Patents Assigned to FPInnovations
  • Patent number: 11834785
    Abstract: The present invention is directed to a method of transforming a pulp fibrous into a pre-dispersed semi-dry or dry fibrous material and to the material produced. The method opens, de-entangles and fibrillates the fibrous material of the input pulp. The method mixes the input fibrous with chemicals while evaporating moisture in an updated mechanical disc refiner process. The refiner operates to set three process variables: 1) applied refining specific energy; 2) refiner gap opening and 3) refiner output consistency. Depending on the feed pulp type and consistency, the refiner's output is a pre-dispersed semi-dry fibrous material of 30 to 99% solids with 70 to 100% of separated fibers that depending on chemical treatment are loosely entangled fibrous that disperse in water using common techniques. The pre-dispersed semi-dry output may be further processed inline or by batch process air agitation at velocities sufficient to further separate fibers and loosen fibrous entanglements.
    Type: Grant
    Filed: September 14, 2017
    Date of Patent: December 5, 2023
    Assignee: FPInnovations
    Inventors: Makhlouf Laleg, Lahoucine Ettaleb, Michael Stacey
  • Patent number: 11802183
    Abstract: The present relates to a process for the depolymerization of lignin using chemicals recoverable by the soda or kraft mill recovery cycles. The process involves the use of sodium hydroxide or white liquor to depolymerize lignin in black liquor or other lignins (e.g. hydrolysis lignin, kraft lignin) by conducting the reaction at 170-250° C. for up to 3 hours in the presence or absence of a co-solvent and a capping agent. The depolymerized lignin is then obtained by acidifying the reaction products to a low pH to precipitate the de-polymerized lignin, followed by particle coagulation, cake filtration and washing with acid and water to obtain a purified depolymerized lignin product.
    Type: Grant
    Filed: May 8, 2018
    Date of Patent: October 31, 2023
    Assignee: FPInnovations
    Inventors: Michael Paleologou, Zaid Ahmad, Chunbao Xu
  • Patent number: 11753770
    Abstract: The present disclosure is directed to a Pickering emulsion comprising cellulose filaments. The heterogeneity of the cellulose filament material is critical and beneficial to the formation of stable emulsions. Emulsions with high stability can be prepared by controlling the CF surface properties. It is provided an emulsion comprising an internal phase dispersed in a continuous external phase and cellulose filaments located at the interface of the internal phase and the external phase, wherein the emulsion comprises 50% in volume or more of the internal phase and a method of producing same.
    Type: Grant
    Filed: June 16, 2017
    Date of Patent: September 12, 2023
    Assignee: FPInnovations
    Inventors: Wadood Yasser Hamad, Chuanwei Miao
  • Patent number: 11708304
    Abstract: The present provides a concrete and mortar mix and composition thereof with poor quality sand such as desert sand, hydraulic binder (cement) and filamentous cellulose, where the desert sand/spherical sand replaces conventional concrete river sands. The present disclosure also relates a filamentous cellulose, such as, cellulose filaments (CF), cellulose nano filaments, cellulose nanofibrils (CNF) and microfibrillated cellulose (MFC) as a concrete/mortar and sand adhesion additive with hydraulic binder (cement), and to a method of making the concrete. This method also relates to a method to prevent the sliding of individual sand grains against one another and therefor similarly contributes to the stabilization of the building materials.
    Type: Grant
    Filed: February 12, 2019
    Date of Patent: July 25, 2023
    Assignee: FPINNOVATION
    Inventors: Eric Olivier, Xiaolin Cai, Carole Larouche, Xiaoyu Wang
  • Patent number: 11441265
    Abstract: Methods and systems for controlling operation of a smelt dissolving tank receiving a flow of smelt and having a vent stack in fluid communication are provided. A dissolving liquid is injected into the smelt dissolving tank at a predetermined injection rate. A temperature of a flow of vapour in the vent stack is measured with a sensor. The injection rate of the dissolving liquid is controlled based on the temperature of the flow of vapour.
    Type: Grant
    Filed: May 1, 2018
    Date of Patent: September 13, 2022
    Assignee: FPInnovations
    Inventors: Bruce James Allison, Wei Ren, Brennan Dubord, Jason Johnson
  • Patent number: 11401252
    Abstract: The present invention relates to a method of producing furfural and extracting lignin from a hemi-cellulosic biomass solution comprising a total quantity of C5 sugars, comprising the steps of heating the hemi-cellulosic biomass solution to a temperature of at least about 200° C.; acidifying the hemi-cellulosic biomass solution with acid to produce the furfural in vapor phase; and condensing the furfural to recover furfural in solution, wherein the furfural is produced at a total molar yield of at least 70% of moles of furfural produced/the total moles C5 sugars present in the initial hemi-cellulosic biomass solution. Low molecular weight lignin can also be recovered from the hemi-cellulosic biomass solution prior to furfural production by membrane concentration, acidification, coagulation and filtration.
