Abstract: A method produces calcium fulvate from naturally-occurring humus material, such as leonardite, or humic shales. The humus material containing solid fulvic acid and solid humic acid is mixed with water and sodium hydroxide for a first selected period of time to form a solution having a pH of approximately 10.0 thereby solubilizing the fulvic acid and the humic acid. The pH of the solution is reduced to approximately 4.5 and is maintained at the approximately pH 4.5 for second selected period of time thereby precipitating the humic acid as a solid while the fulvic acid remains in solution. The fulvic acid solution is separated from the solid humic acid. The pH of the fulvic acid solution is increased to approximately 13 with calcium hydroxide thereby precipitating the solubilized fulvic acid as calcium fulvate.
Abstract: A method produces magnesium fulvate from naturally-occurring humus material, such as leonardite, or humic shales. The humus material containing solid fulvic acid and solid humic acid is mixed with water and sodium hydroxide for a first selected period of time to form a solution having a pH of approximately 10.0 thereby solubilizing the fulvic acid and the humic acid. The pH of the solution is reduced to approximately 4.5 and is maintained at the approximately pH 4.5 for second selected period of time thereby precipitating the humic acid as a solid while the fulvic acid remains in solution. The fulvic acid solution is separated from the solid humic acid. The pH of the fulvic acid solution is increased to approximately 13 with magnesium hydroxide thereby precipitating the solubilized fulvic acid as magnesium fulvate.
Abstract: An internally threaded insert having a knurled outer surface is positioned in an aperture formed in a cover for a capacitor. This provides an antitwist characteristic between the insert and the walls of the aperture to facilitate a seal between the two. An electrical terminal can then be threaded into the insert to electrically connect it to an internal lead of the capacitor. A bushing is also carried in the aperture to provide a seal between the insert and the cover. The insert has a tenon which includes a shoulder providing large and small diameters. The large diameter tenon is deformed to provide a washer and seal at and around the insert at the aperture. After placement of the internal capacitor lead over the formed washer around the insert, the smaller diameter tenon is deformed to provide a rivet head over the lead to hold it in place.
Type:
Grant
Filed:
April 2, 1987
Date of Patent:
July 5, 1988
Assignee:
501 Electrolytics, Inc.
Inventors:
Josef K. Limanowski, Thomas L. Arnold, C. Wayne Hodges