Patents Assigned to Fujian Changting Golden Dragon Rare-Earth Co., Ltd
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Publication number: 20240145137Abstract: A main and auxiliary alloy-based neodymium-iron-boron magnet material and the preparation method thereof. The raw material composition for the main and auxiliary alloy-based neodymium-iron-boron magnet material includes a main alloy raw material and an auxiliary alloy raw material, wherein the mass percentage of the auxiliary alloy raw material in the raw material composition for the main and auxiliary alloy-based neodymium-iron-boron magnet material is 1.0-15.0 mass %. For the main and auxiliary alloy-based neodymium-iron-boron magnet material prepared by using the raw material composition, the coercivity is increased while high remanence is ensured, and the preparation method therefor can be suitable for engineering applications.Type: ApplicationFiled: January 17, 2022Publication date: May 2, 2024Applicant: Fujian Changting Golden Dragon Rare-Earth Co., LtdInventors: Xing WEI, Jiaying HUANG, Zhihui TANG, Qingfang HUANG, Zhipeng JIANG, Deqin XU, Dakun CHEN, Gang FU
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Publication number: 20240127996Abstract: A R-T-B magnet and a preparation method thereof. The R-T-B magnet includes the following components of: ?30.0 wt % of R, said R is a rare earth element; 0.16-0.6 wt % of Cu; 0.4-0.8 wt % of Ti; ?0.2 wt % of Ga; 0.955-1.2 wt % of B; and 58-69% of Fe; wherein wt % is the mass percentage of respective component in the total mass of all components. The R-T-B magnet has higher remanence, coercivity, squareness and high-temperature stability.Type: ApplicationFiled: January 17, 2022Publication date: April 18, 2024Applicant: FUJIAN CHANGTING GOLDEN DRAGON RARE-EARTH CO., LTDInventors: Weiguo MOU, Jiaying HUANG
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Patent number: 11636976Abstract: Disclosed are a device and method for continuously performing grain boundary diffusion and heat treatment, characterized in that the alloy workpiece or the metal workpiece are arranged in a relatively independent processing box together with a diffusion source; the device comprises, in successive arrangement, a grain boundary diffusion chamber, a first cooling chamber, a heat treatment chamber, and a second cooling chamber, and a transfer system provided between various chambers for delivering the processing box; each of the first cooling chamber and the second cooling chamber uses an air cooling system, and the cooling air temperature of the first cooling chamber is above 25° C. and at least differs by 550° C. from the grain boundary diffusion temperature of the grain boundary diffusion chamber; the cooling air temperature of the second cooling chamber is above 25° C. and at least differs by 300° C.Type: GrantFiled: November 5, 2018Date of Patent: April 25, 2023Assignee: Fujian Changting Golden Dragon Rare-Earth Co., LtdInventors: Qingjiang Wang, Zongbo Liao, Yulin Lin, Changgeng Huang
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Patent number: 11508519Abstract: Disclosed are a continuous heat treatment device and method for a sintered Nd—Fe—B magnet workpiece. The device comprises a first heat treatment chamber, a first cooling chamber, a second heat treatment chamber, and a second cooling chamber continuously disposed in sequence, as well as a transfer system disposed among the chambers to transfer the alloy workpiece or the metal workpiece; both the first cooling chamber and the second cooling chamber adopt a air cooling system, wherein a cooling air temperature of the first cooling chamber is 25° C. or above and differs from a heat treatment temperature of the first heat treatment chamber by at least 450° C.; a cooling air temperature of the second cooling chamber is 25° C. or above and differs from a heat treatment temperature of the second heat treatment chamber by at least 300° C. The continuous heat treatment device and method can improve the cooling rate and production efficiency and improve the properties and consistency of the products.Type: GrantFiled: October 9, 2018Date of Patent: November 22, 2022Assignee: Fujian Changting Golden Dragon Rare-Earth Co., LtdInventors: Qingjiang Wang, Ying Luo, Jianpeng Wu
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Patent number: 11501914Abstract: The present invention discloses a grain boundary diffusion method of an R—Fe—B series rare earth sintered magnet, an HRE diffusion source, and a preparation method thereof, comprising the following steps: engineering A of forming a dry layer on a high-temperature-resistant carrier, the dry layer being adhered with HRE compound powder, the HRE being at least one of Dy, Tb, Gd, or Ho; and engineering B of performing heat treatment on the R—Fe—B series rare earth sintered magnet and the high-temperature-resistant carrier treated with the engineering A in a vacuum or inert atmosphere and supplying HRE to a surface of the R—Fe—B series rare earth sintered magnet. The method can reduce the consumption of heavy rare earth element and control the loss of residual magnetism Br while increasing the coercivity.Type: GrantFiled: September 21, 2017Date of Patent: November 15, 2022Assignee: Fujian Changting Golden Dragon Rare-Earth Co., LtdInventors: Yulin Lin, Hiroshi Nagata, Zongbo Liao, Juhua Xie, Hanshen Ye
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Patent number: 10971289Abstract: Disclosed in the present invention is a composite R—Fe—B based rare-earth sintered magnet comprising Pr and W, wherein the rare-earth sintered magnet comprises an R2Fe14B type main phase, and R is a rare-earth element comprising at least Pr, wherein the raw material components therein comprise more than or equal to 2 wt % of Pr and 0.0005 wt %-0.03 wt % of W; and the rare-earth sintered magnet is made through a process comprising the following steps: preparing molten liquid of the raw material components into a rapidly quenched alloy; grinding the rapidly quenched alloy into fine powder; obtaining a shaped body from the fine powder by using a magnetic field; and sintering the shaped body. By adding a trace amount of W into the rare-earth sintered magnet, the heat resistance and thermal demagnetization performance of the Pr-containing magnet are improved.Type: GrantFiled: September 23, 2016Date of Patent: April 6, 2021Assignees: XIAMEN TUNGSTEN CO., LTD., Fujian Changting Golden Dragon Rare-Earth Co., LtdInventor: Hiroshi Nagata
