactions.Type: GrantFiled: September 17, 1999Date of Patent: October 23, 2001Assignee: Chemetall Foote CorporationInventor: Mark J. Hintze
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Patent number: 6207126Abstract: Methods and apparatus for the production of low sodium lithium carbonate and lithium chloride from a brine concentrated to about 6.0 wt % lithium are disclosed. Methods and apparatus for direct recovery of technical grade lithium chloride from the concentrated brine are also disclosed.Type: GrantFiled: July 14, 1999Date of Patent: March 27, 2001Assignee: Chemetall Foote CorporationInventors: Daniel Alfred Boryta, Teresita Frianeza Kullberg, Anthony Michael Thurston
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Patent number: 6143260Abstract: A method for producing lithium carbonate by precipitating magnesium as the hydroxide from a brine concentrated to a lithium concentration of about 6%. Lithium is then precipitated from the brine by addition of recycled limed mother liquor from a previous lithium precipitation step.Type: GrantFiled: July 12, 1999Date of Patent: November 7, 2000Assignee: Chemetall Foote CorporationInventor: Daniel A. Boryta