Patents Assigned to Donghua University
  • Patent number: 11966847
    Abstract: A method for constructing an efficient product surface defect detection model based on network collaborative pruning is provided. According to an initial product surface defect detection model, the method provides a network-based collaborative pruning method and constructs the efficient product surface defect detection model. On a premise of ensuring an accuracy of a product defect detection method, a product surface defect detection time is reduced to satisfy manufacturer's requirements on the product surface defect detection time and accuracy of product surface defects.
    Type: Grant
    Filed: November 16, 2020
    Date of Patent: April 23, 2024
    Assignee: DONGHUA UNIVERSITY
    Inventors: Jie Zhang, Junliang Wang, Xin Liu, Jinsong Bao
  • Publication number: 20240102204
    Abstract: A spinning solution, a heat-resistant creep-resistant fiber and preparation method therefor are provided. The spinning solution includes a polyethylene, a solvent and a photoinitiator, and the content of the photoinitiator is 0.2 wt %-10 wt % of the mass of the polyethylene; gel-spinning and multi-stage drafting the spinning solution; then performing ultraviolet irradiation by an ultraviolet light source to obtain a heat-resistant creep-resistant polyethylene fiber; the light intensity and the time of the ultraviolet light source is 100 W/cm2-5000 W/cm2 and 10 s-600 s, respectively; the gel content and the crystallinity of the heat-resistant creep-resistant polyethylene fiber is 20 wt %-100 wt % and 50 wt %-90 wt %, respectively; the creep rate of the fiber is 10?8 s?1-10?7 s?1 under conditions of a temperature of 70° C. and a load of 300 MPa; the fracture temperature of the fiber is 155° C.-245° C. under conditions of a load of 15 MPa and a heating rate of 2° C./min.
    Type: Application
    Filed: August 27, 2021
    Publication date: March 28, 2024
    Applicants: DONGHUA UNIVERSITY, JIANGSU LIU JIA TECHNOLOGY COMPANY LTD.
    Inventors: Yong HE, Zixian GUO, Jungu GUO, Yadong GUO, Xinpeng WANG, Chaoyang XIANG, Yimin WANG, Jianhua NI
  • Publication number: 20240052561
    Abstract: A digital control method is to accurately calculate the real-time addition amount of each dye in the solution replenishment system in the whole dyeing process based on the initial dyeing rate of each dye, and replenish the dye solution according to the real-time addition amount. A digital control system includes an automatic calculation K0,n value unit, a central processing unit and a replenishment pump. The automatic calculation K0,n value unit is composed of a dye solution concentration detection instrument, a sensor I and a BP neural network model. The BP neural network model is a BP neural network trained by a dye database. The automatic calculation K0,n value unit transmits the K0,n value to the central processing unit, calculates the replenishment amount through the central processing unit, and controls the replenishment pump to replenish the solution.
    Type: Application
    Filed: December 28, 2021
    Publication date: February 15, 2024
    Applicant: DONGHUA UNIVERSITY
    Inventors: Zhiping MAO, Yamin DAI, Hong XU, Yi ZHONG, Hui LU, Linping ZHANG, Xiaofeng SUI, Wei WU
  • Patent number: 11876232
    Abstract: A gas diffusion layer for proton exchange membrane fuel cell and preparation method thereof are provided. The preparation method is to papermake and dry carbon fiber suspension mainly composed of a fibrous binder, water, a dispersant and carbon fibers with different aspect ratios to obtain a carbon fiber base paper, and then carbonize and graphitize under the protection of nitrogen or inert gas to obtain a gas diffusion layer for proton exchange membrane fuel cell; where the fibrous binder is a composite fiber or a blend fiber composed of a phenolic resin and other resin; where the prepared gas diffusion layer for proton exchange membrane fuel cell has a pore gradient, and the layer with the smallest pore size is an intrinsic microporous layer.