    Type: Grant
    Filed: April 20, 2017
    Date of Patent: August 2, 2022
    Assignee: FPInnovations
    Inventors: Naceur Jemaa, Adil Mazar, Waleed Wafa Al Dajani, Michael Paleologou
  • Patent number: 11333561
    Abstract: A temperature sensor device and a system for measuring temperature of a fast moving surface are described herein. A sensor body comprising a temperature sensor for measuring temperature of the moving surface. The sensor body has an engagement surface for contacting the moving surface. A biasing mechanism is coupled to the sensor body for providing pressure to maintain the engagement surface in contact with moving surface and for allowing the engagement surface to pivot with the moving surface when the moving surface deflects. An electronics module is connected to the temperature sensor for determining temperature data indicative of the temperature of the moving surface and for transmitting the temperature data to an external device. The temperature sensor device and/or the system may be used for measuring temperature of a saw blade.
    Type: Grant
    Filed: May 16, 2019
    Date of Patent: May 17, 2022
    Assignee: FPInnovations
    Inventors: Tomo Bonac, Bruce Lehmann, Ahmad Mohammadpanah
  • Patent number: 11306206
    Abstract: A composite and method for producing the composite by incorporating wood or wood pulp fibres with a suitable thermoplastic polymer and coupling agent are described. Homogeneous, void-free transparent/translucent thermoplastic materials in the form of pellets, films or three-dimensional moldable products are produced. The wood pulp fibres can be discrete natural fibres, and flexible assemblies of nano to micro elements, e.g., assemblies of aggregated carbon nanotubes. It is also possible to use our vacuum-assisted co-extrusion process to produce hybrid composites comprising the wood pulp fibre and a further rigid fibre, like glass or carbon fibres, and a flexible fibre or fibrillar network, like cellulose fibres or cellulose filaments. The thermoplastic resin can be, but not limited to, polyolefins, like polypropylene or polyethylene, or polyesters, like polylactic acid, or co-polymers, like acrylonitrile-butadiene-styrene terpolymer.
    Type: Grant
    Filed: July 25, 2017
    Date of Patent: April 19, 2022
    Assignee: FPInnovations
    Inventors: Wadood Yasser Hamad, Shunxing Su, Norman Roberts, Otman Oulanti, Michelle Agnes Ricard, Chuanwei Miao
  • Patent number: 11220446
    Abstract: An acidic water-based process was developed for the synthesis of anionic lignin copolymers with adjustable MW, thermal stability and solubility in water. The anionic lignin copolymer described herein comprises: a molecular weight of 5,000 to 7.4×105 g/mol; and a charge density of ?1 to ?7.2 meq/g. The anionic lignin copolymers described herein which have a molecular weight range of 000-50,000 g/mol can be used as dispersants of negatively charged molecules or particles in numerous process or wastewater streams (e.g. concrete admixtures, gypsum slurries, textile dye) while such copolymers in a molecular weight range of 90,000-740,000 g/mole can be used as flocculants of positively charged molecules or particles in numerous process and wastewater streams including industrial and municipal systems and sludge dewatering in the textile dye, pulp & paper, mining and oil industries.
    Type: Grant
    Filed: March 7, 2018
    Date of Patent: January 11, 2022
    Assignee: FPInnovations
    Inventors: Pedram Fatehi, Fangong Kong, Shoujuan Wang, Jacquelyn Price, Michael Paleologou
  • Publication number: 20210285156
    Abstract: The present invention is directed to a method of transforming a pulp fibrous into a pre-dispersed semi-dry or dry fibrous material and to the material produced. The method opens, de-entangles and fibrillates the fibrous material of the input pulp. The method mixes the input fibrous with chemicals while evaporating moisture in an updated mechanical disc refiner process. The refiner operates to set three process variables: 1) applied refining specific energy; 2) refiner gap opening and 3) refiner output consistency. Depending on the feed pulp type and consistency, the refiner's output is a pre-dispersed semi-dry fibrous material of 30 to 99% solids with 70 to 100% of separated fibers that depending on chemical treatment are loosely entangled fibrous that disperse in water using common techniques. The pre-dispersed semi-dry output may be further processed inline or by batch process air agitation at velocities sufficient to further separate fibers and loosen fibrous entanglements.
