Abstract: Method for controlling perspiration, and kit for carrying out that method. The method involves the separate, sequential application of an AlCl.sub.3 -- or ZrCl.sub.4 -- containing antiperspirant composition and a physiologically tolerable basic buffer-containing composition. The kit involves separate applicators for applying the AlCl.sub.3 -- or ZrCl.sub.4 -- containing antiperspirant, and the buffer. Separate, successive application of the antiperspirant and the buffer prevents skin irritation or damage to the user's clothes attributable to acid formed from the antiperspirant, and provides antiperspirant activity which is equal or superior to previously known AlCl.sub.3 -- or ZrCl.sub.4 -- antiperspirants.