Abstract: The present invention relates to a process for purifying a recycle base solution waste stream of a composition comprising a quaternary ammonium hydroxide comprising the steps of (a) providing an electrolysis cell which comprises an anolyte compartment containing an anode, a catholyte compartment containing a cathode, and a cation-selective membrane separating the anolyte and catholyte compartments, (b) charging the recycle base solution waste stream comprising the quaternary ammonium hydroxide to be purified to the anolyte compartment and charging water, optionally containing a quaternary ammonium hydroxide, to the catholyte compartment, (c) passing a current through the electrolysis cell to produce a purified aqueous quaternary ammonium hydroxide solution in the catholyte compartment, (d) recovering the purified aqueous quaternary ammonium hydroxide solution from the catholyte compartment, (e) washing the anolyte compartment with a suitable solvent, and (f) repeating steps (b)-(e).
Type:
Grant
Filed:
October 7, 2002
Date of Patent:
November 2, 2010
Assignee:
Flexsys B.V.
Inventors:
Fred Korpel, Gerrit Jan Boerman, Roger Keranen Rains
Abstract: A process for enhancing the melt strength of polypropylene includes the steps of: mixing the polypropylene with at least 0.1-8 wt. % of an oligomer of maleimide or a derivative thereof, based on the amount of polypropylene, completely or substantially in the absence of peroxide; reacting the polypropylene and oligomer of maleimide or a derivative thereof at a temperature between 150° C. and 300° C.
Type:
Application
Filed:
August 18, 2004
Publication date:
October 5, 2006
Applicant:
Flexsys B.V.
Inventors:
Lambertus Gerhardus Olde Hanter, Ludwig Eisenhuth, Arie De Hoog, Peter Schneider, Wasil Maslow
Abstract: The present invention relates to a process for improving the purity of a composition comprising a quaternary ammonium hydroxide comprising the steps of (a) providing an electrolysis cell which comprises an anolyte compartment containing an anode, a catholyte compartment containing a cathode, and at least one intermediate compartment, said at least one intermediate compartment being separated from the anolyte and catholyte compartments by cation selective membranes, (b) charging water, optionally containing a supporting electrolyte, to the anolyte compartment, charging water, optionally containing a quaternary ammonium hydroxide, to the catholyte compartment, and charging the composition comprising the quaternary ammonium hydroxide to be purified to the intermediate compartment, (c) passing a current through the electrolysis cell to produce a purified aqueous quaternary ammonium hydroxide solution in the catholyte compartment, and (d) recovering the purified aqueous quaternary ammonium hydroxide solution from
Type:
Grant
Filed:
October 16, 2001
Date of Patent:
August 3, 2004
Assignee:
Flexsys B.V.
Inventors:
Anna Giatti, Fred Korpel, Roger Keranen Rains, Gerrit Jan Boerman
Abstract: The invention relates to a process for preparing a thiuram disulfide comprising reacting a secondary amine with carbon disulfide in the presence of oxygen and a metal catalyst in the absence of a solvent using a secondary amine of which the corresponding thiuram disulfide is liquid under the reaction conditions. The invention also pertains to the use of said thiuram disulfides as vulcanization accelerators or lubricant oil additives.
Type:
Grant
Filed:
October 19, 2001
Date of Patent:
October 15, 2002
Assignee:
Flexsys B.V.
Inventors:
Robertus Hermanus Jozef Bloemenkamp, Antonius Johannes van Hengstum
Abstract: The invention relates to a vulcanizable rubber composition comprising a rubber, sulfur or a sulfur donor, a vulcanization accelerator, a protective agent and 0.1 phr or more of an N,N′-disubstituted p-phenylenediamine protective agent is present in the form of a salt with an acid, and the composition does not comprise an elastomeric copolymer having glycidyl groups. The invention also relates to a vulcanization process comprising mixing and heating said rubber composition and to an article of manufacture comprising the rubber vulcanizate obtained by said process. Preferably, the acid is a C1-C24 monocarboxylic acid or a C2-C24 dicarboxylic acid, more preferably a C12-C20 fatty acid such as stearic acid. Most preferably, the protective agent is 6PPD.