Abstract: To avoid the degradation of thioacetic acid on storage, from 0.005 to 0.5% of a chloroacetic acid, preferably dichloroacetic acid, is added thereto.
Abstract: This process for the synthesis of 3-mercaptopropionic acid esters by addition reaction of H.sub.2 S to the corresponding acrylic acid ester is carried out in the presence of a solid-support functionalized with basic guanidine functional groups, on condition that these groups are free of hydrogen that is directly attached to a nitrogen atom.
Type:
Grant
Filed:
November 21, 1997
Date of Patent:
July 6, 1999
Assignee:
Elf Acquitaine Exploration Production France
Abstract: This process for the synthesis of 3-mercaptopropionic acid by an addition reaction of H.sub.2 S with acrylic acid is carried out in the presence of a solid support having basic guanidine functional groups, provided that the latter do not contain hydrogen bonded directly to a nitrogen atom.
Type:
Grant
Filed:
September 19, 1997
Date of Patent:
March 2, 1999
Assignee:
Elf Acquitaine Exploration Production France