    Type: Grant
    Filed: August 6, 2021
    Date of Patent: January 16, 2024
    Assignee: DONGHUA UNIVERSITY
    Inventors: Biao Wang, Tongqing Qu, Xiyi Huang
  • Publication number: 20230395815
    Abstract: A gas diffusion layer for proton exchange membrane fuel cell and preparation method thereof are provided. The preparation method is to papermake and dry carbon fiber suspension mainly composed of a fibrous binder, water, a dispersant and carbon fibers with different aspect ratios to obtain a carbon fiber base paper, and then carbonize and graphitize under the protection of nitrogen or inert gas to obtain a gas diffusion layer for proton exchange membrane fuel cell; where the fibrous binder is a composite fiber or a blend fiber composed of a phenolic resin and other resin; where the prepared gas diffusion layer for proton exchange membrane fuel cell has a pore gradient, and the layer with the smallest pore size is an intrinsic microporous layer.
    Type: Application
    Filed: August 6, 2021
    Publication date: December 7, 2023
    Applicant: DONGHUA UNIVERSITY
    Inventors: Biao WANG, Tongqing QU, Xiyi HUANG
  • Patent number: 11834781
    Abstract: The disclosure provides a method of continuous dyeing with reactive dyes in wet conditions, the method including: 1) adding fabric to a mixture of a dye liquor and an alkali through a one-bath-one-step method; 2) immersing the fabric pretreated in 1) in a padding liquor with an air film horizontal pad dyeing machine; 3) preheating the fabric after being treated in 2) at a temperature of 50-90° C.; and 4) rolling and batching the fabric after being treated in 3) at a temperature of 10-70° C. for 2-72 hours.
    Type: Grant
    Filed: July 20, 2021
    Date of Patent: December 5, 2023
    Assignees: HUAFANG CO., LTD, DONGHUA UNIVERSITY, BINZHOU HUA TEXTILE ENGINEERING TECHNOLOGY RESEARCH INSTITUTE CO., LTD.
    Inventors: Zhiping Mao, Hongyu Sun, Chunguang Li, Rongxia Jia, Yi Zhong, Hong Xu, Limin Wang, Qi Yu, Xiaomin Liu, Qingbo Lu, Chunying Sheng, Engang Lu, Qisheng Zhao, Wei Wu, Yamin Dai, Jinbo Wang
  • Publication number: 20230185148
    Abstract: A long-range electrochromic fiber for infrared camouflage and preparation method thereof are disclosed. The method includes: coating indium tin oxide dispersion, electrolyte solution, and electrochromic material on the surface of the metal fiber sequentially, and preparing counter electrodes and polymer protective layer on the outside of the electrochromic layer to obtain the long-range electrochromic fiber. The obtained long-range electrochromic fiber can realize the regulation of infrared emissivity, can be continuously prepared for more than 100 meters and has a good application prospect in infrared camouflage, wearable display, etc.
    Type: Application
    Filed: April 30, 2021
    Publication date: June 15, 2023
    Applicant: DONGHUA UNIVERSITY
    Inventors: Hongzhi WANG, Hongwei FAN, Yaogang LI, Qinghong ZHANG, Chengyi HOU
  • Publication number: 20220281174
    Abstract: A photo-curing three-dimensional printing preview method, comprising: obtaining the relationship of the conversion rate of a photosensitive resin system versus time under different curing conditions by measuring the relationship between the absorbance of the photosensitive resin system under different curing conditions and the time; fitting on experimental curves on the basis of a photo-curing kinetic equation by an iterative solution method, and obtaining a photo-curing kinetic constant of the photosensitive resin system; solving a photo-curing reaction kinetic differential equation set by using a fixed-step Euler method, and obtaining the relationship curves of the spatial distribution of each component content of the photosensitive resin system versus time; and conducting simulation printing, in conjunction with the relationship curves obtaining a space distribution of each component content in each layer of structure in a three-dimensional printing product after printing is completed, and completing a pho
    Type: Application
    Filed: November 14, 2019
    Publication date: September 8, 2022
    Applicants: Donghua University, Jiangsu Academy of Agricultural Sciences
    Inventors: Qingbao GUAN, Zhengwei YOU, Yi GAO, Yang ZHAO, Lei XU, Nina YAN
  • Patent number: 11421377
    Abstract: The present invention provides super-hydrophobic fabrics and a preparation method thereof, and belong to the field of textiles. The super-hydrophobic fabrics are obtained by finishing Pickering emulsion formed by amphiphilic particles stabilizing low-surface-energy substances in water. Via a one-step finishing method using Pickering emulsion technology, facile preparation of durable super-hydrophobic fabrics is realized. The static contact angle between the finished fabric surfaces and water droplets is greater than 150 degrees, and the water droplets can roll off easily; and after being subjected to 30 times of standard washing tests, the finished fabrics still maintains excellent water repellency. In addition, the Pickering emulsion preparation and finishing process of the present invention are environmentally friendly, pollution-free, facile to operate and widely applicable.