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Patent number: 10717131Abstract: The present invention discloses a method of manufacturing, powder making device for rare earth magnet alloy powder, and a rare earth magnet. The method comprises a process of fine grinding at least one kind of rare earth magnet alloy or at least one kind of rare earth magnet alloy coarse powder in inert jet stream with an oxygen content below 1000 ppm to obtain powder that has a grain size smaller than 50 ?m. Low oxygen content ultra-fine powder having a grain size smaller than 1 ?m is not separated from the pulverizer, and the oxygen content of the atmosphere is reduced to below 1000 ppm in the pulverizer when crushing the powder. Therefore, abnormal grain growth (AGG) rarely happens in the sintering process. A low oxygen content sintered magnet is obtained and the advantages of a simplified process and reduced manufacturing cost are realized.Type: GrantFiled: March 27, 2018Date of Patent: July 21, 2020Assignees: XIAMEN TUNGSTEN CO., LTD., FUJIAN CHANGTING GOLDEN DRAGON RARE-EARTH CO., LTDInventors: Hiroshi Nagata, Chonghu Wu
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Patent number: 10614938Abstract: The present invention discloses a W-containing R—Fe—B—Cu serial sintered magnet and quenching alloy. The sintered magnet contains an R2Fe14B-type main phase, the R being at least one rare earth element comprising Nd or Pr; the crystal grain boundary of the rare earth magnet contains a W-rich area above 0.004 at % and below 0.26 at %, and the W-rich area accounts for 2.0 vol %˜11.0 vol % of the sintered magnet. The sintered magnet uses a minor amount of W pinning crystal to segregate the migration of the pinned grain boundary in the crystal grain boundary to effectively prevent abnormal grain growth and obtain significant improvement. The crystal grain boundary of the quenching alloy contains a W-rich area above 0.004 at % and below 0.26 at %, and the W-rich area accounts for at least 50 vol % of the crystal grain boundary.Type: GrantFiled: May 13, 2019Date of Patent: April 7, 2020Assignees: XIAMEN TUNGSTEN CO., LTD., Fujian Changting Golden Dragon Rare-Earth Co., LtdInventors: Hiroshi Nagata, Rong Yu, Qin Lan
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Patent number: 10468168Abstract: Disclosed is a Ho and W-containing rare-earth magnet. The rare-earth magnet comprises a R2Fe14B type principal phase, and comprises the following raw material components: R: 28 wt % to 33 wt %, wherein R is a raw-earth element comprising Nd and Ho, and the content of Ho is 0.3 wt % to 5 wt %; B: 0.8 wt % to 1.3 wt %; W: 0.005 wt % to 0.3 wt %, and the balance of T and inevitable purities, wherein T is an element mainly comprising Fe and/or Co. The rare-earth magnet mainly consists of a W-rich grain boundary phase and a Ho-rich principal phase; crystal grain growth of the Ho-containing magnet in a sintering process is constrained by the trace of W, thereby preventing AGG from occurring on the Ho-containing magnet, and obtaining a magnet with high coercivity and high heat resistance.Type: GrantFiled: April 4, 2016Date of Patent: November 5, 2019Assignees: XIAMEN TUNGSTEN CO., LTD., FUJIAN CHANGTING GOLDEN DRAGON RARE-EARTH CO., LTDInventors: Hiroshi Nagata, Jianhong Zhang
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Patent number: 10381141Abstract: The present invention discloses manufacturing methods of a powder for compacting rare earth magnet powder and rare earth magnet that omit jet milling process, which comprises the steps as follows: 1) casting: casting the molten alloy of rare earth magnet raw material by strip casting method to obtain a quenched alloy with average thickness in a range of 0.2˜0.4 mm; 2) hydrogen decrepitation: decrepitating the quenched alloy and a plurality of rigid balls into a rotating hydrogen decrepitation container simultaneously, the quenched alloy is crushed under a hydrogen pressure between 0.01˜1 MPa, cooling the alloy and the balls, then screening the mixture to remove the rigid balls and obtain the powder. As the jet milling process is omitted, the oxygenation during the process of the jet milling may be avoided, therefore the process may be non-oxide, and the mass production of magnet with super high property may be possible.Type: GrantFiled: November 8, 2013Date of Patent: August 13, 2019Assignees: Xiamen Tungsten Co., Ltd., Fujian Changting Golden Dragon Rare-Earth Co., LtdInventors: Hiroshi Nagata, Chonghu Wu
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Patent number: 10381139Abstract: The present invention discloses a W-containing R—Fe—B—Cu serial sintered magnet and quenching alloy. The sintered magnet contains an R2Fe14B-type main phase, the R being at least one rare earth element comprising Nd or Pr; the crystal grain boundary of the rare earth magnet contains a W-rich area above 0.004 at % and below 0.26 at %, and the W-rich area accounts for 5.0 vol %˜11.0 vol % of the sintered magnet. The sintered magnet uses a minor amount of W pinning crystal to segregate the migration of the pinned grain boundary in the crystal grain boundary to effectively prevent abnormal grain growth and obtain significant improvement. The crystal grain boundary of the quenching alloy contains a W-rich area above 0.004 at % and below 0.26 at %, and the W-rich area accounts for at least 50 vol % of the crystal grain boundary.Type: GrantFiled: June 17, 2016Date of Patent: August 13, 2019Assignees: Xiamen Tungsten Co., Ltd., Fujian Changting Golden Dragon Rare-Earth Co., LtdInventors: Hiroshi Nagata, Rong Yu, Qin Lan