Patents Assigned to EASYL
  • Patent number: 11235979
    Abstract: Disclosed is a method for manufacturing crystals of aluminates of one or more element(s) other than aluminium, referred to as “A. The method includes: placing starting reagents, including at least one aluminium element source and a source of the element(s) A that has a degree of oxidation of between 1 and 6, in suspension in a liquid medium, forming a suspension referred to as the “starting suspension”; milling the starting suspension at ?50° C., in a three-dimensional liquid medium ball mill for ?5 minutes; recovering, at the outlet of the three-dimensional ball mill, a suspension referred to as the “end suspension” including the starting reagents in activated form or crystals of aluminate of the element(s) A generally in hydrated form; if required, calcination of the end suspension when it includes the starting reagents in activated form, to obtain generally non-hydrated crystals of aluminate of the element(s) A.
    Type: Grant
    Filed: October 5, 2017
    Date of Patent: February 1, 2022
    Assignee: EASYL
    Inventors: François Lacoste, Valentin Lair, Julien Thiel, Samy Halloumi
  • Patent number: 10941094
    Abstract: A method for manufacturing calcium diglyceroxide crystals includes at least the following steps: placing at least one calcium element source compound, in particular calcium oxide, in suspension in glycerol or in a homogeneous mixture of glycerol and an anhydrous solvent of glycerol, in particular methanol, referred to as the “starting suspension”, the molar ratio being greater than or equal to 2; milling the starting suspension at an ambient temperature of less than or equal to 50° C. in a three-dimensional liquid-phase ball mill for a holding time of 15 minutes or less; recovering, at the outlet of the mill, a suspension of calcium diglyceroxide crystals, and optionally, washing the obtained suspension with a glycerol solvent in order to eliminate any excess glycerol, optionally, drying the suspension of calcium diglyceroxide crystals so as to obtain a powder of calcium diglyceroxide crystals. Also disclosed are uses associated with the calcium diglyceroxide crystals.
    Type: Grant
    Filed: September 29, 2017
    Date of Patent: March 9, 2021
    Assignee: EASYL
    Inventors: François Lacoste, Valentin Lair, Julien Thiel, Samy Halloumi
  • Patent number: 10533145
    Abstract: A method for producing fatty acid alkyl esters and glycerol implementing a set of transesterification reactions between at least one vegetable or animal oil and at least one aliphatic monoalcohol includes: introducing, into a three-dimensional microball mill at least one vegetable and/or animal oil, at least one aliphatic monoalcohol and at least one heterogenous and/or homogenous catalyst in order to form an initial mixture; grinding the initial mixture at a temperature?50° C., in a three-dimensional microball mill, for a residence time?5 minutes; recovering, at the outlet of the three-dimensional mill, a final mixture including at least fatty acid alkyl esters, glycerol, the catalyst and the aliphatic monoalcohol that has not reacted; and separating this final mixture of a first phase including the fatty acid alkyl esters and of a second phase including the glycerol, the aliphatic monoalcohol that has not reacted and the catalyst.
    Type: Grant
    Filed: June 30, 2017
    Date of Patent: January 14, 2020
    Assignee: EASYL
    Inventors: François Lacoste, Julien Thiel, Valentin Lair, Samy Halloumi
  • Patent number: 10472248
    Abstract: Disclosed is a method for manufacturing calcium zincate crystals including: placing calcium hydroxide2 and zinc oxide, one of the precursors thereof, or one of the water mixtures thereof in a starting suspension, the mass ratio of water to calcium hydroxide and zinc oxide, or one of the precursors or mixtures thereof, being greater than or equal to 1; milling the starting suspension to an ambient temperature less than or equal to 50° C. in a wet-phase three-dimensional micro-ball mill for a residence time less than or equal to 15 minutes and in particular from 5 to 25 seconds; recovering a calcium zincate crystal suspension coming out of the mill; and optionally, concentrating or drying the calcium zincate crystal suspension so as to obtain a calcium zincate crystal powder. Also disclosed are uses associated with the calcium zincate crystals obtained according to the method described above.
    Type: Grant
    Filed: March 31, 2016
    Date of Patent: November 12, 2019
    Assignee: EASYL
    Inventors: Francois Lacoste, Julien Thiel
  • Publication number: 20180086646
    Abstract: Disclosed is a method for manufacturing calcium zincate crystals including: placing calcium hydroxide2 and zinc oxide, one of the precursors thereof, or one of the water mixtures thereof in a starting suspension, the mass ratio of water to calcium hydroxide and zinc oxide, or one of the precursors or mixtures thereof, being greater than or equal to 1; milling the starting suspension to an ambient temperature less than or equal to 50° C. in a wet-phase three-dimensional micro-ball mill for a residence time less than or equal to 15 minutes and in particular from 5 to 25 seconds; recovering a calcium zincate crystal suspension coming out of the mill; and optionally, concentrating or drying the calcium zincate crystal suspension so as to obtain a calcium zincate crystal powder. Also disclosed are uses associated with the calcium zincate crystals obtained according to the method described above.
    Type: Application
    Filed: March 31, 2016
    Publication date: March 29, 2018
    Applicant: EASYL
    Inventors: Francois LACOSTE, Julien THIEL