    Type: Grant
    Filed: August 16, 2017
    Date of Patent: August 23, 2022
    Assignee: DONGHUA UNIVERSITY
    Inventors: Zhiping Mao, Lingli Liu, Ruyi Xie, Xiaofeng Sui, Hong Xu, Linping Zhang, Yi Zhong
  • Patent number: 11414795
    Abstract: A stable conductive myocardial patch with a negative Poisson's ratio structure is provided. The preparation method includes preparing a myocardial patch substrate with concave polygons as the structural units by weaving or knitting, and then a conductive coating is coated on the surface of the substrate. Alternatively, the yarns can be processed into conductive coated yarns first, and then used as the raw material to weave or knit a stable conductive myocardial patch with a negative Poisson's ratio structure. The prepared myocardial patch has a relative resistance change of less than 5% at 50% tensile strain. When the strain of the structural units is within 50%, the fabric exhibits a negative Poisson's ratio structure, which expands in the perpendicular direction of the tensile load. The fabric exhibits a negative Poisson's ratio effect and anisotropy of Young's modulus, which matches the mechanical behavior of natural myocardium.
    Type: Grant
    Filed: May 19, 2021
    Date of Patent: August 16, 2022
    Assignee: DONGHUA UNIVERSITY
    Inventors: Jifu Mao, Yimeng Li, Yaya Gao, Chaojing Li, Fujun Wang, Lu Wang
  • Publication number: 20210404097
    Abstract: A stable conductive myocardial patch with a negative Poisson's ratio structure is provided. The preparation method includes preparing a myocardial patch substrate with concave polygons as the structural units by weaving or knitting, and then a conductive coating is coated on the surface of the substrate. Alternatively, the yarns can be processed into conductive coated yarns first, and then used as the raw material to weave or knit a stable conductive myocardial patch with a negative Poisson's ratio structure. The prepared myocardial patch has a relative resistance change of less than 5% at 50% tensile strain. When the strain of the structural units is within 50%, the fabric exhibits a negative Poisson's ratio structure, which expands in the perpendicular direction of the tensile load. The fabric exhibits a negative Poisson's ratio effect and anisotropy of Young's modulus, which matches the mechanical behavior of natural myocardium.
    Type: Application
    Filed: May 19, 2021
    Publication date: December 30, 2021
    Applicant: DONGHUA UNIVERSITY
    Inventors: Jifu MAO, Yimeng LI, Yaya GAO, Chaojing LI, Fujun WANG, Lu WANG
  • Publication number: 20210295165
    Abstract: A method for constructing an efficient product surface defect detection model based on network collaborative pruning is provided. According to an initial product surface defect detection model, the method provides a network-based collaborative pruning method and constructs the efficient product surface defect detection model. On a premise of ensuring an accuracy of a product defect detection method, a product surface defect detection time is reduced to satisfy manufacturer's requirements on the product surface defect detection time and accuracy of product surface defects.
    Type: Application
    Filed: November 16, 2020
    Publication date: September 23, 2021
    Applicant: Donghua University
    Inventors: Jie ZHANG, Junliang WANG, Xin LIU, Jinsong BAO
  • Patent number: 11124900
    Abstract: A type of flame-retardant cellulosic fiber and a preparation method thereof are disclosed. The preparation method includes extruding the cellulosic solution through a spinneret, coagulating, stretching, and water-washing to obtain a water-washed filament, which is then treated with a flame-retardant solution, and then rinsed and dried to prepare the flame-retardant cellulosic fiber. The water-washing temperature is ?90° C., the temperature of the flame-retardant solution during treatment is 60-90° C., and the rinsing temperature is 20-40° C. The flame retardant contains more than one of a group that forms a covalent bond with a hydroxy group of the cellulosic macromolecule, a group having the ability of self-crosslinking reaction, and a group that forms a hydrogen bond with a hydroxy group of the cellulosic macromolecule. The prepared flame-retardant cellulosic fiber is mainly composed of the cellulosic fiber matrix and the flame retardant dispersed in the matrix.