    Type: Application
    Filed: September 14, 2017
    Publication date: September 16, 2021
    Applicant: FPInnovations
    Inventors: Makhlouf LALEG, Lahoucine ETTALEB, Michael STACEY
  • Publication number: 20210198434
    Abstract: A water-based process was developed for the synthesis of aminated lignin copolymers with high MW, thermal stability and solubility in water over a wide range of p H values. The cationic lignin copolymer described herein comprises: a grafting ratio of (weight of cationic amine compound)/(weight of lignin) of 70 to 200% and a charge density of +1.4-3.0 meq/g. This cationic lignin copolymer can be used as a flocculant in numerous wastewater streams including municipal and industrial systems and sludge dewatering in the pulp & paper, mining and oil industries.
    Type: Application
    Filed: March 7, 2018
    Publication date: July 1, 2021
    Applicants: FPInnovations, LAKEHEAD UNIVERSITY
    Inventors: Pedram FATEHI, Shoujuan WANG, Jacquelyn PRICE, Naceur JEMAA, Talat MAHMOOD, Michael PALEOLOGOU
  • Publication number: 20210010200
    Abstract: Methods and systems for controlling operation of a smelt dissolving tank receiving a flow of smelt and having a vent stack in fluid communication are provided. A dissolving liquid is injected into the smelt dissolving tank at a predetermined injection rate. A temperature of a flow of vapour in the vent stack is measured with a sensor. The injection rate of the dissolving liquid is controlled based on the temperature of the flow of vapour.
    Type: Application
    Filed: May 1, 2018
    Publication date: January 14, 2021
    Applicant: FPInnovations
    Inventors: Bruce James ALLISON, Wei REN, Brennan DUBORD, Jason JOHNSON
  • Patent number: 10858554
    Abstract: Most processes currently being proposed and/or used for the production of lignin from kraft or soda black liquors are capable of producing two main types of lignin: high residual content (HRC) lignin and low residual content (LRC) lignin. Surprisingly, it was discovered that HRC lignin, is a suitable ingredient in alkaline adhesives, particularly wood adhesives of the phenolic type (e.g. resole resins). This biomaterial is environmentally green and remarkably low cost, which makes it an industrially viable material to be used as a novel and major ingredient in phenolic adhesives for the manufacture of exterior grade plywood, laminated veneer lumber, oriented strand board (OSB) and other wood products—this was successfully demonstrated in a number of laboratory experiments as well as several different mill trials. The composition, preparation and application of such wood adhesives are hereby disclosed.
    Type: Grant
    Filed: April 15, 2016
    Date of Patent: December 8, 2020
    Assignee: FPInnovations
    Inventors: Martin W. Feng, Guangbo He, Yaolin Zhang, Xiang-Ming Wang, Lamfeddal Kouisni, Michael Paleologou
  • Publication number: 20200325111
    Abstract: The present invention relates to a method of producing furfural and extracting lignin from a hemi-cellulosic biomass solution comprising a total quantity of C5 sugars, comprising the steps of heating the hemi-cellulosic biomass solution to a temperature of at least about 200° C.; acidifying the hemi-cellulosic biomass solution with acid to produce the furfural in vapor phase; and condensing the furfural to recover furfural in solution, wherein the furfural is produced at a total molar yield of at least 70% of moles of furfural produced/the total moles C5 sugars present in the initial hemi-cellulosic biomass solution. Low molecular weight lignin can also be recovered from the hemi-cellulosic biomass solution prior to furfural production by membrane concentration, acidification, coagulation and filtration.
    Type: Application
    Filed: April 20, 2017
    Publication date: October 15, 2020
    Applicant: FPInnovations
    Inventors: Naceur JEMAA, Adil MAZAR, Waleed WAFA AL DAJANI, Michael PALEOLOGOU
  • Patent number: 10801051
    Abstract: A fractionation process for producing value-added products from a lignocellulosic biomass, comprises: a) mechanically refining the lignocellulosic biomass under mild refining conditions to form a refined biomass pulp with enhanced susceptibility to separation of hemicellulose, cellulose and lignin, and enhanced digestibility of carbohydrates in hydrolysis b) separating hemicellulose and sulfur-free high-quality lignin from cellulose in the refined biomass, and, optionally c) producing various bioproducts from the above said process.