    Type: Grant
    Filed: October 14, 2019
    Date of Patent: September 21, 2021
    Assignee: DONGHUA UNIVERSITY
    Inventors: Tiehan Wang, Shiqiang Cui, Hong Jin, Yang Zhang, Yan Liu, Yumei Zhang
  • Publication number: 20210198813
    Abstract: A type of flame-retardant cellulosic fiber and a preparation method thereof are disclosed. The preparation method includes extruding the cellulosic solution through a spinneret, coagulating, stretching, and water-washing to obtain a water-washed filament, which is then treated with a flame-retardant solution, and then rinsed and dried to prepare the flame-retardant cellulosic fiber. The water-washing temperature is 90° C., the temperature of the flame-retardant solution during treatment is 60-90° C., and the rinsing temperature is 20-40° C. The flame retardant contains more than one of a group that forms a covalent bond with a hydroxy group of the cellulosic macromolecule, a group having the ability of self-crosslinking reaction, and a group that forms a hydrogen bond with a hydroxy group of the cellulosic macromolecule. The prepared flame-retardant cellulosic fiber is mainly composed of the cellulosic fiber matrix and the flame retardant dispersed in the matrix.
    Type: Application
    Filed: October 14, 2019
    Publication date: July 1, 2021
    Applicant: DONGHUA UNIVERSITY
    Inventors: Tiehan WANG, Shiqiang CUI, Hong JIN, Yang ZHANG, Yan LIU, Yumei ZHANG
  • Patent number: 11041084
    Abstract: A finishing method for reactive dye inkjet printing based on a cationic modifier includes: using the inkjet printing method to spray print the cationic modifier ink and the reactive dye ink on the cellulose fiber fabrics' pattern area after being subjected to sizing treatment, then subjecting the fabrics to steaming or baking treatment, and subjecting the fabrics to soaping to get the reactive dye inkjet printing fabrics. The timespan of spray printing the cationic modifier ink and reactive dye ink is 0-2 min. Cationic modifier ink includes 1.0-60.0 wt % cationic modifier. The cationic modifier refers to the molecular whose structure contains reactive group and positive charge group and the number average molecular weight of 100-30000. The reactive group is one or more in the group containing epoxy group, triazine, pyridine, and olefin. The positive charge group is one or more in the group containing quaternary ammonium salt, and ammonium chloride.
    Type: Grant
    Filed: November 2, 2018
    Date of Patent: June 22, 2021
    Assignee: DONGHUA UNIVERSITY
    Inventors: Kelu Yan, Lei Wang
  • Publication number: 20200317943
    Abstract: A finishing method for reactive dye inkjet printing based on a cationic modifier includes: using the inkjet printing method to spray print the cationic modifier ink and the reactive dye ink on the cellulose fiber fabrics' pattern area after being subjected to sizing treatment, then subjecting the fabrics to steaming or baking treatment, and subjecting the fabrics to soaping to get the reactive dye inkjet printing fabrics. The timespan of spray printing the cationic modifier ink and reactive dye ink is 0-2 min. Cationic modifier ink includes 1.0-60.0 wt % cationic modifier. The cationic modifier refers to the molecular whose structure contains reactive group and positive charge group and the number average molecular weight of 100-30000. The reactive group is one or more in the group containing epoxy group, triazine, pyridine, and olefin. The positive charge group is one or more in the group containing quaternary ammonium salt, and ammonium chloride.
    Type: Application
    Filed: November 2, 2018
    Publication date: October 8, 2020
    Applicant: DONGHUA UNIVERSITY
    Inventors: Kelu YAN, Lei WANG
  • Publication number: 20200224361
    Abstract: The present invention provides super-hydrophobic fabrics and a preparation method thereof, and belong to the field of textiles. The super-hydrophobic fabrics are obtained by finishing Pickering emulsion formed by amphiphilic particles stabilizing low-surface-energy substances in water. Via a one-step finishing method using Pickering emulsion technology, facile preparation of durable super-hydrophobic fabrics is realized. The static contact angle between the finished fabric surfaces and water droplets is greater than 150 degrees, and the water droplets can roll off easily; and after being subjected to 30 times of standard washing tests, the finished fabrics still maintains excellent water repellency. In addition, the Pickering emulsion preparation and finishing process of the present invention are environmentally friendly, pollution-free, facile to operate and widely applicable.
    Type: Application
    Filed: August 16, 2017
    Publication date: July 16, 2020
    Applicant: DONGHUA UNIVERSITY
    Inventors: Zhiping MAO, Lingli LIU, Ruyi XIE, Xiaofeng SUI, Hong XU, Linping ZHANG, Yi ZHONG
  • Patent number: 9644290
    Abstract: Processes for producing carbon fiber, the filament thereof and pre-oxidized fiber are provided. In one embodiment, the gel spinning of polyacrylonitrile filament is achieved by using small-molecule gelling agent, and the carbon fiber obtained thereby is increased by 15% to 40% in tensile strength and by 20% to 35% in toughness. In another embodiment, the melt spinning process of polyacrylonitrile is conducted by using imidazole type ion liquid as plasticizer, the process reduces environment pollution, is suitable for industrial production and the fiber produced thereby is improved in its strength. In yet another embodiment, polyacrylonitrile pre-oxidized fiber is produced by melt spinning, so low cost and controllable pre-oxidization of polyacrylonitrile can be achieved. In a further embodiment, high strength carbon fiber is manufactured by using polymer thickening agent.
    Type: Grant
    Filed: October 20, 2014
    Date of Patent: May 9, 2017
    Assignee: Donghua University
    Inventors: Muhuo Yu, Huaiping Rong, Keqing Han, Zhaohua Wang, Yincai Tian, Hui Zhang
  • Patent number: 9476147
    Abstract: Processes for producing carbon fiber, the filament thereof and pre-oxidized fiber are provided. In one embodiment, the gel spinning of polyacrylonitrile filament is achieved by using small-molecule gelling agent, and the carbon fiber obtained thereby is increased by 15% to 40% in tensile strength and by 20% to 35% in toughness. In another embodiment, the melt spinning process of polyacrylonitrile is conducted by using imidazole type ion liquid as plasticizer, the process reduces environment pollution, is suitable for industrial production and the fiber produced thereby is improved in its strength. In yet another embodiment, polyacrylonitrile pre-oxidized fiber is produced by melt spinning, so low cost and controllable pre-oxidization of polyacrylonitrile can be achieved. In a further embodiment, high strength carbon fiber is manufactured by using polymer thickening agent.
    Type: Grant
    Filed: October 20, 2014
    Date of Patent: October 25, 2016
    Assignee: DONGHUA UNIVERSITY
    Inventors: Muhuo Yu, Huaiping Rong, Keqing Han, Yiwei Zhang, Yincai Tian, Qinli Dong, Hui Zhang
  • Patent number: 9428850
    Abstract: Processes for producing carbon fiber, the filament thereof and pre-oxidized fiber are provided. In one embodiment, the gel spinning of polyacrylonitrile filament is achieved by using small-molecule gelling agent, and the carbon fiber obtained thereby is increased by 15% to 40% in tensile strength and by 20% to 35% in toughness. In another embodiment, the melt spinning process of polyacrylonitrile is conducted by using imidazole type ion liquid as plasticizer, the process reduces environment pollution, is suitable for industrial production and the fiber produced thereby is improved in its strength. In yet another embodiment, polyacrylonitrile pre-oxidized fiber is produced by melt spinning, so low cost and controllable pre-oxidization of polyacrylonitrile can be achieved. In a further embodiment, high strength carbon fiber is manufactured by using polymer thickening agent.
    Type: Grant
    Filed: October 20, 2014
    Date of Patent: August 30, 2016
    Assignee: DONGHUA UNIVERSITY
    Inventors: Muhuo Yu, Huaiping Rong, Keqing Han, Zhaohua Wang, Yiwei Zhang, Qinli Dong