    Type: Grant
    Filed: January 17, 2017
    Date of Patent: October 13, 2020
    Assignee: FPInnovations
    Inventors: Zhirun Yuan, Thomas Carl Browne, Xiao Zhang
  • Publication number: 20200207663
    Abstract: Cement composite boards comprising cellulose filaments (CF) and/or CF-containing pulp, are described. The composite boards have at least an improved modulus of rupture when compared with similar board that are free of CF. Methods for producing the CF and/or CF-containing pulp reinforced cement boards are also described. The CF cement composite board comprises: cellulose filaments (CF) and/or CF-containing pulp, and cement, wherein the CF has an aspect ratio of 200 to 5000, comprising a weight % of CF is from 1% to 20% by weight of the composite board. The composite boards herein described may have a modulus of rupture of more than 7 MPa.
    Type: Application
    Filed: May 18, 2018
    Publication date: July 2, 2020
    Applicant: FPInnovations
    Inventors: Xiaolin CAI, Yuxia BEN, Xujun HUA, Michelle RICARD, Carole LAROUCHE, Xiang-Ming WANG
  • Publication number: 20200189242
    Abstract: There is provided a sound insulating mat for sound insulation comprising at least a layer of combined natural fibers-binder web. The web comprises natural fibers in the range of 60 to 9 wt. % of the web; and a synthetic binder in the range of 5 to 40 wt. % of the web. The web comprises a thickness and at least an upper surface and a lower surface opposite each other, and has a bulk density of 40 to 150 kg/m3. There is also provided a method for manufacturing the sound insulating mat and a noise control system comprising the sound insulating mat.
    Type: Application
    Filed: December 13, 2017
    Publication date: June 18, 2020
    Applicant: FPInnovations
    Inventors: Xiaolin CAI, Fabrice ROUSSIERE, Lin HU, Xixian (James) DENG, Anes OMERANOVIC, Ayse ALEMDAR-THOMSON, Gilles BRUNETTE
  • Publication number: 20200148835
    Abstract: The present relates to a process for the depolymerization of lignin using chemicals recoverable by the soda or kraft mill recovery cycles. The process involves the use of sodium hydroxide or white liquor to depolymerize lignin in black liquor or other lignins (e.g. hydrolysis lignin, kraft lignin) by conducting the reaction at 170-250° C. for up to 3 hours in the presence or absence of a co-solvent and a capping agent. The depolymerized lignin is then obtained by acidifying the reaction products to a low pH to precipitate the de-polymerized lignin, followed by particle coagulation, cake filtration and washing with acid and water to obtain a purified depolymerized lignin product.
    Type: Application
    Filed: May 8, 2018
    Publication date: May 14, 2020
    Applicant: FPInnovations
    Inventors: Michael PALEOLOGOU, Zaid AHMAD, Chunbao XU
  • Publication number: 20200040143
    Abstract: An acidic water-based process was developed for the synthesis of anionic lignin copolymers with adjustable MW, thermal stability and solubility in water. The anionic lignin copolymer described herein comprises: a molecular weight of 5,000 to 7.4×105 g/mol; and a charge density of ?1 to ?7.2 meq/g. The anionic lignin copolymers described herein which have a molecular weight range of 000-50,000 g/mol can be used as dispersants of negatively charged molecules or particles in numerous process or wastewater streams (e.g. concrete admixtures, gypsum slurries, textile dye) while such copolymers in a molecular weight range of 90,000-740,000 g/mole can be used as flocculants of positively charged molecules or particles in numerous process and wastewater streams including industrial and municipal systems and sludge dewatering in the textile dye, pulp & paper, mining and oil industries.
    Type: Application
    Filed: March 7, 2018
    Publication date: February 6, 2020
    Applicants: FPInnovations, LAKEHEAD UNIVERSITY
    Inventors: Pedram FATEHI, Fangong KONG, Shoujuan WANG, Jacquelyn PRICE, Michael PALEOLOGOU
  • Publication number: 20190360151
    Abstract: The present disclosure is directed to a Pickering emulsion comprising cellulose filaments. The heterogeneity of the cellulose filament material is critical and beneficial to the formation of stable emulsions. Emulsions with high stability can be prepared by controlling the CF surface properties. It is provided an emulsion comprising an internal phase dispersed in a continuous external phase and cellulose filaments located at the interface of the internal phase and the external phase, wherein the emulsion comprises 50% in volume or more of the internal phase and a method of producing same.
    Type: Application
    Filed: June 16, 2017
    Publication date: November 28, 2019
    Applicant: FPInnovations
    Inventors: Wadood Yasser HAMAD, Chuanwei MIAO